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HomeMy WebLinkAboutVolume I GME - Response Action Plan Implementation Report SW Corner of 58th St. N & Oakgreen Ave N 1 1 1 I i ' RESPONSE ACTION PLAN IMPLEMENTATION REPORT OUTLOT E 1 SOUTHWEST CORNER OF 58TH STREET NORTH AND OAKGREEN AVENUE NORTH OAK PARK HEIGHTS, MINNESOTA GME PROJECT NO. 7735-E VOLUME I 1 1 Prepared for: Senior Housing Partners 2845 North Hamline Avenue, Suite 100 Roseville, Minnesota 55113 I August 12, 2005 i 1 Copyright, 2005 - GME Consultants, Inc. 1 11 GME CONSULTANTS.INC. I GME CONSULTANTS, INC. Erg Geotechnical • Materials • Environmental Engineers 14000 21st Ave. No. / Minneapolis, MN 55447 E �;, Phone (763) 559-1859 / Fax (763) 559-0720 I/ August 12 , 2005 Mr. Mike Price Senior Housing Partners 2845 North Hamline Avenue, Suite 100 Roseville, Minnesota 55113 GME Project No. 7735-E RE: Response Action Plan Implementation Report for Outlot E in the southwest quadrant of 58th Street North and Oakgreen Avenue North in Oak Park Heights, Minnesota Dear Mr. Price : In accordance with Mr. Allen Black' s written authorization of our contract dated November 7, 2004 , we have completed our services for this phase of the project . The purposes of this report are to ' summarize and interpret the results of the field and laboratory work. We appreciate this opportunity to be of service to you. If you have questions regarding this report, please contact us . Sincerely, GME CONSULTANTS/ ILC. I of ', • Eric P. S. mes Senior E►, ronmental Scientist Project Manager I EPS : jmg W:\EPS\7735-E RAP.jmg I I WILLIAM C. KWASNY, P.E. THOMAS P. VENEMA, P.E. GREGORY R. REUTER, P.E., P.G. RYAN F. SCHMIDT, P.E. WILLIAM BLOEMENDAL, P.E. RICHARD W. PENNINGS, P.E. An Equal Opportunity Employer 1 . TABLE OF CONTENTS IRESPONSE ACTION PLAN IMPLEMENTATION REPORT 1 OUTLOT E IN SOUTHWEST CORNER OF 58TH STREET NORTH AND OAKGREEN AVENUE NORTH OAK PARK HEIGHTS, MINNESOTA GME PROJECT NO. 7735-E SECTION PAGE 1 . INTRODUCTION 1 2 . PROJECT LOCATION 1 3 . PREVIOUS EXPLORATION RESULTS 1 3 . 1 Phase I Environmental Site Assessment 1 3 . 2 Phase II Environmental Site Assessment Report 2 3 . 3 Surficial Clean-up of Debris on the Property 3 3 .4 Limited Soils Assessment 4 4 . PROJECT DESCRIPTION AND APPROVALS 5 II5 . RAP RESULTS 5 5 . 1 Area 1 6 5 . 2 Area 2 7 5 . 3 Area 3 7 6 . CONCLUSIONS 7 II 7 . RECOMMENDATIONS 8 8 . GENERAL QUALIIFICATIONS 8 9 . SIGNATURES 9 FIGURES Figure 1 : Regional Location Diagram Figure 2 : Test Pit Location Diagram (11-17-05) Figure 3 : Confirmation Soil Sample Location Diagram 1 1 GME CONSULTANTS.INC. II ITABLE OF CONTENTS (Continued) RESPONSE ACTION PLAN IMPLEMENTATION REPORT OUTLOT E IN SOUTHWEST CORNER OF I 58TH STREET NORTH AND OAKGREEN AVENUE NORTH OAK PARK HEIGHTS, MINNESOTA GME PROJECT NO. 7735-E I TABLES ITable 1 : Test Pit Observations (11-17-04) Table 2 : Soil Chemistry Results (Stockpile samples) I Table 3 : Soil Chemistry Results (Confirmation Samples) IAPPENDICES Appendix A: Phase I ESA report of May 28, 1999 IIAppendix B: Phase II ESA report of August 9, 1999 Appendix C: Legend Technical Services, Inc. Laboratory Report Appendix D: EMSL Analytical Reports Laboratory Reports I Appendix E: GME Photographic Record Appendix F: EnChem, Inc. Laboratory Reports Appendix G: SKB Environmental Manifests & Ticket Summary I I I I I I I I ' GME CONSULTANTS,INC. I 1. INTRODUCTION This Response Action Plan/Contingency Plan (RAP/CP) Implementation Report has been prepared to summarize the results of the response actions undertaken to remove impacted fill soil with debris from Outlot E near the southwest quadrant of 58th Street North and Oakgreen Avenue North in Oak Park Heights, Minnesota. Senior Housing Partners, Inc . entered into the Minnesota Pollution Control Agency (MPCA) Voluntary Investigation and Cleanup the Voluntary Petroleum Brownfields Pro ram (VIC) Program and liability assurance letters regarding environmental conditions. Although a Response Action Plan (RAP) was not approved by either voluntary program because of project time constraints, we did discuss aspects of the project with Ms . Stacy Hendry-Vanpatten with the PBP on November 23 , 2004 and Mr. Larry Quandt with the VIC Program on December 15, 2004 . This work was authorized by Mr. Allen Black with Senior Housing Partners on November 10, 2004 . 2 . PROJECT LOCATION The Property is southwest of the intersection of 58th Street North and Oakgreen Avenue North in Oak Park Heights, Minnesota. The Property lies in the northwest quadrant of Section 5, Township 29 North and Range 20 West, Washington County, Minnesota. A Regional Location Diagram is presented as Figure 1 . A detailed diagram of the Property is presented as Figure 2 . 3 . PREVIOUS EXPLORATION RESULTS 3 . 1 Phase I Environmental Site Assessment On May 28, 1999, we completed a Phase I Environmental Site Assessment (ESA) on a larger site including the Property; the larger site included the parcel north of 58th Street North. Historically, a greenhouse and garage occupied the Property (Outlot E) . The former greenhouse was reportedly used to grow winter vegetables, flowers, and house plants; they also operated a landscape business from this location where vehicle and equipment maintenance occurred in the former garage. In the early 1970s, the greenhouse was razed, except for the north wall of the building. During our site reconnaissance in 1999, we observed several piles of landscaping supplies, tires, vehicle parts, dimensional lumber, concrete block, household appliances, metal fencing, and other landscape equipment on the Property. ' GME CONSULTANTS,INC. I II Mr. Mike Price 2 GME Project No. 7735-E August 12, 2005 IIDuring the Phase I ESA, the former owner explained floor drain was present in the basement of heformer greenhouse IIoffice . This drain was reportedly used to prevent flooding of the basement and was connected to concrete tank located south of the former garage . During our site reconnaissance, we observed an Iaccess pipe for this tank, and liquid was present in the tank. The on-site recognized environmental conditions (RECs) included a IIburied concrete tank next to the south side of the former garage, a 265-gallon fuel oil above-ground storage tank (AST) without secondary containment, vehicle maintenance in the former garage IIsince at least 1938, scattered piles of fill soil/debris across the Property, and the coal-fired heating system that was used in the former greenhouse. IIThe off-site RECs included the Baytown plume a Y own Township groundwater contaminant P approximately mile south of the Property and the II presence of a salvage yard (former Stillwater Auto Parts) to the north. A copy of the Phase I ESA is appended. II3 .2 Phase II Environmental Site Assessment Report On August 9, 1999, we completed a Phase II ESA Report on the ll: Property. We assessed the RECS that we identified in the Phase I ESA, by observing and monitoring test pits that were excavated by others on the Property. We observed the soil conditions and collected soil samples for field and laboratory analytical testing; groundwater was not encountered during this assessment . Based on the Minnesota Geological Survey (MGS) Geologic Atlas for Washington I County, groundwater is likely deeper than 100 feet below grade. Our subcontract laboratory, Enchem, Inc . (Enchem) detected shallow II petroleum impacts including diesel range organics (DRO) at 5 . 6 and 16 parts per million (ppm) , in the gravel driveway east of the former garage . During our Phase I ESA, we observed oil staining on II the surface of the driveway. In this same area, we also collected a soil sample from 4 to 6 feet below for analytical testing; there were no detections of DRO, gasoline range organics (GRO) , or I volatile organic compounds (VOCs) . We also identified petroleum impacts beneath the former wood debris II pile, west of the garage . The laboratory detected DRO at 58 ppm from the soil sample collected from 0 to 4 feet below grade; there were no detections of DRO, GRO, or VOCs in the soil sample collected I from 4 to 6 feet below grade . I/ GME CONSULTANTS,INC. I Mr. Mike Price 3 August 12, 2005 GME Project No. 7735-E A test pit was excavated on the east side of the concrete tank, located south of the former garage . The top of the tank was about 6 feet below grade and the base was about 4 feet deeper. We did not observe staining or unusual odors in the soil samples collected from this test pit . We collected a liquid sample from this tank for analytical testing of GRO, DRO, VOCs, and Minnesota Department of Agriculture (MDA) List 1 base/neutral pesticides . Enchem only detected DRO at 490 ug/L. We collected a composite soil sample inside the footprint of the former greenhouse that was analyzed by MVTL Laboratories, Inc. (MVTL) for MDA List 1 pesticides . Alachlor (Lasso) was detected at 0 . 13 parts per million (ppm) and Metolachlor (Dual) was detected at 0 . 05 ppm. These levels are below the MDA Preliminary Soil Cleanup Goals using a moderate to low risk to groundwater scenario for these compounds . We collected a sample of the fill in the former greenhouse basement that was analyzed for polynuclear aromatic hydrocarbons (PAHs) and the eight RCRA metals . The metals results were either below reporting limits or within the range of naturally-occurring concentrations for this area, in our opinion. In the PAH analysis, Enchem detected five constituents, but they were below MPCA residential soil reference values (SRVs) . We also collected a soil sample from below the 265-gallon AST located on the west side of the former garage . We did not observe soil staining or detect an elevated PID reading, but Enchem detected DRO at 4 . 9 ppm. We also identified buried debris on the west side of the garage in the former greenhouse basement . The Phase II ESA Report and appended. 3 .3 Surficial Clean-up of Debris on the Property In May 2000, Senior Housing Partners contracted Ray Anderson and Sons, Inc . to raze the garage on the Property, remove the concrete tank (cistern) on the south side of the garage, and remove additional surficial debris on the Property. GME was not contracted to observe these clean-up measures . On July 21, 2005, Mr. Richard Orthmeyer with Ray Inc . said that they completed clean-up activities between May 9 and 23 , 2000 . Mr. Orthmeyer explained that about 50 loads (about 35 to 45 cubic yards) of construction-related debris was removed from the I/ Property and disposed of at the SKB landfill in Rosemount, GME CONSULTANTS,INC. 1 IIMr. Mike Price 4 August 12 , 2005 GME Project No. 7735-E 1 Minnesota. He added that they hauled about 80 loads of concrete rubble and brick, mostly consisting of the former greenhouse 1 footings and floor slab of the garage, to several concrete recyclers in the area. In addition, they hauled about eight loads of brush and stumps and three smaller loads of tires, to recycling IIfacilities . 3 .4 Limited Soils Assessment IOn November 17, 2004 , Bolander and Sons Company excavated 21 test pits on the Property ranging from 2 to 5 feet below grade to further II assess the vertical and horizontal extents of the previously identified impacted soil with debris and to further characterize the waste for off-site disposal . We also collected soil samples from I the test pits and conducted field headspace testing using a photoionization detector (PID) which can detect certain volatile vapors in parts per million. Bolander backfilled the test pits with 1 the excavated soil and then bucket compacted the pit . We identified and delineated three areas (Areas 1, 2 , and 3) with II soil impacts and/or buried debris (Figure 2) ; we did not observe groundwater during this assessment . Our test pit observations are described in Table 1 . IIIn Area 1, we found dark brown fill soil with debris consisting of pieces of concrete, stumps, branches, and metal with lesser amounts II of glass and plastic ranging in depth from 2 to 4 feet . This fill was underlain by naturally-occurring reddish-brown silty sand and sandy clay. Based on our observations, it appears that Area 1 was 1 likely a former depression that had been filled in the past . The north, west, and south extents of the dump ended near the adjoining tree lines; the eastern extent of the dump was about 50 feet west of Ithe former garage. We also collected three soil samples from Area 1 labeled SP-1, SP-2 , 1 and SP-3 . Enchem analyzed SP-1 for PCBs, priority pollutant pesticides, herbicides (2, 4-D, and 2 , 4 , 5-TP-Silvex) and samples SP-2 and SP-3 for PCBs, eight RCRA metals, priority pollutant pesticides, 1 and herbicides; SP-2 was also analyzed for GRO, DRO, and VOCs . The testing of samples these samples revealed that DRO was detected in SP-2 at 48 ppm. There were no detections of GRO, PCBs, and VOCs 1 above laboratory reporting limits . In the RCRA metal analyses, the lead concentrations in SP-2 and S-3 were 64 and 88 ppm, which are below MPCA residential soil reference values (SRVs) and Tier 1 soil 1 leaching values (SLVs) . In samples SP-2 and SP-3 , Enchem detected several PAH constituents at relatively low levels; the I/ benzo (a) pyrene (BaP) equivalent calculation for SP-2 was 2 . 15 ppm GME CONSULTANTS,INC. I IIMr. Mike Price 5 August 12, 2005 GME Project No. 7735-E IIand for SP-3 at 1 . 99 ppm. The residential SRV for the BaP equivalent is 2 ppm and the Tier 1 SLV is 10 . 2 ppm. In the I herbicide and pesticide analyses, Enchem detected low levels of 4, 4-DDE, 4 , 4-DDT, a-chlordane, gamma-chlordane, and heptachlor epoxide (Table 2) . In addition, we did not record PID readings above 1 background level or about 3 ppm. Area 2 was located east of the former garage, where we had observed 1 soil staining on the surface of the gravel driveway. Test pits were not located in this area, because the extents of the shallow impacts had been previously identified. IIThe former greenhouse basement occupied Area 3 . Within the fill soil, we observed red bricks, likely from the former chimney, 1 several pieces of plastic, and a concrete slab about 7 feet below grade. We also observed portions of the former basement walls . 1 During this assessment, we observed suspect asbestos-containing material (ACM) in Areas 1 and 3, and our GME Certified Asbestos 11 Inspector mobilized to the site to collect samples for analytical testing. The suspect ACM included asphalt shingles and a piece of material that appeared to be floor tile. We collected six pieces of suspect ACM; EMSL Analytical, Inc . (EMSL) analyzed the samples for 1 asbestos . EMSL did not detect asbestos above 1% in the six samples that we submitted. The EMSL analytical results are appended. I Three test pits also were excavated within the former garage footprint . In these test pits, we did not observe stained soil, debris, or detect elevated PID readings . 1 4 . PROJECT DESCRIPTION AND APPROVALS ISenior Housing Partners elected to remove the identified soil impacts and buried debris for the purpose of preparing the Property for development or sale in the future . Prior to completing the Iremoval of the soil and debris, the City of Oak Park Heights required that Senior Housing Partners obtain a conditional use permit (CUP) because this clean-up fell under the City' s Land 1 Reclamation and Grading Ordinance - 308 . 08 . In addition, prior to excavation on the Property, Senior Housing Partners obtained approval to dispose of the material at the SKB Landfill in IIRosemount, Minnesota. 5 . RAP RESULTS IIOn March 1 and 7, 2005, Bolander "ripped" the frost ost in Areas 1, 2, and 3 that ranged from 1 to 4 feet below grade. On March 3, 4, and 1 GME CONSULTANTS,INC. I Mr. Mike Price 6 August 12, 2005 GME Project No. 7735-E 8, 2005, Bolander excavated impacted soil with debris in the three areas . The impacted soil with debris was directly placed into end dumps and trucked to the SKB Landfill in Rosemount, Minnesota. Shortly after removal of the fill soil with debris, Bolander backfilled the excavations with an environmentally clean (non- 11 impacted) sandy fill (see appended GME Photographic Record) . During excavation, our GME Environmental Scientist observed the excavated material for signs of unusual soil conditions and debris and also conducted field headspace testing with a PID on each soil sample collected for about every 10 cubic yards of soil removed. In addition, our Licensed Certified Asbestos Inspector observed the excavated material for suspect ACM. 5 . 1 Area 1 During the excavation of Area 1, we observed fill soil with pieces of concrete, asphalt, brick, dimensional lumber, branches, stumps, metal debris, broken glass, fencing, and several tires . We did not observe possible hazardous substances such as intact containers, unusual sludges, powders, or additional suspect ACM. The excavation depth ranged from 2 to 4 feet, except for two deeper excavations to about 9 feet below grade to remove buried tree stumps. Following the removal of the fill soil and debris from Area 1, we collected eight confirmation soil samples from the base of the excavation and seven samples from the sidewalls (Figure 3) . We did not collect confirmation soil samples from the west and a portion of the north sides, because the sidewall had been completely removed; these two sides sloped downward towards a wooded area. The confirmation soil samples were analyzed for DRO, RCRA metals, PAHs, and the priority pollutant pesticides . During our field headspace testing of the excavated soil from Area 1, we did not detect elevated PID readings above 3 ppm, which is indicative of background level, in our opinion. In the analytical testing of the confirmation bottom and sidewall samples, Enchem did not detect DRO above reporting limits and the RCRA metal results were near naturally-occurring levels for this area and below MPCA residential SRVs and Tier 1 SLVs (Table 3) . In the PAH analysis, fluoranthene was detected in samples B-4 (5 feet) and S-5 (2 feet) ; these concentrations were just above reporting limits and well below applicable MPCA residential SRVs and Tier I SLVs . In sample B-5 (9 feet) , EnChem detected several PAHs, but the BaP equivalent calculation was 0 . 04 ppm, which is well below the MPCA residential SRV of 2 ppm and Tier 1 SLV of 10 . 2 ppm. In the priority pollutant pesticide analysis, 4, 4-DDE and 4, 4-DDT were GME CONSULTANTS,INC. I Mr. Mike Price 7 GME Project No. 7735-E August 12, 2005 detected at 0 . 041 and 0 . 015 ppm, respectively, in sample S-5 (2 feet) ; the MPCA residential SRV for 4, 4-DDE is 40 and 4, 4-DDT is 15 ppm. 5.2 Area 2 Area 2 is located on the east side of the former garage . Durin g our Phase I ESA, we observed soil staining on the surface likely from vehicles that had been repaired or stored there. The excavation was approximately 18 feet wide by 42 feet long and about 2 . 5 feet deep. Following excavation of the soil, we collected four confirmation soil samples from the sidewalls and two confirmation samples from the base of the excavation (Figure 3) . EnChem analyzed these samples for DRO, GRO, and benzene, toluene, ethylbenzene, xylenes, and methyl tertiary butyl ether (MTBE) . There were no detections above EnChem' s reporting limits . 11 Bolander also excavated a test pit in the former location of the fuel oil AST formerly located on the west side of the garage. We collected sample TP-10 (3 feet) for DRO testing. Enchem did not detect DRO above their reporting limit . 5.3 Area 3 Area 3 is located to the southeast of the former reportedly occupied by the former greenhouse basement. During our Phase II ESA, we collected a soil sample from this fill material and detected low levels of PAHs and observed a limited amount of debris . The excavation was about 12 feet wide by 17 feet long and about 7 feet deep. At 7 feet below grade, Bolander encountered a concrete floor slab. During the excavation of this fill within the former basement, we observed several pieces of red chimney brick, pieces of concrete and plastic, and the apparent base of the chimney, and an apparent coal stoker. After Bolander removed the floor slab and remaining concrete walls of the basement, we collected four confirmation soil samples from the sidewalls and one confirmation soil sample from the base of the excavation (Figure 3) . Enchem analyzed these soil samples for DRO and PAH analyses . There were no detections of analyzed parameters above EnChem' s reporting limits . 6. CONCLUSIONS During our Phase I and Phase II ESAs in level petroleum impacts along with buried debris in nldthreef areas lon the Property (Areas 1, 2 , and 3) . In 2000, Senior Housing Partners subcontracted Ray Anderson and Sons to raze the garage and remove the surficial debris including concrete, brush, tires and other GME CONSULTANTS,INC. 1 IIMr. Mike Price 8 August 12, 2005 GME Project No. 7735-E 1 construction-related debris; the concrete tank (cistern) was also reportedly removed at this time . This material was either hauled to II the SKB landfill or recycled. From 2000 to 2005, the Property reportedly remained vacant . In March 2005, response actions were undertaken to remove the impacted soil with buried debris in areas II discussed above . Based on the SKB load tickets, approximately 2, 016 tons of impacted soil with debris was hauled to the SKB Landfill in Rosemount, Minnesota. The waste manifests are appended. Shortly il after excavation of these areas, they were backfilled by Bolander with a clean sandy fill . tBased on the results of our field observations and analytical testing, it appears that the impacted soil and buried debris in Areas 1, 2 , and 3 has been removed and properly disposed of at the 11 SKB landfill . The analytical testing of the soil samples from the bases and sidewalls of the three excavations indicate that the soil impacts have been removed, except in two locations in Area 1 where Enchem detected several low detections of PAHs and pesticides; however, these residual concentrations are well below applicable MPCA SRVs and Tier I SLVs . i7 . RECOMMENDATIONS I We recommend that you submit this Implementation Report to the MPCA VIC Program for their review and request a limited "No Action" letter for soil . If you elect to pursue a "Retroactive No I Association Determination" letter, the MPCA will require an affidavit listing the names and addresses of the individuals requesting the determination, a past actions letter that includes a statement on any past association with the Property and releases at I the Property, and an affidavit including a statement that the party did not contribute or associate itself in any manner with the IIreleases to be named in the determination. We also recommend that this report be submitted to the MPCA II Petroleum Brownfields (PBP) requesting a non-tank site file closure letter. II8. GENERAL QUALIIFICATIONS II The interpretations and conclusions submitted in this report are based on the data produced during our observations and screening. This report does not account for any variations that may occur II between or outside of the sampling locations . Furthermore, we did not explore outside of the excavation areas . We were not responsible for hauling or disposal of the soil . IIGM CONSULTANTS,INC. I IIMr. Mike Price GME Project No. 7735-E 9 August 12, 2005 I The conclusions in this report represent our professional judgment . IWe have endeavored to prepare this report in accordance with the current local standard of practice for our profession, using the normally available sources of information. No warranty, express or IIimplied, is presented in this report with respect to the environmental conditions at this Property. I9. SIGNATURES We appreciate the opportunity to work with you on this project . If you have questions regarding this report, please contact us . II II Prepared by: IEri f p. .. mes Senior E vironmental Scientist Project Manager Reviewed by: i G4 Richard W. Pennings, P.E. Senior Environmental Engineer Icc: Mr. Eric Johnson City of Oak Park Heights I EPS :j mg W:\EPS\7735-E RAP.jmg I I I II ME CONSULTANTS,INC. I I I I I FIGURES FIGURE 1: REGIONAL LOCATION DIAGRAM FIGURE 2 : TEST PIT LOCATION DIAGRAM FIGURE 3 : CONFIRMATION SOIL SAMPLE LOCATION O DIAGRAM I GRAM I I I t I 1 I I 1 I I IThis diagram was created using portions of the Stillwater Minnesota USGS Quadrangle Topographic Map I � --� f ' l' ri it:11 '','"'Tf– i-::.----71.'--:---- ---" .ti:l..:,_1':;;;1,1 --I-..-r'',.. 141,11;:::,1 —41 1 •I' kiiihraiii;" t .'-'"/CI :I I t a li 1 "-') i . I • all ) .. 440,344:3 ' ' I ° J. --- (i. ....,../..,:,,IL) i , ,,, , ,„„ pi c-7___,..., , ,A.:: 4 i ,,,,).4----: •li# , ) CN- �� L---_ \, iada` f1 +� jjj f l,•J K xa'i p�-^� 5 ( ' !�� '1. L B ✓y. 1 :. '1✓ PROPERTY _ i • y ' ' y'" , ' 1 I1 r . LOCATION i �t.. '. � �, " ' : .•'-. . ' ..; '''' it). \ 1--t-i t I -! 1{ f --'f') v }' T/ - . _fi r____),.t krW ► ...._.r..,,ra r� _„t.„�e 1 Y'f mil, ,„"i,,,,,\ t� "1 f t .;„. I Ni.,, ,.e. c j -:-..., , 3,...e ,,,, .?,„ a ,-q \,.........: I c'N i i 1,,,,. _ '3'0,,,, _(__ _11\''d.n-,,, "7: '_'7 ..c-1.*; ,:c„ '1:0.l'1"4:r.i‘?"..rti '":). :0-7 't:: _..E''''. ± ''.1 I'''CI\''-'-•”'%-) I Scale 1 : 24,000 N I 0.5 0 0.5 1 Niles I GME CONSULTANTS, INC. REGIONAL LOCATION DIAGRAM �_: FIGURE 1: I/ Geotechnical•Materials•Environmental ,� 14000 2151 Avenue North OUTLOT E Minneapolis,Minnesota 55447 !" 58TH STREET NORTH AND OAKGREEN AVENUE NORTH (763)559-1859 %� !1_ OAK PARK HEIGHTS,MINNESOTA EPS EPS AUG-05 GME Project No. 7735-E NM MI an MI an on am i no on — on as w - um re an — OAKGREEN AVENUE NORTH I y/////////////// / / / / I / / / / / GARAGE / • / I / / / / / / //////////////// 1 WOODED AREA • 501-p-36 I APPROXIMATE–/' EDGE OF CURB 1— I X ITP-37 � AREA 2 I L I AREA 3 L_ —I \ flFORMERGARAGETPT CA X X X • I TP-33 TP-34 TP-35 I 20 N -o 1G o\ 58TH STREET NORTH oc\ ' \ r X TP-30 /� - - � _ ` TP,32 IX TP 31 ■ \ ITP-29 'g Q ■ AREA 1 T x21 TP 22 0 o 3 N o \ X WOODED \\P -20 AREA x TP-17 1 TP-18 \ 1 X X TP-23 TP-28 \\ T X19 \ \ • • ss _ I TP 24 TP-27 � � ■ TP-25/ TP-26 \ LEGEND —APPROXIMATE PROPERTY BOUNDARY \ 0 X TEST PIT LOCATION APPROXIMATE SCALE I I NOTE: ALL LOCATIONS ARE APPROXIMATE 0� FEET 30' GME CONSULTANTS, INC. FIGURE 2: TEST PIT LOCATION DIAGRAM (11-17-05) Geotechnical•Materials•Environmental OUTLOT E 14000 21st Avenue N. 1 / OAKGREEN AVENUE AND 58TH STREET NORTH Minneapolis,Minnesota 55447 ELF OAK PARK HEIGHTS, MINNESOTA 7735e.dwg (763)559-1859 VJL I EPS I AUG 05 I GME Project No. 7735-E MO In - - - In MB MI ■O NM MI N MN MI 1 w • OAKGREEN AVENUE NORTH I j/////////////// / / I GARAGE / / / I/ / / / //////////////// WOODED AREA S-10(3') DW-B-10(3') DW-S-15(1') S-9(3') • APPROXIMATE _ _ _ OW-B-1 1(3') S-11(3') EDGE OF CURB f B-9(7') L + DW—S-12(1') } • • • DW—S-14(1') s-8(3.) `AREA 3 LAREA 2• DW-S-13(1') \ FORMER GARAGE FOOTPRINT _1 0 • O 58TH STREET NORTH o� ' r S-6(2..) — S-7(2') S-3(2') 1 B• 4' S-7(2') cr \ • \ a AREA 1 B-1(3') \ \\ 5(2') • �tt 0 • S-2(2') WOODED \ B-6(3') B-4(5') I AREA B-3(3') • \ 1` I s-4(1') B-5(9') • \ B-2(4') \\ • LEGEND B-1(3') = CONFIRMATION BOTTOM SAMPLE LOCATION \ (11:1) S-1(2') = CONFIRMATION SIDEWALL SAMPLE LOCATION APPROXIMATE —' • —APPROXIMATE PROPERTY BOUNDARY SCALE 1 0' FEET 30' NOTE: ALL LOCATIONS ARE APPROXIMATE GME CONSULTANTS, INC. FIGURE3: CONFIRMATION SOIL SAMPLE LOCATION DIAGRAM Geotechn ical•Materials•Environmental �� OUTLOT E 14000 21st Avenue N. I�� OAKGREEN AVENUE AND 58TH STREET NORTH Minneapolis,Minnesota 55447 ELF OAK PARK HEIGHTS, MINNESOTA 7735e.dwg (763)559-1859 VJL I EPS I AUG 05 I GME Project No. 7735-E 1 1 1 1 ' TABLES TABLE 1: TEST PIT OBSERVATIONS S (11-17-04)(STOCKPILE SAMPLES) ' TABLE 2 : SOIL CHEMISTRY TABLE 3 : SOIL CHEMISTRY RESULTS (CONFIRMATION SAMPLES) 1 1 1 1 I 1 II ITABLE 1 TEST PIT OBSERVATIONS (NOVEMBER 17, 2004) I OUTLOT E 58TH STREET NORTH AND OAKGREEN AVENUE NORTH OAK PARK HEIGHTS, MINNESOTA IIGME PROJECT NO. 7735-E TEST PIT NUMBER DEPTH OF FILL/DEBRIS DEBRIS DESCRIPTION IITP-17 4 FEET CONCRETE, WOOD, BRICK CONCRETE, WOOD, BRICK, TP-18 4 FEET AND SHINGLES II TP-19 3 FEET CONCRETE CONCRETE, BRICK, METAL TP-20 2 FEET STRAP, AND ROCK II TP-21 3 FEET CAR HOOD, CONCRETE, WOOD, AND BRICK II NONE TP-22 NONE TP-23 NONE TP-24 NONE NONE LOGS, CONCRETE, TP-25 4 FEET BRANCHES TP-26 2 FEET BITUMINOUS II TP-27 NONE NONE TP-28 NONE NONE CONCRETE, ROCK, BRICK, TP-29 2 FEET BITUMINOUS II TP-30 NONE NONE TP-31 1 FOOT BRICK AND WOOD II TP-32 NONE NONE NONE NONE TP-33 TP-34 NONE NONE TP-35 NONE NONE II BRICK, PLASTIC, FLOOR TP-36 7 FEET TILE, AND CONCRETE SLAB BRICK, PLASTIC, AND TP-37 7 FEET CONCRETE SLAB II II I II II II ' TABLE 2 SOIL CHEMISTRY RESULTS (STOCKPILE SAMPLES) II OUTLOT E 58TH STREET NORTH AND OAKGREEN AVENUE NORTH OAK PARK HEIGHTS, MINNESOTA GME PROJECT NO. 7735-E PARAMETER SP-1 SP-2 SP-3 Residential TIER I SRV SLV DRO NA 48 NA - II GRO NA <4 .7 NA - - PCBs <0.24 <0.23 <0.23 1.2 2.1 VOCs NA ND NA - - II Mercury Arsenic NA <0.11 <0.12 0.7 1.6 NA 3 .2 4.1 10 15 .1 Barium NA 86 73 1,200 842 Cadmium NA 0.79 0.32 35 4 .4 II Chromium NA 13 15 71 (hex) 18 (hex) Lead NA 64 88 400 525 Selenium NA <0.57 <0.58 170 1.5 i Silver NA <0 .29 <0.29 170 3 .9 Acenaphthylene NA 0.43 0 .38 1,200 50 Benzo(a)anthracene NA 1.5 1.4 see BaP see BaP 1.6 1.5 see BaP see BaP Benzo(a)pyrene NA 1 8 see BaP see BaP Benzo(b) flouranthene NA 1.9 Benzo(g,h, i)perylene NA 1.0 0.97 see BaP see BaP Benzo(k) flouranthene NA 0 .91 0.78 see BaP see BaP Chrysene NA 1.8 1.7 see BaP see BaP Flouranthene NA 2 .9 3 .0 1, 080 295 Indeno(1,2,3- NA 1.0 0.76 see BaP see BaP cd)pyrene NE Phenanthrene NA 0.89 1.4 NE Pyrene NA 2.3 2 .4 890 272 BaP Equivalent NA 2 .15 1.99 2 10-.2 Other PAHs NA ND ND - 4,4' -DDE 0 .084 <0 .046 <0.047 40 NE 4,4' -DDT 0.22 <0 .046 <0.047 15 NE II a-chlordane 0.23 <0.046 0.24 13 NE Gamma-chlordane 0.23 <0.046 0.28 13 NE Heptachlor epoxide 0.061 <0.046 <0.047 0.4 NE II Other Pesticides ND ND ND - 2,4-D - <0 .167 <0.167 <0.167 285 NE 2,4, 5-TP (Silvex) <0 .0167 <0.0167 <0.0167 290 NE Notes : Units in mg/kg (parts per million) ' ND - Not detected above laboratory reporting limits NA - Not Analyzed < - Less than laboratory reporting limits ' SRV - soil reference value SLV - soil leaching value GRO - gasoline range organics DRO - diesel range organics PCBs - polychlorinated biphenyls NE - Not established < - less than laboratory reporting limits IIBaP - Benzo(a)pyrene II 1. 1 0 .-4 a a a a s -H rti ca m t rd N W• w 0 O N N p • O O W PQ cu W o 1 N 1 Ri N'd N N M 4 O H H N N N N N 0 ao N a N ' a ca H a a a a s H W PO L� N CI O N d' N to �0 to 0\ LQ 01 N t ° fn tll 6-3 Z d■ .4 N U 4) CO L(1 r1 r•I M N U a) N N N N r-{ ▪,� rl as a) a) N N N a) -H El r-i Ul Ul Ul Ul co 4) E N i N N N N N N N N N N °` ^ °� rC rC rC FC rC rC rC FC N N N 0 0 0 0 o p Z O Pq - V Z Z Z Z Z Z Z Z •0 0 0 0 0 0 0 0 4) i) v v V v v V V V V 0 I O N N. r r r r Z W ^ M H H H M N N N N N N N N nC H H H r p r-I r N 0 0 0 O O 0 0 0 0 0 i4 > 'a a0 Ga - v' o H M o v ° 0 0 0 0 0 0 0 0 a) Z v v v v v a) N O � W� EH H N N N N N NNNN -rl U1 al H z W H r i. 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O N V V V V V 0 00 N � S � �. N N N N 0 p CT1 Gi Q1 N al H i .-. 0 0 0 0 ri r, . ZZZ ZZZ • 0 0 � r� aa o 111 V v V O OV E N ri H N H •0 0 U) H m FC r.0 r,C rC FC 0 0 0 0 0 0 0 0 p u) i i i a) a) C l) V zzz • O p p p o 0 0 �� O � � a cji.,V V v PG �] Ri A A cA cn N m rd N r0 A N a) N ri N W (1J N 0 O ni O 0 0 0 cd u) N G �+ W ro oo0 0 � H04a10000P0 � . a0N a A � oow � Hw goo aw� wm v uw RS CV I I 1 I I I APPENDIX A PHASE I ESA REPORT OF MAY 28, 1999 I I I I I I I I i OPY i i PHASE I 11 ENVIRONMENTAL SITE R HOUSING p,DDITI PORT ON PROPOSED SENI NORTH 58TH STREET NORTH HEIGHTS,AN AKG MI�ESOTA ` OAK PARK 7735-B GME PROJECT NO. i i Prepared for: MR. GREG COLLATE SENIOR HOUSING PARTNERS 40 2345 RICE STREET, ST. PAUL, MINNESOTA 55113 i iMay 28 , 1999 i 1 I Inc. Copyright, 1999 - GME Consultants , 1 1 II 1 May 28, 1999 Mr. Greg Collatz II Senior Housing Partners 2345 Rice Street, Suite 240 St . Paul, Minnesota 55113 GME Project No. 7735-B RE : Phase I Environmental Site Assessment (ESA) Report for the Proposed Senior Housing Addition located at 58th North and Oakgreen Avenue North in Oak Park Heiights, Minnesota Dear Mr. Collatz : ll: We have prepared this report proceed on May 18, 1999 p t following your verbal authorization to proceed May 18, , followed by your written authorization of Y , 1999 confirming contract . We are submitting of this report to you. g three copies 1 We appreciate the opportunity you have questions regarding Y to work with you on this project . If g this report, please contact us . 1 Sincerely, GME CONSULTANTS, INC. 1 COpy 1 Kurt J. Steffen Environmental Geologist Project Manager II IITimothy F. McGlennen Senior Environmental Scientist Property Development Assistance Group Manager KJS II W•\7735-B Ph I ESA KJS IIIIIIIIIIIIIIIIIIIIIIIIIIIMIIIIIIIII I 1 il IITABLE OF CONTENTS PHASE I ENVIRONMENTAL, SITE P II ROPOSED SENIOR HOUSING DDITO REPORT A OAK PARK HEIGHTS, ADDITION GME PROJECT MINNESOTA II NO. 7735-B SECTION III . EXECUTIVE SUMMARY PAGE II. INTRODUCTION 1 A. Purpose B. Special Terms 1 C. Limitations and Conditions and User and Exceptions Responsibilities 1 D. Limiting Conditions and Scope of ofsessment 1 Services/Methodology Scope of 3 II 1. Standard gY Used 3 ASTM Elements IIa. Records Review b. Site Reconnaissance 3 c. Interviews 3 4 II d. Report Pre 2. Non-ASTM Scope Preparation 5 Pe Considerations 5 III. PROPERTY DESCRIPTION 5 II A. Location and Le B. Property Legal Description 5 Y and Vicinity Characteristics C. Descriptions of Structures, 5 II Improvements on the Roads, and Other 5 Ro 1 . and Interior prOPerty 6 2. Roads nterior Observations 6 II 3 . Heating Source 4 . Sewage Disposal 7 7 5 . Water Supply ID Specialized 7 by User and Owner of Property Reported 8 E. Current Ownershi 8 F. Past Uses of p and Uses of the Pro G. Current and the Property Property Past Uses 8 of Adjoining Properties 8 P 8 I IV. RECORDS REVIEW A. Standard Environmental Record Sources - Federal and State 9 II1 . National Priorities List 9 2. Leaking Underground Stora e T 3. No Further Remedial Action Tanks (LUST) 10 4 . VISTA Unma on Planned (NFp) 11 Pped Sites 11 B. Physical Setting Sources C. Historical Use Information 11 12 I g Pro 1. Property 2. Surrounding 13 Properties 13 I 14 1 II TABLE OF CONTENTS (Continued) PHASE I ENVIRONMENTAL SITE ASSESSMENT REPORT PROPOSED SENIOR HOUSING ADDITION OAK PARK HEIGHTS, MINNESOTA GME PROJECT NO. 7735-B ill SECTION PAGE II D. Additional Record Sources 15 E. Physical Setting Analysis for Possible Migrating 15 Hazardous Substances IIV. PROPERTY RECONNAISSANCE AND INTERVIEWS 16 A. Hazardous Substances in Connection with 16 II Identified Uses B. Hazardous Substance Containers and 17 Unidentified Substance Containers II C. Storage Tanks and Pipelines 17 D. Indications of PCBs 18 E. Indications of Solid Waste Disposal or Fill Soils 18 F. Other Environmental Conditions of Concern 19 1 1 . Additional Exterior Observations 19 VI . FINDINGS AND CONCLUSIONS 19 11 A. Recognized Environmental Conditions 19 1 . Property 19 2 . Off-Site 21 I B. Other Possible Environmental Issues Identified 21 C. Non-ASTM Scope Considerations 22 IVIII . STANDARD OF CARE 22 IX. SIGNATURES OF ENVIRONMENTAL PROFESSIONALS 23 I II Figures Figure 1: Regional Location Map Figure 2 : Property Diagram 11 Figure 3 : VISTA Radius Map of Government Sites Appendices 11 Appendix A: Qualifications of Environmental Professionals - Resumes Appendix B: Regulatory Documentation - VISTA Report II Appendix C: ASTM Owner Questionnaire Appendix D: Property Reconnaissance Photographs II II I I . EXECUTIVE SUMMARY t on the located at 58tH Avenue North and performed a Phase I Environmental Site Assessment (ESA)p Addition 1 Proposed Senior Housing Heights, Minnesota. This ESA was Oakgrsed Avenue North in Oak Park ocate and limitations North ASTM completed Avenue accordance with the and it has revealed on-site and Practice E 1527-97 and our contract, RECs) • off-site recognized environmental conditions presence of an underground tank or dry e tank used to store fuel oil, the use of The on-site ab Reground storage g the p coal well, an aboveg the former presence of a a garage for vehicle maintenance, greenhouse, and the surficial fired heating system for the former g dumping of solid waste on the Property. e RECs include the presence of a automobile salvage yard The off-sit to the north and the presence of the on the adjacent property identified to be Baytown Township Groundwater Contamination Plume, approximately 1� mile south of the Property. (Section RECs are discussed in the 'Findings and Conclusions" These Other possible environmental conditions of concern of this report. To ncern or issues are discussed in Sections tirety,d as this is report should be read in The whole rep resented in other sections . dependent upon information p II . INTRODUCTION I A_ Purpose llatz of Senior Housing Partners (i . e . , the "User" of Mr . Greg Co proceed on May 18, 1999, and this report) verbally authorized us to p 18, 1999 . This Phase I ESA signed our confirming contract dated May acre parcel (i .e . , the was conducted on the approximately "Property" ) located at 58th Avenue North and Oakgreen Avenue North in recognized Park niz Heights, Minnesota. The purpose of this ESA is to identify recog nized environmental conditions associated with the Property. 1 al Terms and Conditions and User Res•onsibilities B. S.eci and " We This ESA was performed in general accordance with the scope ' ns of ASTM E 1527-97 "Standard Pr the purpose Environmental Site limitations by ASTM 0 Site Assessments : Phase I ESA Process • conditions" (RECs) hazardous the term "recognized environmental presence of any definition means "the presence or likely p substances or petroleum products on a property under conditions that indicate an existing release, a past release, or a material threat of ' II Senior Housing Partners 2 May 28, 1 999 GME Project No. 7735-B ' etroleum products into a release of hazardous substances or p groundwater, or surface structures on the Property or into the ground, q water of the Property. " The term includes hazardous substances Tor petroleum products even under conditions in compliance with laws .generally t term is not intended to include de 1 condior tions the envi ronment and do not present a risk of harm to p ublic that generally would not be t government agencies . subject of an enforcement action 1 brought to the attention of appropriate uarantee or warranty that This Phase I ESA is not to be considered a q environmental conditions there never has been or never will be aintended to identify RECs at II associated with the Property. It is only one point in time on the basis of a specific, limited scope of services . II ainty regarding the potential RECs No ESA can wholly eliminate unc Pe formance of this standard practice in connection with a property. uncertainty regarding the is intended to reduce, but not eliminate, potential for RECs in connection with a property. report to meet ASTM E 1527-97, the User of this In order for this rep responsibilities : report is required to have satisfied the following p II 1 , The User is required to check title records for if any, that are currently environmental liens, and report them to recorded against the Property us . 2 . The User is required to communicate e toth s any specialized knowledge or exp material to recognized environmental conditions in connection with the Property. II 3 , The User is required to communicate purchase e to us the actual knowledge that the p rchae Property is significantly less tln such case u , the II price of comparable properties . User is required to identify an explanation for II the lower price and to make a written record of such explanation. II d that the User obtain and review a copy of E 1527-97 to We recommend responsibilities and scope ensure their knowledge of other User resp 11 I May 28. 1999 3 Housing Partners Senior No 7735-g and GME Project report the User review attorney• end that this environmental II Also, we recommend with their limitations .ential environmental their p tions of Assessment The li This Exce our Client. C. Limitations and been prepared for any other party, li has art, to confidential and in whole or in p written permission report is the prior may be report may not be circulated, without the report other party. however, that or Federal li be used by any GME agrees, State nor Client. to interested Completion, of GME and our attorneys with financing, only. to Client' s associated purposes conveyed other parties informational P to no other II or to to be read for our Client and the agencies, Property, only to unless GME and or sale of the obligations extend report, and Client rely on this GME' s duties Client may party only our otherwise. in our provide written consent opinions presented Client p and p of report delivery• that the information the date within understood only as not be considered li It is applicable date will report will be after that Events or occurrences Individual li the scope of our report . as a whole . interpreted remainder of this interp upon be read and upon the dependent up report must are dependent also are project li This this report of this report in the p portions of of the sections stipulations contained II report . All stip accepted by GME. II conditions, and accep the terms,and any written amendments Contract, Used D. I,imitin• Conditions and 5co•e of Services/Methodolo � ems in our 1 . Standard ents AS`rM I ESA is outlined components this Phase standard comp services for the four with a II The scope 99 our proposal and includes outlined below along 18 , 1 prOp1527-97 • These are May E that we used• li given in AST STM: description of the methodology Review Conjunction with a Records RECs in assess I to help identify migration, and records Our review various possible contaminant area. We reviewed assess p and surrounding II the Property, the property previous uses of included the following services: 1 Senior Housing Partners 1i 4 May 28, 1999 IIGME Project No. 7735-B a government records and reviewed Solutions for We requested Information from VISTA or threatened information a release or indicating pollutants,releasetion substances, p The records release of hazardous the property• at or near environmental contaminants Federal and State the size li search included E 1527-97 • Due to required by were extended II databases Property the search distances of the Prop by 1/8 mile . h sisal reasonably ascertainable Ety--ea We reviewed pertaining sources for information p in assessed setting drogeologic conditions .the potential II geology and hY it relates to These the information as onto the Property. 7 . 5 Minute II migration of contaminants U S G S , Survey included the Geological sources and the Minnesota County. Quadrangle Map Washington Q is Atlas for (M.G.S) Geologic review, records a historical zing to review We performed or attempting reviewing standard or additional including includes reasonably ascertainable information ludes This maps property historical sources . the ra hs, fire insurance records, aerial photog p land title local files, recorded uadrangle Map, tax 7 .5 Minute Q records, current USec building department a, street directories, building and interviews, II land use Use Information" zoning/ the "Historical described in ort . IIsection of this rep li Reconnaissance b• Site identify Property to observed the of past uses, current visually uses and evidence of II Property the current prop characteristics 19, surface On May and r identify presence of RECs . Property for the p GME Environmental Mr. Kurt Steffen, 1998, property reconnaissance . II Geologist, conducted a reconnaissance .Geolog and Mr. Timothy F. an Kurt J. Steffen Scientist, performed Mr. ental on May 27, GME Senior Environmental II property reconnaissance econna ssanceed of walking additional the Property 1999 . This reconnaissance along to the Property, vehicle tracks II boundaries, and on roads or the notable features . We observed boundaries, observe for 11 ' Senior Housing Partners 5 May 28, 1999 GME project No. 7735-B structures to identify portion of on-site (from the interior p visually observed ( for We also Dining properties Property RECs .undaries) the adz of past and Property for indications evidence of RECs and current land use. i c, Interviews a representative of contacted and interviewed for information the Mr . Tim Ritter, uses, and the owner, and past land regarding current Ritter on May RECs . We interviewed Mr . it 1999 May potential telephone and on 24, 1999 by questionnaire. others for local officials and uses of the t ➢ information interviewed current and p potential the information regarding area, and P Property and the surrounding interview dates) RECs . These individuals (and were: Bayport Fire Carmichael - City of Fire* Mr. Brad Park Heights (May Chief, which serves Oak 1999) d Re ort Pre aration the general format We prepared this report lnheadings suggested by 1527-97 • The that we outlined in E this report except used in titles and their ASTM were of the to, in our slightly modified some added some subheadings summarize the order and describe and opinion, better information. 2 . Non- ASTM Sco e Considerations by the No additional "Non-ASTM" scope considerations were requested user . DESCRIPTION III . PROPER'T'Y p, l Descri tion Le a Location and North in Oak Park west of Oakgreen Avenue was provided by is located The Property The following legal description Heights, Minnesota. Senior Housing Partners 6 May 28, 1999 GME Project No. 7735-B of the Northeast Southeast Quarter except the the Range 20 West, one-half of South you: 'The North 29 North, North 218' of the of of East Township t the State of quarter 200' , and except County, 100' of the East Washington Diagram is North East 200' thereof, A Regional Location 400' of the Property and surrounding to public roads ." the Minnesota, subject diagram of presented as Figure 1 . A properties is presented as Figure 2 . rt and Vicinit Characteristics Pro•e that B. agricultural area a historically commercial development . Property is ing residential s located in and comet The Prop undergo recently had been Property uses single family on the adjacent p roperties include ard. homes, vacant land, and a salvage y retail Highway 36 and associated land use includes Property. The surrounding uses approximately 2000 feet north of the Prop C. Descri•tions of Structures, Roads, and Other Im•rovements on the Pro ert - 1 . Structures and Interior Observations wood framed garage 100 foot by 15 foot, Sliding and approximately of the Property. four We u ture an app portion the building accessed We structure on the eastern P side of structure . on the eastern north end of the hand overhead doors on the We observed ' located space .areas, the southern sp this space. We enclosed shop in in a maintenance bobcat loader used oil . Much observed inoperative that contained observed tools and an a 55-gallon drum and we observed was oil stained and automotive additionally in this space products of the concrete floor antities of petroleum p small quantities of the concrete floor were cracked. storage of space . Portions fluids in this p metal gasoline apes, wood, glass panes, used oil the storage of plastic piping, We observed spaces . Two p sp empty plastic containers, in the other enclosed end of containers, located on the filters and other automotive supplies the storage of maintenance bays s we observed the non-enclosed bays, equipment, and small the structure . r the maintenance landscaping of the garage• truck, gas powered spaces an old pickup in the enclosed p eared to e. to those found floor that app Ttems entire had a concrete be ' The entire garage structure I 11 Senior Housing Partners 1111 GME Project No. 7735-B May 28, 1999 damaged in a few loc11 ations . The surface in front of the garage was gravel covered. and 10 foot tall concrete approximately 150 foot long We observed a observed an app ortion of the Property• of enclosed an area wall on the southeast P wall which this attached to this to I,o , Ritzer, ' foundation 30 feet . According present on the approximately 150 feet by greenhouse formerly p foundation is a remnant of a g 1 Property. 2 . Roads east vehicle yards on the south, s and Property. Access east We observed gravel driveways structure on the to garage that was located north this west a area sides of was provided by a driveway 58th Avenue being graded for 58" ' this area formerly west toward the of the residence, in the area currently running We observed a less used vehicle yard. North. Property from the central portion of the Prop Avenue North across the of 58th gravel hauled central observed the subgrade preparation we observed sand and portion of the Property. to p to raise the roadbed. to the Property ' � uPatin�urCe west side of the garage . This 265 gallon AST on the the tank had g strong AST observed a but the inside of strong AST appeared to be empty, We observed four We did not observe obvious i1 staining fuel oil odor. i ing for and flue side of the garage, brick tank i bysowonhethetewesteprn two flue boink ions in the enclosed spaces . We observed connections in three of The floor in these spaces was oil furnaces in the northern space . stained with some type of petroleum product . III, We end of the north of the western part of a brick chimney that this chimney was p We observed greenhouse .was r of greenhouse wall . Mr . Ritter indicated former g system for the in the basement Ritzer a the hat water heatcoal stoker was located indicated that a of the chimney and that coal was stored in just west oil was not to heat office located stoker. He reported that heating a bin near the the greenhouse . 4 Sewage sal sewage system. an on-site seage disposal y evidence of floor drain was located in the We observed no that a However, Mr . Ritzer indicated May 28, 1999 Senior Housing Partners 8 GME Project No. 7735-B Mr . Ritzer stated that this greenhouse office . space and that it basement of the g prevent flooding of this sP owned collected was used water rp during the time that the Ritzer family toelected nly the garage Mr .. Ritzer stated that this drain south was o f connected to a the Property.r well located just arag . tank or possible dry for this tank or dry ' structure . We observed an access pipe well . Liquid was present in this tank or dry 5 Water Supply We observed no evidence of water supply wells on the Property. Mr . greenhouse was located Property. A review of near indicated that and dtiswnot located on the Prop presence of the the database residence the the CWI database did not reveal records indicating 1111 wells on the Property. 5secialized Knowledse of Pro•ert Resorted b User and Owner D . The ecialized " representatives of the 'User" reported no sP with regard to the User responsibilities knowledge ow edge or rep ledge of the Property, identified in E 1527-97 ; the User and Owner knew of no environmental liens on the Property. E . Current Ownershis and Uses of the Pro.ert and subgrade is owned by Mrs . Helen Ritzer . Ig rad g an artificial The Property A on the central portion of the Property. preparation for 58th Ave North and the development resent on the wetland is occurring greenhouse are p Property is garage and foundation for erty°andrthe remainder of the eastern portion of the Prop fallow or is grass and tree covered. g Past Uses of the Pro ert agriculture To the extent identified, the Property has been used for and as a landscaping a greenhouse and row crops, included vehicle including operations . These uses contractor' s base of maintenance . G. Current and Past Uses of Ad' oinins Pro.erties t to the Current and past use activities adjoining the Property, extent identified, are summarized below. 1 May 28, 1999 II Senior Housing Partners 9 GME Project No. 7735-B II II --___—__-__-------------- r - : ENT it§E :_ � �����N III I': residences, vacant land Agricultural and residential 1 Single family g North and a automobile salva:e and homes Agricultural and residential II South Subdivision of single family Agricultural and residential (! ' I Single family homes -- �i Agricultural and residential Vacant land �'�-'—___-_-- - made during our our limited observations of these sites, arts, including During we observed automobile p Property reconnaissance, adjacent fuel tanks, gearcases and transmisspo��sst stored outside, radiators, fu Stillwater Auto on the ground surface at debris was about ten feet property to the north. The closest salvage from the Property boundary. in the surrounding area included retail outlets such Other uses mall along Highway 36, approximately new Wal-Mart o and a shopping ro rty. The surrounding area to the south 2000 feet north of the Pedpor is undeveloped. is agriculturally develop 11 IV. RECORDS REVIEW pertained to the Property L potential Rert, Certain record properties sources reviewed past and uses�t from possible and nearby properties impacts to the Property and the likelihood of potential imp roducts . migrating hazardous substances or petroleum p II A. Standard Environmental Record Sources - Federal and State obtained II a VISTA file evaluation of Federal redleas State databases for We r tio known or threatened Property. Each information indicating determine if the substances, pollutants, or contaminants revoeweda to the or other sites within the I Property, database oini g listed properties, (shown e Ppppopty, the adjoining The Property boundary appropriate ASTM minimum search distances from the Property in parentheses) , were identified in the database. Property. I was extended by 1/8 mile due to the size of the Prop II NPL: Federal National Priority List (1 1/8 mile) II 1 Senior Housing Partners 10 May 28, 1999 1111 11 GME Project No. 7735-B CORRACTS: Federal RCRA Corrective Actions and Associated TSDs ' 11 (1 1/8 mile) SPL: SCL: State Equivalent Priority List (1 1/8 mile) State Equivalent CERCLIS List (5/8 mile) CERCLIS: Federal Sites Currently or Formerly Under Review by the US EPA (5/8 mile) Federal RCRA Permitted Treatment, Storage, Disposal TSD: - non-CORRACTS sites (5/8 mile) Facilities State Leaking Underground Storage Tanks (5/8 mile) LUST: State Permitted Solid Waste Landfills, Incinerators, SWLF: 5 or Transfer Station (5/8 mile) / AST: State Registered Aboveground Storage Tanks (Property and adjoining properties) State Registered Underground Storage Tanks (Property UST: and adjoining properties) Federal Emergency Response once Notification System of ERNS; Spills (Property and adjoining properties) Federal RCRA Registered Large Generators of Hazardous Wastes (Property and adjoining properties) Federal RCRA Registered Small Generators of Hazardous Wastes (Prop SM GN:SPILLS: (Property and adjoining properties) State Spills List (Property) There were four mapped sites identified within deisearch distances for these The VIISTAsreportsis attached eas Appendix A ' sections . 1 . National Priorities List (NPL) PL site within one mile of the Property (the ASTM VISTA deno ted one N the Baytown Township Groundwater P This site is of the plume is search Pluume me (VVISTA A Map ID No . 1) . The northern edge I May 28, 1999 Senior Housing Partners 11 IIGME Project No. 7735-B Property. The ' approximately 1/2 mile south of the Airport, groundwater to be aPP ortedly originates from the Lak mo eAirport, II ro plume rep Property. This plume located 2 1/2 miles southwest of the Prof The extends to the east . Contaminants such as tricilor etstue and carbon the Minnesota Department of Health as a tetrachloride have been detected in 34 wells area is designated by special well construction zone . II2 . Lekkin• Under•round Stora•e Tanks (LUSTS) II erty (The ASTM VISTA denoted two LUST sites wwaslnr reported of at Thumb Store the the Prop northeast theast re search distance) . A release 2000 feet nor 2) located approximately (VISTA Map ID NO ' orted in October of 1993 and the the Property. This release was rep this site was "closed" in December of 1993 . II inv esti investigation at �� However, it is our in petroleum impacts can exist at ` closed sites . ' on that this is a de minimis condition notsbe the is our opinion because it 'generally would s t definition of a REC, government enforcement action if brought to the attention of appropriate government agencies ." of II A (VISTA Map ID No . 2) in May 1998,release was reported at Yocum Oil ( This site if 1998, and investigation at this site remainert'open" . approximately 2000 feet northeast of the Prop PP II 2 , No Further Remedial Action Planned (NFRAP) FRAP site located approximately 2000 feet VISTA denoted one N VISTA Map ID No . 2) . The UFE Industrial Property ( assessment and was placed northeast of the Prof preliminary Incorporated site list . A underwent review a P of the MPCA website indicated that 200 gallons of methyl ethyl between the 1974 list . A approximately ethyl between waste and solvent was dumped at this site . However, ketone waste solvent and no evidence of their presence was evaporate quickly groundwater of these discovered evin 1984 investigation of the soil and g II discovered in a the site, and no further work was rep ortedly required to investigate or remediate the site . 11 3, Vista Unma ed Sites 20 "unmapped sites" that are listed dPtobase sites that VISTA listed code or city of the registered are located in the same zip These sites included registe of insufficient address data SWLF map .nd AST sites . Our cur sort' review IISCL, CERCLIS/NFRAP, II 1 May 28, 1999 Senior Housing Partners 12 GME Project No. 7735-B ed sites" revealed no obvious sites within the the VISTA .,unm a pp appropriate ASTM search distance . f services did not include a survey of the business names as these would not be practically within scope o possible that within these search distances, ESA. Therefore, it is reviewable for a typical Phase I Property; additional work would an "unmapped site" is located near the Prop be required to confirm this possibility. g, Ph sisal Settin Sources erty The estimated physical conditions in the vicinity of the Prop are summarized below. _OtTItCE 4F EqI TA ` HT - — The gently rolling surface of the Property Site observations and USGS 7.5 Minute has TOPOGRAPHY Quadrangle Map I. elevations ranging from 910 feet to 940 feet .I NGVD. M.G.S. Geologic Atlas for Washington II SURFICIAL GEOLOGY Sandy outwash and sandy loam g lacial till M.G.S,. Geologic Atlas for Washington II DEPTH TO GROUNDWATER Estimated to be 30 feet to 60 feet. Count ,MN,and CWI database to the east, toward the M.G.S. Geologic Atlas for Washington DIRECTION OF REGIONAL Estimate d to be County,MN SHALLOW GROUNDWATER Mississippi River Washington 'I FLOW M.G.S. Geologic Atlas for Estimated to be 50 to 150 feet Count ,MN DEPTH TO BEDROCK G.S. Geologic Atlas for Washington g Sandstone of the St. Peter and Jordan M.G.S. ,MN BEDROCK GEOLOGY Formations. Site observation, wetland delineation flags 1i from a previous survey performed by another 'I SURFICIAL WATER Wetland areas were present on the north central consultant were observed performed the Property__/WETLAND portion of the Property I I II Partners 13 May 28, 1999 Senior Housing GME Project No. 7735-B II C. Historical Use Information IIThe following information sources were used to compile past and present land use activities on and near the Property; these uses are IIdescribed in the sections following this table . SCO Cg SO^aCg ,OI✓A U Y PHOTOGRAPHS - AERIAL HO 1928, 1953, 1957, 1963, 1980,1987, University Map Library Minnesota Photographs are not available previous to development of the site. 1990 Wilson Map Scales: 1 inch=800 feet to 7500 feet Fire insurance maps were not known to exist for this previously undeveloped FIRE INSURANCE MAPS City of Oak Park Heights rural area. Property tax files only record assessed II City of Oak Park Heights value and were not useful for historical I, PROPERTY TAX FIL ES data. Only current records are readily III RECORDED LAND TITLE City of Oak Park Heights available. II RECORDS USGS TOPOGRAPHIC MAP In-house library Base map and revisions. Stillwater Quadran_le, 1967 City Directories do not exist for this LOCAL STREET DIRECTORIES City of Oak Park Heights undevelo eed, ereviousl rural site. The only records available for the BUILDING DEPARTMENT City of Oak Park Heights Property related to the current RECORDS develo•ment. INTERVIEWS , This"other historical source" was used Mr.Ritzer,Mr. Carmichael to sue element the standard sources. --_---_____________________ 1 1 . Property II resence of the greenhouse and The 1938 aerial photograph showed the P A small vehicle yard was the garage building on the PropertY'arage structure . The central apparent on the eastern side of the a eared to be cultivated in II and western portion of the Property PP P small fields separated by tree stands . Building department records it was only recently because were not available for the Property does not annexed into the City of Oak Park Heights . Baytown Township 1 maintain historical inspection records . The 1953 and 1957 aerial photographs showed a similar arrangement of structures and agricultural fields on the Property. purchased the Property. Mr . Ritzer In 1958 the Ritzer family P used the greenhouse to indicated the previous owners of the Property 11 II Senior Housing Partners GME Project No. 7735-B 14 May 28, 1999 family continued to use the vegetables . The Ritzer Mr. Ritzer stated that grow winter houseplants . Property but dad greenhouse to grow flowers and remainder of the for their did not cultivate the and storage area his family Property as a shop use parts of the Prof landscaping equipment . Mr . Ritzer indicated that the greenhouse was partially demolished and the house, two-car garage and associated parcel were sold inrty Ritzer continued to use the Proper II late 1960s and early 1970s . Mr . for his landscaping business . property II the garage on the showed that unimproved road that The accessed aerial photograph North by an unimp for from Oakgreen Avenue the subgrade preparation was locateed to the garage without was located in the current location provided access 1g70s . This road p sold in the late to be 58th Avenue North. appeared the portion of the Ritter property he Property crossing western portion The central and resent . fallow and some small trees were p hs showed similar features to The 1987, 1990, 1991 aerial photographs the 1980 aerial photograph. the Property prior to II not identify according to prior AS TM Because the reviewed sources do ata failure" either this represents sources were development, the standard historical and either standard, because due to their non-usefulness whatever II or eliminated E 1527-97 allows reviewed 7 . 3 .2 . 3 be deemed resulted. Section of ��whatever . . . shall history uses is derived Ii history of previous tactics ." sufficient, • , .to comply with this p 2 . Surroundin Pro erties at II graph showed the presence of a residence and The 1938 aerial p hotoin s at the current locat location to the Stillwater of the Auto three lvagelyard, on the adjacent Property photograph and this Auto Pious salvage Y was evident on the p garage and residence and farm. The No obvious edrficiae dumping part of the appeared to be used as a which were p rite app Property to east, on the the adjacent PrO e and greenhouse structures 1 residence on the garage two outbuildings were same homestead as residence and ding Avenue Property, were present . A across Oakg to be Prop adjacent Property to the east, sites appeared II located on the adj of the surrounding City of Stillwater North. The remainder areas for the arty• agricultural in use . Residential were present approximately one mile northeast of the Prop I II II Senior Housing Partners GME Project No. 7735-B 15 May 28, 1999 II The features to the 1938 photograph showed similar features to the aerial 1953 aerial p ngle Avenue photograph. The 1957 aerial photograph Oakgreen p to the north along on the homes on the adjacent properties constructed on the farm North. A larger barn had been adjacent property to the north. II sold the parcel, home, and two- In the late 1960s the Ritzeracent family Property to the east . car garage located on the adjacent h showed the presence of an automobile photograph to the northwest. Additional II The 1980 aerial p acent property salvage yard on the adjacent t along Oakgreen Avenue to the North. single family homes were present was present on the adjacent le family A residence and two A subdivision of sing across Oakgreen Avenue . to the south. Property to the east, adjacent property li outbuildings were located on the adjacent 2000 feet north of the Highway 36 was present app Property. completed II photograph showed that the roads psty adtoeenhcomplete The 1987 aerial p the adjacent p Highway 36 . for the subdivision on was present along Hig Additional commercial activity photographs showed similar conditions to The 1990 and 199 IIII p the 1987 aerial p D , Additional Records Sources d source used was that of "non-standard" record as described The only additional, reported by the interviewees, the personal knowledge rep above . liE . Ph sisal Setting. Anal sis for Possible Mi•ratin• Hazardous Substances parts gearcases, and transmission p We observed fuel tanks, radiators, the adjacent located on the ground surface at SeorAotherasutomotive fluids to the north. Petroleum products salvag e activities .automotive site property vehicles during than the can o released from slightly higher elevation similar to slig groundwater flow is located at a regional geologic atlas indicates g osition. In II Property and y, le� in a sidegradient p placing the Property petroleum or other to be easterly, p groundwater of the our opiII nion, a significant surface release 5eand g automotive fltodthe could proximityCt the Property, due I 1 May 28, 1999 11 Senior Housing Partners GME Project No. 7735-B 16 I of a an open investigation Were of a LUST site, of solvents investigation ation of a release of the A closed and a closed investigation 2000 feet northeast and reported Sete, roximately the Property pet at sites located approximately flow to be elevation to sites are at a similar groundwater Property. These indicates g frem the Property• Tonal geologic atlas and away suggest the regional the Mississippi River, from the Property toward and distances Property, in out easterly, , affect the The do these s nt positions unlikely to that these sites are detected as opinion. has been the chlorinated solvents originated at A groundwater plume of Property This plume orig the approximately 2-1, miles southwest migrating to � mile south of the Prop Lake Elmo Airport located app lame is Lake Elmo Airp groundwater flow to that the p The investigation indicates indicates g to the II Property• regional geologic atlas radiegr position the east . The placing h Property in a sideg the groundwater of the placing prop affect the east, this plume could if the groundwater flow plume . However, date, in our opinion, chlorinated solvent Property at a future or if the ion becomes more northerly in the reg local geology• migration was affected by INTERVIEWS V PROPERTY RECONNAISSANCE AND interviews Ireconnaissance and the Information obtained from our provided in this section. regarding potential on-site RECs is p ii A. Connection with Identified Uses in, Hazardous Substances property, Mr . maintenance on the of vehicle performs vehicle evidence company often p that R observed that his landscaping Ritzer also stated the Ritter indicated near the garage . Mr ' near inside or performed vehicle maintenance of stained III maintenance owner also p of the presence of the previous was unaware Hoesenc , the stained e building • Mr . Ritter Property. that garage vegetation on the indicates Property for vehicle maintenance Property and may soils or distressed P g present on the portions of the were p troleum or automotive fluids efore, could affect the soil and shallow I petroleum and therefore,have been released, groundwater of the Property. used for Property was formerly family indicate that the 1958 his stated that since Aerial photographs Mr . Ritzer other then associated crop agriculture . for agriculture, portion of the row the Property the eastern I has not used Before 1958, with the greenhouse . I ' Senior Housing Partners II GME Project No. 7735-B 17 May 28, 1999 II the greenhouse was used to s and was wa used to II was cultivated in row crops the greenhouse Property After 1958 the greenhouse was raise winter vegetables . plants until flowers and household P the that his family produce Mr . indicated that late 1970' s . Ritze the Property and demolished in the on products . agricultural chemicals but no other p did not use ag greenhouse, owner used whether the previous li previous owner usedo�aninaicate the cultivation. Mr . uiturr did to the row crop agricultural chemicals in relation have used agricultural Property may fertilizers can The cormer owner of the pesticides and applied of herbicides, P levels if aPP chemicals . The use above background Department of II impact the soil and groundwater the Minnesota rates, according to and no extraordinary II above labeled areas, ro reties . We did not observe mixing or adjacent properties . re eases a. reported on the Prop releases have been rep B. Containers and Unidentified Substance Hazardous Substance Containers five empty, gallon metal containers stored two, five g amber glass etal gasoline cans and the We observed gallon, clear and were present on approximately one g Although labels 1 gallon, inside the garage structure . illegible . We observed two they were illeg of the garage structure . glass containers, non-enclosed portions metal cans in the unknown substance . These cans contained paint and an used oil in the northern space that 55-gallon drum of Ritter stated that an oil II We observed a Mr .is used for vehicle maintenance . Ma regular basis . IIservice company empties this drum on Tanks and Pi elines of the II C. Stora a western side 26S-gallon fuel oil AST on the We observed a 265-g or evidence of release soil staining however the tank or its exterior piping, garage . We observed no obvious associated with this was petroleum stained. concrete floor near the furnaces located just south of II tank or dry well is drain to south f Ritter stated that a that a Mr . Mr . Ritter indicated to this the former basement te . greenhouse office was connected keep the in drain was used the former basement of the gthat this that hazardous substances tank. Mr . Ritter indicated for basement dry. Mr . Ritter had no knowledge li had been disposed of in the drain. We did observe an access pipe II 1 Senior Housing Partners 18 May 28, 1999 GME Project No. 7735-B this tank or dry well and it appears that liquid was present at the time of our reconnaissance . D . Indications of PCBs air compressor located motors on an Property. It L older electrical dumped on the Prop We observed in other appliances contain PCBs and within the garage and appliances equipment that these older electrical aPphe electrical is possible no placards or labels on no obvious of PCBs . We observed we observed they were free indicating that spillage of fluid from the equipment . evidence of leakage or sP E . Indications of Solid Waste Dis.osal or Fill Soils resent on the waste was P of five cubic yard pile site .observed. We numerous In approximately where western end of the We observed an of the wes site . located just north automobile tires, former greenhouse structure . lumber, concrete, debris such as timbers, of side of the vehicle path located southwest and observed on construction and brick on the south the garage structure . various household as water heaters, within the items such tarpaper located We observed fencing, and observed a carseat, metal We also appliances, former greenhouse . foundation. for the greenhouse foundation just south of the g and couch in the woods j such as wood, household buried solid waste location of the wa observed partially of the current the brush shingles, justnOAvenue North and south of waste, and 58th grading preparation for pile . inside the garage waste near and tractors and siding, old the s ucture . small amounts tires,soli lumber, east of observed tires, and located structure . We the vehicle y of located waste inside garage ages trucs, and wire in parts . Oxide arc e structure . We observed small amounts windowpanes, g g and electrical p broken automobile e including windo. the items nge, repair w the garage and indo pale , air were stored in air compressor the lumblumber, did tools such an were located within lumber, and an older truck and tractor Additionally, garage . I II Senior Housing Partners GME Project No. 7735-B 19 May 28, 1999 II approximately 10 to 15 cubic piles of fill soils, We also observed We observed two p garage structure . ve . to the west of the g garage structure . yards in size, and brush pile west of the q a 20 to 30 cubic yard stated that none of II landscaping stated that the soil and brush were derived from residential landscaping p rojects . Mr . Ritter additionally II the soils were known to be contaminated. to a burner barrel near 500-gallon tank converted feces b the ash We also observed aWeO observed observed and metal p the brush pile . contained in this burner barrel . IF. Other Environmental Conditions of Concern II 1 , Additional Exterior Observations servations that we made no other exterior ob Other than stated above, erty. indicate potential RECs on the Prop 1l11l1I VI . FINDINGS AND CONCLUSIONS A, Reco nized nmental Conditions eneral accordance erty in g We have p imitations of ASTM Practice E 1527-9�7 and our rop erformed a Phase I ESA for the ractice are scope and l from, this p I woth the or deletions ort, as well as any doncrabt. Any exceptions to,ro riate sections of this rePn our opinion. The potertbal R the app p during our de minimis conditio encountered potential REC that was a the data failure to pre- II development of the Property. evidence of ASTM defined on-site or This assessment has revealed no e the Property, except for those off-site RECs in connection with described below. I 1 Property tank or dry well south of the The presence of a REC, in our opinion. Mr . II garage represents a Ritzer indicated that this tank was connected o a drain located in the basement of the greenhouse offof ice . Mr. Ritzer stated that he was the aware a n or hazardous materials disposed of II I Senior Housing Partners 20 May 28, 1999 GME Project No. 7735-B the tank and drain were present dry well . However, previous to 1958, when his family p urchased the the Property, and Mr. Ritter was unaware practices of the former owner. The presence of a 265-gallon fuel oil AST without T p Property represents a secondary containment on the Prop we observed no REC, in our opinion. Although evidence of obvious soil staining near the AST or outdoor piping, we did observe petroleum stained concrete in the garage near the fuel oil furnaces. A significant release of fuel oil u from this system the could affect the soil Property. presence of a vehicle maintenance t ➢ The continued p represents a garage structure since befoRetzer8indicated that REC, in our opinion. Mr. continually occurred on vehicle maintenance has cWe observed a 55-gallon the Property in the past. Ritter inside the garage . Mr . used oil drum is regularly emptied by indicated that this drum ny We observed fuel an oil service garage containers and automobile parts within the vehicle of the garage for structure . The use maintenance indicates that p o possibly hazardous fluids were ha products spill re petroleum P ts or automotive Property. A possible sP handled on the Prop have affected the or release dofuoflthe Property. soil an groundwater he presence of solid waste represents a REC, in T P the our opinion. We observed numerous wheretsolidowaste 11 our portion of the Property household waste, such as tires, appliances, and construction debris were automobile parts, erty. We also observed on t he where solid hwa was appeared to be observed one area erty• partially buried on the Prop presence of a coal fired heating system The former p greenhouse represents a associated with the former g eenho e that some ash in our opinion. It is p buried on the REC, could remain or unburned coal be unearthed during earthwork. Property and may Coal and coal ash can contain elevated levels of I May 28, 1999 Senior Housing Partners 1111 11 21 GME Project No. 7735-B II II heavy metals and semi-volatiles . 2 . Off-Site ➢ The presence of the Baytown Township Groundwater Plume, approximately ,. mile south of the Property, represents a REC, in our opinion. solvents apparently released at the Lake ke Elmo to airport have migrated approximately h the Property appears to be in a the east. Althoug lumen groundwater side-gradient position to this P groundwater conditions and flow directions transverse to time, and solve groundwater flow due to their relatively high specific gravity. �, and on the adjacent The presence of a salvage represents a REC, in our property to the north rep opinion. We observed the presence of radiators, fuel tanks, and other automobile parts on the ground surface . A significant surface release or llI11ll1l1 spill of petroleum, or other automobile fluids P groundwater of the could affect the soil and g Property. B. Other Possible Environmental Issues Identified The temporary storage of fill soils on the Property represents a possible environmental P opinion. Mr . Ritter stated that he issue, in our oP on the stored fill soils from residential needed projects for other Property temporarily until We are relying upon Mr. Ritzer' s projects . not aware of any statement that he was present or contamination in the fill soils p formerly present on the Property The former use of agricultural chemicals represents Property and adjacent properties rep possible environmental issue, in our opinion. to the Minnesota Department of According gr cult pesticides, herbicides, Agriculture, the use of P groundwater. and fertilizers can impact soil Would have been However, these chemicals likely II II II IIwidely used in this region, and no extraordinary II Senior Housing Partners 22 May 28, 1999 GME Project No. 7735-B 11 releases have been reported. - STM Sco a Considerations C Non A the user No ��Non -ASTM Scope Considerations" were requested by VII . STANDARD OF CARE with the scope and in general accordance We assume no limitations report has been prepared E 1527-97 and our contrac limitations of ASTM Practice inadvertently omitted addresses in the or the database rata provided for incorrect State and local officials,responsibility database rovpor to us by we can assume no for data p or other incorrect report. Additionally, through personal interviews incorrect information obtained sources . with generally conducted in accordance level of care Phase I ESA has been with the standard This consistent professionals currently of care accepted practices similar other environmental p and under exercised by the same locality No warranty or ordinarily in performing ond conditions of time projects of information. of time and accessibility this report with respect conditions implied, is intended in guarantee, express or imp Property. to the environmental conditions on the Prop I t I I I 1 11 i Senior Housing Partners 23 May 28, 1999 GME Project No. 7735-B ' PROFESSIONAL'S VIII . SIGNATURES OF ENVIRONMENTAL' I A Kurt J. Steff Prepared by: b logist Environments O Project Ma Timothy F. McGlennen Reviewed by: Group Manager Senior Environmental Property Develop Mark D. Millsop Reviewed by: Principal HydrogeOlogist Environmental Division Manager L KJS W.\594_B Ph I ESA KJS 1 I I 1 . 1 FIGURES FIGURE 1: REGIONAL LOCATION MAP FIGURE 2: PROPERTY DIAGRAM GOVERNMENT SITES FIGURE 3: VISTA RADIUS MAP OF i I 1 Iv •11 STILLWATER, MINN.—WIS. i 1 '1 •_ + -�. 103 STILLWATER QUADRANGLE �= t. N4500—w9245i�•5 MINNESOTA—WISCONSIN _ f 7.5 MINUTE SERIES (TOPOGRAPHIC) ,F.� '® 1967__,___ er lJS r:�i 1� I PHOTOREVISED 1980.,, . „, A,i( o I. 0 e�, , q' o ) c:) a4�- �r*III=a iI ' ' ,_ �� •1_� Ielpi S:°? 0 v:_-_, 0 ilio, 'f" !w..7.„.t4, _ 4 ., _ I Iv / Nriet7P=-10%, 0 1'.,- 950 O O '� 4 % ��',�. 1: �g itt.ig:il)sch= I -41-11rt g ic.) rs J •*LI,i ( ,Tniiikok , ----_---c ._ p..s_______., r .... . I „II _ „9„), 6 tea =-, Z� g a� 16_, _ ., ....iti....i, . ------ I .. �” O S 1 . , ' PROPT ON ' ... .. ...6 a lit ea g IN fr. . _.$1:20# o o rr �� l ill D I O c O e:111114\__14---6 '-A —aogei°6 Jar(97 t .. 0 • .0 Lfi. O ® . - -� O 9� fp- ----,\-111/ 1110r IffOr r �i •J�tia a�, _ � �),O III 1 O o ,�pp� \, ° O•: � ,`` ..O_1 � © I' '930 �, � � 950'/1/�\ -✓�/)� CJ� .-.1// 'I I ' 1 SCALE 1:24 000 1 MILE 0 __ -- 2000 3000 4000 000 6000 7000 FEET MINN. I I 1000 0 1000 — ,--— 1 KILOMETER 0 I y 5 0 CONTOUR INTERVAL 10 FEET QUADRANGLE LOCATION NATIONAL GEODETIC VERTICAL DATUM OF 1929 I _ Regional Location Diagram GME CONSULTANTS. INC. rm I Senior Housing Addition Gaot.1400 l• Materials •Environmental mental Oak Park Heights, Minnesota 14000 21st Avenue North lEr-...IM`� 5/99 CIE Project No.7735-A Minneapolis. Minnesota 1612) 559-1859 I SINGLE FAMILY HOMES OAKGREEN AVENUE N. HOUSE WALL HOUSES FOUNDATION LGJ DEBRIS IN FOUNDATION FARM EQUIPMENT CHIMNEY I rilL I •TIRES I AST - TRUCTION CONS�� DEBRIS BUN TANK ROCKN BRUSH I M Lo I o • — • I VACANT WET LAND B R EID WOOD F' ILL I . PILES I w ; � \ J ; ✓ 0 Z w z LiJ !> ii LEGEND _______ PROPERTY 1 in Iw BOUNDARY I' Q TREE LINE o ��' (APPROXIMATE) I m WETLAND 1 — • — ' —' (APPROXIMATE) STILLWATER AUTO PARTS �- TREE LINE ec SALVAGE YARD I w I I X 0 O 1 4 L ----L - _1 - APPROXIMATE VACANT VACANT SCALE ' FEET 0' 200' 1 7735A.GCD APPROXIMATE SITE SKETCH GME CONSULTANTS. INC. SENIOR HOUSNG ADDITION GeoteeF,nicd • 21st ds •Envirormentd Er OAK PARK I-EIGHTS. I ESOTA 1 14000 21st Avenue N. M'nneapoh. Minnesota 55447 I.(612) 559-1859 VJL SENIOR MAY 99 GME Pro jest No. 7735-A 1 1 SITE ASSESSMENT REPORT � S �r RTY BOUNDARY EXTENDED 1 /8 MILE) (PRQPE Map of Sites within 1 Mile•-'41411111:40#T '''-- -\. 111111PIIIIIIIN111111111111' ,� 1 V •'.o ems, ° ��,.�..oxw ,. �,� -�' .��� �� ®�®- ° ' } m Orleans St (D NI a � gE ., Go ,� •• :I) * 62nd St DWI IIW till �., t n '. Tower Dr W, s >' �, a {° Z n C �_ - CS • \ .. s l ' '\ iE ® $ e'` ' ; :` 5Ith$t N# a m 1 1 (s !3 '< O :t1\1 � gf � � 6t t, * h St N 'f < 6 i' rn ,. Co (..)1 •\$%-x � N .,,,et►th St N 15 � A°ttlstN / ' o a III III I II 1y L D I ^aW :.y' 0 0 �+" M %vrrx. ti • ' Miles 45th St N 1 B - C D Category: A 1/2 mi. 1/4 mi. 1/8 mi. Subject Site Databases Searched to: 1mi. 4 Single Sites al YF.f r�f� 0 0 Multiple Sites ERNS, • CERCLIS\ UST NPL, SPL, CERCLIS\ Highways and Major Roads CORRACTS NFRAP, �\ Roads (TSD) TSD, LUST, I Railroads SWLF, SCL i Rivers or Water Bodies Utilities Date of Report: May 20, 1999 For More Information Call VISTA Information Solutions, Inc. at 1 - 800 -767 -0403 Page#3 Report ID: 7735AOKPH 1 1 t I APPENDIX A QUALIFICATIONS OF ENVIRONMENTAL PROFESSIONALS - RESUMES 1 1 1 r , 1 I I r I GME CONSULTANTS, INC. TIMOTHY F. McGLENNEN Property Development Assistance Group Manager Senior Environmental Scientist I EDUCATION 111 Bachelor of Arts in Biology Minnesota, 1988 St. John's University, Collegeville, Coursework in Hydrogeology, Wetland Soil Science University of Minnesota, Minneapolis, Minnesota, 1992, 1996 CERTIFICATIONS 40-hour HAZWHOPER, Annual Refresher Training AHERA Certified Asbestos Inspector, 1990, Annual Refresher Training III AHERA Certified Asbestos Management Planner, 1990, Annual Refresher Training Certified Wisconsin Tank Site Assessor Wetland Delineation Training, 1994 - Franklin J. Svoboda& Associates, Minneapolis, Minnesota i SSIONAL AFFILIATIONS PROFS Member - Minnesota Groundwater Association Member - National Groundwater Association Member -Wetland Delineators Association IIEXPERIENCE 1997 -Present: Senior Environmental Scientist/Property Development Assistance Group M aand, GME ing, and Consultants, Inc., Minneapolis, Minnesota. Responsible for environmental staff management senior technical assistance and review of Phase I Environmental Site Assess cents, Brownfield astudies, underground storage tank removals, remedial investigations/feasibility 1 wetland evaluations. Minneapolis, Minnesota. Project 1989 - 1997: Environmental Biologist/Project Manager, GME Consultants, Inc.,the areas of Minneapolis, Minnesota.nesota. Pro management, data collection and review, consultation, and report preparation ` studies, cleanup designs, Phase I and II Environmental Site Assessments of buildings and property, under/aboveground storage tank maintenance and removal, asbestos inspection and management, wetland delineations and mitigation plans. 1986 - 1989: Instrument Operator on land and construction survey crew, Or- surveying yeron &d use& precision Engineers-Surveyors-Planners, Minneapolis, Minnesota. Land and construction optic instruments, reading blueprints, recording data, and mathematical computations. Assisted crew chief in problem solving and in consulting with contractors and city inspectors. 1988: Intern, Ecological Services Section of Fish and for identification ,Dfepar Department of Natural is r with acid rain Ststuade Paul, Minnesota. Performed gel electrophoretic work purple loosestrife and aided in mapping its statewide and invertebrate identification. Compiled distributional data on pure distribution on U.S. Geological maps. 1 1 GME CONSULTANTS M , INC. ARK MILLS OP Corporate Environmental Division Manager Principal Hydrogeologist Crosby Office Manager EDUCATION Master of University of North DakotnateGrand FooD D. M rks, 1985 Bachelor of Science Degree in Geology, Minor in Computer Science University of Minnesota at Duluth, 1983 Associate of Science Degree Brainerd Community College, 1981 CERTIFICATIONS Wisconsin Professional Geologist Certification#G-1012 PROFESSIONAL AFFILIATIONS Member - National Ground Water Association Member - Minnesota Environmental Initiative Member - Minnesota Ground Water Association uaternary Association Member - American Q g Advisory Board - Underground Tank Technology Update (University of Wisconsin Engineering Department Publication) Moderator - National Ground Water Association Outdoor Action Conference 1994, 1995 and 1996 EXPERIENCE 1989 -Present: Principal Hy dro eolo ist, Corporate Environmental Division Manager, and Cr osbyO O ffice fi ce Manager, GME Consultants, Inc., Crosby and Minneapolis, Minnesota. Responsibilities include project management, calculations, consultation and report preparation in the areas of hydrogeology and environmental eng ineerin g for forensic studies, l underground storage � � er and groundwater studies, contamination assessme nts and remedialaction feasibity studies. Management of ects corporate-wide. environmental staff and review of environmental p ro j let. espons bnvironmcludl drojects 1989: Hydrogeologist, Widseth, Smith, and Nolting, B and Comp Minnesota. Responsibilities include 19 Y development of an environmental studies workload. Managed such as underground storage tank closures,eis studies, and recycling plant permits.remedial investigations, soil cleanups, landfill closure/management plans, landfill hydrog olo g Barr Engineering Company, Bloomington, Minnesota. 1988 - 1989: Hydrogeologist and Project Manager, petroleum product and wood preservative contamination Managed several multi-disciplinary RI/FS projects at VOC, p sites. Managed a landfill hydrogeologic/engineering study. Ltd., Green Bay, Project Manager, STS Consultants, 1985 - 1988: Hydrogeologist, Environmental Geologist, and Wisconsin. Managed numerous multi-disciplinary RI/FS p ro eels, including three Wisconsin State Superfund (ERF) j and several landfill projects. Designed and implemented remedial actions at several sites including projects, an wells, soil treatment and vapor mitigation. groundwater recovery trenches, recovery 1 1 I 1 1 1 I APPENDIX B I REGULATORY DOCUMENTATION - VISTA REPORT I 1 i t 1 1 t 1 1 1 I I ASSESSMENT REPORT E SITE A L (PROPERTY BOUNDARY EXTENDED 1 /8 MILE) c LINT``` INFORMATION FORM RTI INFORMATION Mr. Greg Collatz Senior Housing Partners Project Name/Ref IV. Not Provided Senior Rice Street, Suite 240 Senior Housing Additon St, Paul, MN 55113 i 58th Street MN 55082 Oak Park Height, M 45.031141, 92.825971 ) Latitude/Loneitude: .1l4 rQ `. lf2 to•ytirEtmi TI8 lit to 112 mile 1 mile•Site Distribution 5urnrnary• mik i!d mile atab!ase -TYp of Records Agency �cy � o A) Databases searched to 1 mile. 0 o National Priorit List — 0 0 0 0 0 US EPA CO Corrective Actions and -_ 0 0 -- US EPA RRACTS RCRA 0 (TSD) associated TSD I SPL State e e uivalent'e riorit list STATE 0 0 B) Databases searched to 1/2 tulle: iStateeeuivalent CERCLIS liist p 2 STATE SCL 0 --- __ CERCLIS / Sites currently or formerly II US EPA NFRAP review b US EPA story e, permitted treatment, g 0 RCRA a 0 —? US EPA ISO diseosal':facilities LeakirteUndereround'St ra.eTanks o 0 I STATE LUST --- SWLF Permitted as solid waste STATE. incinerators, or transfer stations -- 0 � C) Databases searched to 1/4 mile: UST Registered underg round storage I STATE tanks 0 0 Registered aboveground storage STATE AST tanks., i t t 111 767 - 0403. Date Inc. at 1 -rt, May 20, 1999 �"'���' • ore information call VISTA Information Solutions, c. at 1 - BOO Page#1 For m Report ID: 7735A0KPH Version 2.6.1 1�4 t 1f2 to Within 1!$ if$t0 1/Z mire 1 rtrite I Site Distribution Summary mile Tf4 mile Agency I Database -Type oi Records D) Databases searched to 1/8 mile: Emergency Response Notification 0 US EPA ERNS S stem of sills I LG GEN RGR A registered large generators of 0 US EPA hazardous waste 0 RCRA!registered small generators of US EPA SM GEN 0 hazardous waste �_ STATE SPILLS State sills list government database t. A (-) mdica es a distance not searched the ASTM standard E-1527 for standard federal and state g This report meets th ammeters. research [t exceeds these ASTM search P SSess because it with any transaction. art,prior to proceeding. on VISTA services,in whole or in p or for customer's use of data. r3 to tel in conversion of data, FVISTA can OF be an insurer of the information,errors occurring customer se of 6ust°met,proeeeds at its own risk in choosing Y employees and independent contractors canin°omba`ion held liable for accuracy, anise,officers,d agents,customer or indirecti from an VISTA cannot be an insurer otthe accuracy customer resultin•!directl VISTA and its affiliated companies, suffered b___. story•e,relive ,loss or ex NOTES i • 1 i II 111 i 1 Iat 1 - S00 - 767 0403. Date of Report. May 7 040 Page#2.7•60560.----,00,017,-ini For more information call VISTA Information Solutions, n 1 F, Report.61 7135AOKPH 1999 Version 2.6.7 r - ESSMENT REPORT' SITE ASS EXTENDED 118 MILE} 11 ' (PRQPERTf B( UN©A street Map . awls / PIn- 7r �FtN s�«. x ti • N - �n 1®11'„„, <„, � w mI ) Orleans St / °dy t0Ue . .0 co- F o� m m 62nd St • Towe cn � . ',. z c a; {' �✓ .4k Q o st� a s 5)11)St Q iE O 1 hSt ■ ; i ' 55th StN� s ct3 2 i < z • ? {'' icy w J^ o the St N • • • • • 0. �.wm wn Miles • • 45th St • • Highway sand Major Roads Roads Subject Site Railroads Rivers or Water Bodies Utilities Date of Report. May 20' 1999 ation Call VISTA Information Solutions, Inc. at 1 - 800 -767 -0403 Page#5 For More Inform Report ID: 7735AOKPH I SITE ASSESSMENT REPORT (PROPERTY BOUNDARY EXTENDED 1 /8 MILE) SITE I NVENTORY B D I PROPERTY AND THE ADJACENT AREA ` MAP (within 1/8 mile) N Z y2d ID' W vt VISTA!D U M .� _ DISTANCE Z O o-`. 44 ri A ',� t >= a W. -_ 'N` DIRECTION Z U � t",; d No Records Found A B U SITES IN THE SURROUNDING AREA 0 r MAP (within 1/8 - 1/4 mile) ID 9 H 2 Z ' VISTA f4 J 1 Cd G1 N N :2 47 c.w 7,DISTANCE :0. C) =� t�ix' a W J VI a/+: _> DIRECTION No Records Found I A B SITES IN THE SURROUNDING`,AREA D MAP within 1/4 -1/2 mile) Z in Z ID cA tyd r t H `c0� VISTA!D OG J i1" :� N y In .0 0. DISTANCE a 4 0. U W .H '�� 2 H DIRECTI�N.'Z C1 cn rnCy: r- .rvsa. W .� 11 BAYTOWN TOWNSHIP GROUNDWATER PLUME 3722 MI 1 SEC18 T29N R2OW BAYPORT, MN 55003 603.3396 YOCUM O IULLWATER, MN 55082 gg5g078 TOM THUMB STORE #283 0.3971 2 1903 S GREELEY NE STILLWATER, MN 55082 436390 UFE IND INC 0.43 MI 2 1850 GREELEY ST S NE STILLWATER, MN 55082 I T— search criteria; X = to along (beyond search criteria).v.,a,,,,,.................0;,:._,_,v._.4 to_ L For more information call VISTA Information Solutions,atenof Report: May 20, 1999 Report ID: 7735AOKPH Page#6 III Report 2.6.1 1 SITES IN THE SURROUNDING AREA o Ark AA •MAP (within 1/2 1 mile) z ID N W N � 1 No Records Found I I t I I I I 1 I 1 iX = search criteria; • = tag-along (beyond search criteria). For more information call VISTA Information Solutions, Inc. at 1 - 800 - 767 - 0403. Report ID: 7735AOKPH Date of Report: May 20, 1999 Page#7 Version 2.6.1 I AD B UNMAPPED SITES n Z' 5 Z y� to ce cd Lid N 4 V v> "�0 0 yisra to 4914164 LAKE ELMO AIRPORT/EQUIPMENT BLDG 111111111111111111111111 i LAKE ELMO, MN 55042 278417 MN CORRECTIONAL FAC OLD SOUTH FARM DUMP CO RD 21 NR BAYPORT STILLWATER, MN 55082 8141297 STILLWATER FORD 1111111111111111 13523 N GOTH ST STILLWATER, MN 55082 2938360 IIIIIIIIIIIIII PARKING LOT BLOCK 18 BLOCK 27 STILLWATER, MN 55082 3508911 WEST OF JUNKERS/NSP TR 56TH S N 11111111111111 STILLWATER, MN 55082 6641667 OLIVE STREET DUMP STTIILLWATOER, M�EER PATH ,,,,, 2931148,,,,,,©„ STILLWATER PRISON I STILLWATER, MN 55082 5774352 KING COAL ASH TH36 COUNTY ROAD 23 STILLWATER, A. 55082 743753011111111111111111111111 1 NSP FLY ASH STILLWATER, MN 55082 KING #1 NSP KING PLANT SLAG DISPOSAL AEA NO. 7437531111111111111111111111111 I STILLWATER, MN 55082 17azzo GRANT TWP 3M DUMP SITE NE1/4 SE1/4 SEC28 T30N R21W II STILLWATER, MN 55082 s3zzaz STILLWATER 63 SAINT CRO X RAILRHWY gMENT PLAN 61 STILLWATER, MN 55082 5zs4oas MYRTLE STREET T30N R20WES29 NE1/4 STILLWATER, MN 5300761 111111111 111111 T30TN5R20W SEC21 SW1/4 SW1/4 NE1/4 STILLWATER, MN 34 o72 7 1 MCINICY OF THE THE CO RD 12 AND DEER PA STILLWATER, MN 55082 3406469 NSP KING PLANT SURFACE IMPOUNDMENTS EAST APPROXIMATELY MILE FRO THE HW I STILLWATER, MN 55082 STILLWATER PRISON HEALTH SERVICES BLDG 4740868 COUNTY RD 28 IIIIIIIIIIIIII STILLWATER, MN 55082 I X = search criteria; • = tag-along (beyond search criteria). For more information call VISTA Information Solutions, Inc at 1 - 8:00 - 7 0403. I Report ID. 7735A0KPH Page 48 Version 2.6.1 Date g D f UNMAPPED SITES y z 7244188 MCKUSICK DUMP VICINICY OF THE CO RD 12 AND DEER PA 11111111111111 STILLWATER, MN 55082 1952677 TRANSPORTATION DEPARTMENT 1111111111111111 NORTH ISD#834 606 STIILLWA ER MN 55082 STREET 2 I i I f 1 1 I I L I I t X = search criteria; • = tag-along (beyond search criteria). For more information call VISTA Information Solutions,Datenof Repor8: May 20, 9993 Report ID: 7735AOKPH Pagers Version 2.6.1 SSESSI�E�T REPORT 1 .._ , SITEA DED 1I8MILE) V PROPERTY BOUNDARY EATEN Sites Represented. as polygons Rillinsiiii , I .taw - • ? pin_ ' > , Ra ll O-- �. rte` I' -• m fi� a O Orleans S[ pi e il a c N a ''ee�" ,Ill - cu m Q I r" i • 0 c 1 coo 62nd St rill Tower Dr W (n'`".-•p' a ' U, Q. v 0 • .:. rn o ro c f , ° i -.01111AlfA7:41.111".- 1 . . ,.„.----,.,„,.....1 ,1c l' w. 5S• s,c0 ® iq c.1ST ' ? a i rC # ;. St hr{ r '- I 571,° cam. 3 3 > } j i , �, n 6t N h.St i I, % F 55th StNi i m 1 \\.. < z a I °�' I " �.., 1 f •i�v''`:L::ii::::•;.iiiii:L::v:'ii:i:Li}: • v.:„j :!:v:{::v:::v':s4i:::::i:':::''i::::'::::::�:is i::i::i:'i:.:i::':........... a S ..... .... ... . 5 z. ..... ...:.: .. 1 4 m z 0.3 0.6 Milesle S approximated from agency records or other sources such areas. These boundaries are app fe represent property boundaries, impact zones, or study t published maps. They may p source number in the site listing. For more information contact the agency referenced by �,,,.-- Highways and Major Roads I �/\ Roads �`� Railroads Subject Site Rivers or Water Bodies I - Utilities Date1999 For More Information Call VISTA Information Solutions, Inc. at 1 - 800 -767 -Q403 of Report: May 20 Page, #4 Report ID: 7735A0KPH I REPORT SITE. (PROPERTY BOUNDARY EXTENDED 1 /8 MILE) DETAILS PROPERTY AND THE ADJAGENT AREA (within 1/8 mile) INo Records Found 1 SITES IN THE SURROUNDING AREA (within 118 1/4 mile) No Records Found I SITES IN THE SURROUNDING AREA (within 1/4 - 1/2 mile) I _ Maple VISTA lD 3722362 VISTA BAYT:fJWIM TOW N SHIP GROUIMUVV I R Distanc 0,35 Mk 1 ' AddreSS'. PLUME Plotted as Polygon SEC1BT29N R20IN BAYPORT,'MN 55003 EPA ID: MND982425209 Agency/ Sddr 5594 BAYTOWN TOWNSHIP GROUND WATER PLUME Agency Address: SIB, T29N,R2OW BAYTOWN TWP, MN 55042 S EPA Region: o Congressional District: Federal facility: () COUNTY OWNED Agency code de O Facility Ownership: unknown Site Incident Category: SITE IS NOT INCLUDED ON THE DOCKET Federal Facility Docket: CURRENTLY ON FINAL NPL NPL Status: unknown Incident Type: o Proposed NPL Update #: o IFinal NPL Update #: oSNx Financial Management System ID: o Latitude: o Longitude: Agency Code () Lat/Long Source: Unknown I Lat/Long Accuracy: Unknown Dioxin Tier: �otozos USGS Hydro Unit: Unknown RCRA Indicator: BAYTOWN TWP GROUNDWATER CONT Alias Name: I * VISTA address includes enhanced city and ZIP. For more information call VISTA Information Solutions,ate Date Repora: May 20, �99 3 Report ID: 7735AOKPH Page#10 Version 2.6.1 SITES IN THE SURROUNDING AREA (within 1/4 - 1/2 Mile) CONT. NOT REPORTED Alias Street: Alias City: REPORTED Alias Latitude: 0 Alias Zip: NOT REPORTED Alias Longitude: Alias State: MN NOT REPORTED Alias Description: LAKE ELMO AIRPORT GROUNDWATER PLUME Alias Name: NOT REPORTED Alias Street: Alias City: NOT REPORTED Alias Latitude: Alias Zip: NOT REPORTED Alias Longitude: 0 Alias State: MN NOT REPORTED Alias Description: BAYTOWN TOWNSHIP GROUNDWATER PLUME/LAKE Alias Name: 518, i29N,R20W Alias Street: 4459480 BAYTOWN TWP Alias Latitude: Alias City: 9252540 Alias Zip: 55042 Alias Longitude: Alias State: MN NOT REPORTED Alias Description: BAYTOWN TOWNSHIP GROUNDWATER PLUME/LAKE Alias Name: NOT REPORTED Alias Street: o Alias City: NOT REPORTED Alias Latitude: 111111111 1 Alias Zip: NOTREPORTED Alias Longitude: Alias State: NOT REPORTED NOT REPORTED Alias Description: °Unit Id: SIIEWIDE Unit Name: 1 Unit Id: STATE DEFERRAL SITE Unit Name: STATE,FUND FINANCED Type: DISCOVERY Lead Agency: Cate Of Unknown UNKNOWN g y'Qualifier: NOT REPORTED Name: NO1 REPORTED Actual Start Date: Plan Status: unknown Actual Completion APRIL 6, 1988 Date: Type: HAZARD RANKING SYSTEM SCORE Lead Agency: STATE,FUND FINANCED UNKNOWN Category: unknown Qualifier: NOT REPORTED Name: NOTREPORTED Actual Start Date: OCTOBER 14, 1992 I Plan Status: Unknown Actual Completion Date: Type: FINAL LISTING ON NPL Lead Agency: STATE,FUND FINANCED Category: unknown Qualifier: UNKNOWN NOT REPORTED Name: NOT REPORTED Actual Start Date DECEMBER 16, 1994 Plan Status: unknown Actual Completion Date: * VISTA address includes enhanced city and ZIP. For more information call VISTA Information Solutions,atenoF Report May May 20, 1999 Report ID: 7735AOKPH Page#11 Version 2.6.1 I SITES tNTHE SURROUNDING AREA (within 1/4 - 1/2 mile) CONT. EPA FUND FINANCED Lead Agency: Unknown Type: PROPOSED FOR NPL Category: NOT REPORTED UNKNOWN Name: NOT REPORTED Actual Start Date: OCTOBER 14, 1992 Name: Actual Completion Unknown Date: Plan Status: STATE,FUND FINANCED LOWER PRIORITY PRELIMINARY ASSESSMENT Lead Agency: unknown Type: Category: NOT REPORTED Qualifier: Actual Start Date: JANUARY 4, 1989 NOT REPORTED Completion Name: Actual Comp Unknown Date: Plan Status: STATE,FUND FINANCED SCREENING SITE INSPECTION Lead Agency: Unknown Qual Category: NOT REPORTED HIGHER PRIORITY Namle: Actual Start Date: OCTOBER 2T D NOT REPORTED Completion Name: Actual Comp . Unknown Date: Plan Status: PRP LEAD UNDER STATE COMBINED RI/FS Lead Agency: Unknown Type,. Category UNKNOWN SEPTEMBER 30, 1991 Namleef: Actual Start Date: NOT REPORTED NOT REPORTED Completion Name. PRIMARY Actual Comp Plan Status: Date: �NQ98z425209 EPA ID:NPL . National Priorit List/ $RC# 5691 BAYTOWN TOWNSHIP GROUND WATER PLUME 518,129N,R2OW Agency AddreSS: BAYTOWN TOWNSHIP,MN 55042 0 EPA Region: o Congressional District: Agency Code () Federal Facility: NOT AVAILABLE Facility Ownership: unknown Site Incident Category: Code () Federal Facility Docket: Agency c C UNKNOWN I NPL Status: Unknown Incident Type: o proposed NPL Update #: o Final NPL Update #: NOT REPORTED Financial Management System ID: o Latitude: o Longitude: Agency Code () Lat/Long Source: unknown Lat/Long Accuracy: Unknown Dioxin Tier: o USGS Hydro Unit: Unknown RCRA Indicator: BAYTOWN TWP GROUNDWATER CONT Alias Name: NOIREPORIED Alias Street: NOT REPORTED NOT REPORTED 0 Alias Latitude: o Alias City: Alias Longitude: 1 Alias Zip: NOT REPORTED Alias State: i ` VISTA address includes enhanced city and ZIP. 1999 Date of Report: May 20, e#12 For more information call VISTA Information Solutions, Inc. at 1 - 800 - 761 - 0403. II F 9 Report ID. 7735AOKPH Version 2.6.1 I E IN THE SURROUNDING AREA (within 1/4 - 112 mile) CONT. rV1a:p la I SITES VISTA In#. 633673 VISTA YOCUM 41L Distance/Qirectton■ () 39 Ml/ NE Plotted as. `, point Address 1940 $ GREELEY ST 1 EPAtAgeneylD: N/A STIILWATER,I�N 55082 STATE LUST - State Leaking Underground Storage,Tank/ SRC# 5518 SAME AS ABOVE Agency Address: 129z Leak ID#: 1 1129296 I Leak Report Date: TOM Lead Agency: Contact: TOM WASHINGTONOWNER INFO:YOCUM OIL C0,2719 STILLWATER RD,STILLWATER MN,55119 Map ID Description / Comment: 4858078 VISTA i--, Distance/111ecton:fl.39 MI / NE TOM THUMB STORE #28 Point VISTA plotted es: Address: 1g03!S GREELEY N/A STILLWATER, MN 55082! EPA/Agency ID: I State Leaking Underground Storage Tank / SRC# STATE LUST. S 5518 SAME AS ABOVE Agency Address: 3 Leak ID#: 6893 Leak Report Date: 12/30/93 Case Closed Date: Remediation Status: GREG CLOSED SWANSON Lead Agency: GREG SWANSON Contact: COUNTY:WASHINGTONOWNER INFO:TOM THUMB INC,110 E 17TH ST,HASTINGS,MN,55033 Map1D Description / Comment: 4363917 VISTA ID# VISTA `! UFE IND INC Distance/Ditectcn:0.43 MI/ NE `: Platted as Point ,: Address:` 1850 G.REELE1 STS MNDo2a5so75s STILLWATER, MN 5508:2 EPA ID:t NFRAP /SRC# 5595 UFE INDUSTIAL INCORPORATION Agency Address: 1850 GREELEY STREET SOUTH STILLWATER,MN 55082 1 Alias Name: UFE IND INC NOT REPORTED 4503120 Alias Street: WASHINGTON Alias Latitude: 9249000 U Alias City: Alias Longitude: NOT REPORTED Alias Zip: Alias State: MN NOT REPORTED Alias Description: UFE IND INC Alias Name: 1850 GREELEY ST SOUTH 4503120 Alias Street: STILLWATER Alias Latitude: 9249000 Alias City: 55082 Alias Longitude: Alias Zip: Alias State: MN NOT REPORTED Alias Description: I v:14:0070 0 0,,.I 2,,0 'at.----------—-le,,. VISTA address includes enhanced city and ZIP. 1999 more information call VISTA Information Solutions, Inc. at 1 - 8:00 - 767 0403. For m Page Report ID. 7735A0KPH 1 Version 2.8.1 I SITES IN THE SURROUNDING AREA (within 1/4 - 1/2 mile) CONY. 5 EPA Region: 0 I Congressional District: Agency Code () Federal Facility: OTHER Facility Ownership: unknown Site Incident Category: SITE IS NOT INCLUDED ON THE DOCKET Federal Facility Docket: NOT ON NPL NPL Status: 1 Incident Type: unknown 0 Proposed NPL Update #: o Final NPL Update #: NOT REPORTED Financial Management System ID: o RLatitude: o Longitude: Agency Code () Lat/Long Source: Unknown Lat/Long Accuracy: Unknown Dioxin Tier: 1o3000s II USGS Hydro Unit: Unknown RCRA Indicator: o Unit Id: ENTIRE SITE EPA FUND FINANCED 1 Unit Name: DISCOVERY Lead Agency: Unknown Type: Category: UNKNOWN QUalil OT: Actual Start Date: NOT REPO NOT REPORTED NT REPO Name: Actual Completion Unknown Plan Status: Date: STATE,FUND FINANCED PRELIMINARY ASSESSMENT Lead Agency: Unknown Type: NO FURTHER REMEDIAL ACTION Category: NOT REPORTED Qualifier: PLANNED Actual Start Date: NOT REPORTED Actual Comp IetlOn UNKNOWN I Name: Unknown Date: Plan Status: SITES IN THE SURROUNDING AREA (within 1/2 1 mile) INo Records Found 1 1 1 1 I - ' VISTA address includes enhanced city and ZIP. For more information call VISTA Information Solutions, Incf at 1 - 800 - 7 - 0403. 9 0 Report ID 7 1 735AOKPH Version 2.6.1 Date I II UNMAPPED SITES #: 49141 fi4 VISTA LAKE EEMO1RPORTIEQUIPMENT BLDG VISTA ID Address', LAKE EtMO, MN 55{}42 EPA/Agency ID: N/A STATE LUST - State Leaking Underground Storage Tank /'SRC# 5518 LAKE ELMO AIRPORT/EQUIPMENT BLDG Agency Address: WEST LAKELAND/BAYPORT,MN 55042 4513 Leak ID#: 451 /sl I Leak Report Date: 1/15593 Case Closed Date: CLOSED Remediation Status: DICK KEINTZ I Lead Agency: DICK KEINTZ Contact: COUNTY:WASHINGTONOWNER INFO:METROPOLITAN AIRPORTS Description / Comment. COMMISSION,PO BOX 11700,SAINTPAUL,MN,55111 VISTA MN CORRECTIONAL FAC OLD SOUTH FARM VISTA tD#> 278437 '. Address*: DUMP . CO RD 21 NR BAYPORT W10981089758!: STILLWATER, MN 550$2<' . EPA ID: NFRAP /SRC# 5595 SAME As ABOVE I Agency Address: 5 EPA Region: o Congressional District: Agency Code () Federal Facility: o1HER Facility Ownership: known Site Incident Category: un unk IwOT INCLUDED ON THE DOCKET Federal Facility Docket: NOT ON NPL NPL Status: Unknown Incident Type: o I Proposed NPL Update #: o Final NPL Update #: NOT REPORTED Financial Management System ID: o Latitude: o Longitude: Agency Code () Lat/Long Source: nknown Lat/Long Accuracy: Unknown Dioxin Tier: 7030005 USGS Hydro Unit: 103unk0nown I RCRA Indicator: 0 Unit Id: ENTIRE SITE Unit Name: STATE,FUND FINANCED DISCOVERY Lead Agency: Unknown Type: Category: UNKNOWN NOT REPORTED Name: Actual Start Date: NOT REPO NOT REPORTED Name: Actual Completion 1 Unknown Plan Status: Date: I ,,,a w a....,'*.4 seste.: 0--,..---4 * VISTA address includes enhanced city and ZIP. For more information call VISTA Information Solutions, Inc. at 1 - 8 0- 20 99 3 Report ID: 7735 AOKPH age>/9 Version 2.6.1 Date I UNMAPPED SITES CONT. STATE,FUND FINANCED PRELIMINARY ASSESSMENT Lead Agency: unknown Type: Qualifier: LOWER PRIORITY Category: NOT REPORTED I NOT REPORTED Actual Start Date: AUGUST 1, 1985 Name: Actual Completion Unknown Plan Status: STATE,FUND FINANCED SCREENING SITE INSPECTION Lead Agency: Type: Date: NO FURTHER REMEDIAL Category: Unknown Qualifier: PLANNED NOT REPORTED APRIL 2, 1989 Actual Start Date: NOT REPORTED Name: Actual Completion Plan Status: Unknown Date: VISTA lD#: 23:8360 IVISTA PARKING COT `. Rd re S BLO.CK 18 BLOCK 27 STILLWATER {VIN 55082 EPA/Agency ID: N/A 5518 STATE LUST State Leaking Underground'.Storage Tank / SRC# SAME AS ABOVE Agency Address: 4204 Leak ID#: 7/3/91 leak Report Date: /3/91 s2 Case Closed Date: LOSED 1 Remediation Status: CAVE MAGNUSON Lead Agency: DAVE MAGNUSON Contact: COUNTY WASHINGTONOWNER INFO:CITY OF STILLWATER,324 S MAIN 1 D@scrlptlOn / Comment: ST,STILLWATER,MN,55082 I I I I 1 I I I ,04 s,,,a.saw,,,,,-—,:64 0 s w's'a00 .--,.1/40 t,f-e„, For more address includes enhanced city and P. F for more information call VISTA Information Solutions,atenof Repor8:OMay 20, 1999 Report ID: 7135AOKPH Page#16 Version 2.6.1 UNMAPPED SITES CONT. VISTA [D#: ' 3508911 VISTA JUNKERS/NSP SITE Add:ress , WEST Of STAGECOACH TR 56TH $ N'. STILLWATER,:MN 550&`t EPA' ID: MND985749811 NFRAP f SRC# 5595 'I JUNKERS/NSP SITE Agency Address: WEST OF STAGECOACH TR 56TH S N OAK PARK HEIGHTS, MN 55082 5 EPA Region: 0 Congressional District: Agency Code () Federal Facility: UNKNOWN Facility Ownership: Unknown Site Incident Category: SITE IS N01 INCLUDED ON THE DOCKET Federal Facility Docket: Nor oN NPL NPL Status: Unknown Incident Type: 0 Proposed NPL Update #: o Final NPL Update #: NOT REPORTED Financial Management System ID: 0 Latitude: o Longitude: Agency Code () Lat/Long Source: unknown Lat/Long Accuracy: Unknown Dioxin Tier: 7030005 USGS Hydro Unit: unknown RCRA Indicator: 0 Unit Id: ENTIRE SITE 1 Type: Name: Lead Agency: STATE,FUND FINANCED Type. DISCOVERY Unknown UNKNOWN Category: Qualifier: NOT REPORTED Name: NOT REPORTED Actual Start Date: SEPTEMBER 1, 1992 ' Unknown Actual Completion Plan Status: Date: Lead Agency: STATE,FUND FINANCED INTEGRATED ASSESSMENT/FIELD DATA Unknown L Type COLLECTED Category: Qualifier: NO FURTHER REMEDIAL ACTION JUNE 1, 1993 PLANNED Actual Start Date: NOT REPORTED SEPTEMBER 1, 1995 Name: Actual Completion Unknown Date: Plan Status: STATE,FUND FINANCED PRELIMINARY ASSESSMENT Lead Agency: Unknown Type: Qualifier: HIGHER PRIORITY Category: NOT REPORTED t Name: NOT REPORTED Actual Start Date: SEPTEMBER REPORTED 3, 1992 Unknown Actual Completion Plan Status: Date: STATE,FUND FINANCED SCREENING SITE INSPECTION Lead Agency: Unknown Type: Qualifier: NO FURTHER REMEDIAL ACTION Category: JUNE 1, 1993 PLANNED Actual Start Date: Name: NOT REPORTED SEPTEMBER 1, 1995 Actual Completion Plan Status: ov000,1 Unknown Date: * VISTA address includes enhanced city and ZIP. For more information call VISTA Information Solutions, na3 Report ID: 7735A0KPH Page 99 Version 2.6.1 Date of Report: May 20, 999 UNMAPPED SITES CONT. II I i VISTA ID#: > 6&4'E6&7 VISTA! OLIVE .STREET. DUMP address , LOT 1 BLOCK. 1 DEER PATH STILLWATER,iMN Agency ID: 7590 SCL - State Es uivalent CERCLIS List/ SRC# 5437 AS ABOVE Agency Address: UNKNOWN Status: NOT AVAILABLE Facility Type: NOT AVAILABLE ' Lead Agency: ACTIVE SITE State Status: UNKNOWN UNKNOWN UNKNOWN Pollutant 1: Pollutant 2: Pollutant 3: �(ISTA ID# Zg311�8 VISTA STILLWATER`PRiSON Address'. STILLWATER, MN 55082 STATE LUST - State Leaking Underground Storage Tank / SRC# EPA/Agency ID N/A 5518 SAME AS ABOVE Agency Address: 2802 Leak ID#: 582i90 Leak Report Date: 12i26i90 Case Closed Date: CLOSED Rerediation Status: PETER BJURSTROM Lead Agency: PETER BJURSTROM Contact: COUNTY:WASHING 10NOWNER INFO:STILLWATER Description / Corn rnent: PRISON„STILLWATER,MN,55082 I VISTA ; KIND COAL ASH IISTA ID Address TH36 COUNTY ROAD 23 ST VII MN' 55082 Agency ID. 5770 SCL - State E.uivalent CERCLIS List/SRC# 5437 COAL ASH 00410 0,0?1°'70.•s -00/1,•Agency Address: TH35 COUNTY ROAD 23 OAK PARK HEIGHTS,MN UNKNOWN NOT AVAILABLE NOT AVAILABLE ACTIVE SITE UNKNOWN UNKNOWN UNKNOWN Status: Facility Type: Lead Agency: State Status: Pollutant 1: ' Pollutant 2: Pollutant 3: I I • VISTA address includes enhanced city and ZIP. For more information call VISTA Information Solutions, Inc, at 1 - 8:00 - 20, 949 0403. Report ID: 7735A0KPH Page#18 2.6.1 r UNMAPPED SITES CONT. VISTA fD#: 7437530 VISTA NSF FLY; ASH A.S. KlMG #1 Addressx; STILLWATER, MN 55082 [STATE SWLF- Solid Waste Landfill/ SRC# 4837 Agency ID: SW-053 Agency Address: NSP FLY ASH A.S.KING 11 OAK PARK HEIGHTS, MN 55082 INDUSTRIAL Facility Type: CLOSED Facility Status: PERMITTED/LICENSED Permit Status: VISTA NSP IN AN T $LAG DISPOSAL AEA NO VISTA ID-#: ' 7433.531 Address*: STILLWATER ION 55082 SW-054 I,STATE SWLF-Solid Waste Landfill/ SRC# 4837 Agency ID: Agency Address: NSP KING PLANT SLAG DISPOSAL AEA NO. OAK PARK HEIGHTS,MN 55082 INDUSTRIAL Facility Type: ACTIVE/OPEN Facility Status: PERMITTED/LICENSED Permit Status: GRANT TWP 3M DUMP SITE VISTA lD#; 178.220 VISTA:, Address` NE1/4 SE1/4 5EC28 T30N RZ1W STILLWATER MN 55082' EPA ID: MNDSa15zs42s NFRAP / SRC# 5595.! Agency Address: GRANT TOWNSHIP 3M DUMP SITE g y NEI/4 SEI/4 SEC28 T30N R2IW STILLWATER,MN 55082 111 5 EPA Region: 0 Congressional District: Agency Code () Federal Facility: OTHER Facility Ownership: unknown Site Incident Category: Federal Facility Docket: SITE IS NOT INCLUDED ON THE DOCKET NOT ON NPL NPL Status: Unknown Incident Type: Proposed NPL Update #: 0 0 Final NPL Update #: NO1 REPORTED Financial Management System ID: 0 Latitude: 0 Longitude: Agency Code O Lat/Long Source: Unknown Lat/Long Accuracy: Unknown Dioxin Tier: 7030005 USGS Hydro Unit: Unknown RCRA Indicator: 0 Unit Id: ENTIRE SITE Unit Name: r VISTA address includes enhanced city and ZIP. For more information call VISTA Information S o l u t i o n s, Inc at 1 - 800 : May 7 0403. Report ID: 7735AOKPH Page#19 Version 2.6.1 Date I 1 I)NMAPPED SITES CONT I Type: DISCOVERY Lead Agency: STATE,FUND FINANCED UNKNOWN Category: Unknown Qualifier: NOT REPORTED Name: NOT REPORTED Actual Start Date: Plan Status: Unknown Actual Completion UNKNOWN I Date: PRELIMINARY ASSESSMENT Lead Agency: STATE,FUND FINANCED Type: Unknown Qualifier: LOWER PRIORITY Category: NOT REPORTED Actual Start Date: NOT REPORTED Name: JUNE 3, 1987 Plan Status: Unknown Actual Completion Date: SCREENING SITE INSPECTION Lead Agency: EPA FUND FINANCED ' Type: Unknown Qualifier: NO FURTHER REMEDIAL ACTION Category: PLANNED Actual Start Date: NOT REPORTED Name: NOT REPORTED OCTOBER 3, 1991 Unknown Actual Completion Plan Status: Date: VISTA VISTA IQ#: 5264046 STILLWATER CITY DUMP SITE Address": INYRTLE STREET T3ON. R2OW S29 `NE1/4 STILLWATER, MN 1 f SCL - State Equivalent CERCLIS List/ SRC# 5437 Agency ID: 0040 Agency Address: UNKNOWN NOT AVAILABLE NOT AVAILABLE ACTIVE SITE UNKNOWN UNKNOWN UNKNOWN Status: Facility Type: lead Agency: State Status: Pollutant 1: Pollutant 2: Pollutant 3: SAME AS ABOVE ISTA LOT 7 VISTA OP 5300761 V ' 5' Address*: T3ON.R20WjSEC21 SW114 SW1/4 NE1/4 STILIW ATER', M N SCL - State Equivalent CERCLIS List/ SRC# 5437 Agency ID. 5470 SAME AS ABOVE Agency Address: UNKNOWN NOT AVAILABLE NOT AVAILABLE CLOSED UNKNOWN UNKNOWN UNKNOWN Status: Facility Type: Lead Agency: State Status: Pollutant 1: Pollutant 2: Pollutant 3: I * VISTA address includes enhanced city and ZIP. For more information call VISTA Information Solutions, Inc. at 1 - 800 - 767 - 0403. Report ID: 7735AOKPH Date of Report: May 20, 1999 Page#20 Version 2.6.1 • I UNMAPPED SITES C01gT. I VISTA .:' MCKUSICK Dump . VISTA ID#: 34.07210 I Address' VICINICY OF :THE CO RD.12 ANI) DEER PA TILLwATER, mN 550&2. (STATE SWLF - Solid Waste Landfill L SRC# 5694 EPA/Agency ID: N/A I Agency Address: Facility Type: SAME AS ABOVE OPEN DUMP Facility Status: NOT AVAILABLE I Permit Status: NOT AVAILABLE VISTA:;; NSP KING PLANT SURFACE IMPOUNDMENTS' VISTA ED#: • 3406469 Address*: EAST APPROXIMATELY MILE FRO THE HW tSTILLWATER,MN 5508.2 EPA/Agency ID: N/A (STATE SWLF - Solid Waste Landfill / SRC# 5694 I Agency Address: NSP KING PLANT SURFACE IMPOUNDMENTS g Y EAST APPROXIMATELY MILE FRO THE HW OAK PARK HEIGHTS,MN 55082 Facility Type: OPEN DUMP Facility Status: NOT AVAILABLE Permit Status: NOT AVAILABLE STATE SWLF - Solid Waste Landfill! SRC# 5694 EPA/Agertey ID: IN/A' Agency Address: NSP KING PLANT SURFACE IMPOUNDMENTS g Y EAST APPROXIMATELY MILE FRO THE HW OAK PARK HEIGHTS,MN 55082 Facility Type: OPEN DUMP Facility Status: NOT AVAILABLE Permit Status: NOT AVAILABLE I VISTA STILLWATER RAISON HEALTH SERVICES BLDG VISTA 1D11: 41408&B Address COUNTY RD 28 STILLWATER, MN 55082 enc EPA/A ID: N/A STATE LUST - State Leaking Underground Storage Tank./ SRC# 9 y 5518 Agency Address: SAME AS ABOVE Leak ID#: 6531 I Leak Report Date: 7/12/93 Case Closed Date: 2/8/94 Remediation Status: CLOSED I Lead Agency: RON SOCKNESS Contact: RON SOCKNESS Description / Comment: COUNTY:WASHINGTONOWNER INFO.STILLWATER PRISON,BOX Ip 55,STILLWATER,MN,55082 I I 1 '6:47'''wlig °"....0.0.----....----0,000000,.."4,..01_ If. VISTA address includes enhanced city and ZIP. For more information call VISTA Information Solutions, Inc. at 1 - 800 - 767 - 0403. I Report ID: 7735A0KPH Date of Report: May 20, 1999 Page#21 Version 2.6.1 I UNMAPPED SITES CANT. VISTA MfCKUSICK DUMP VISTAJD#: 72443$8 Address'; VICINICY OF THE CO RD 12 AND DEER PA STILLWATER, MN 55082 STATE SWLF - Solid Waste Landfill/ SRC# 5694 EPA/Agency ID: N/A Agency Address: sAMEASABOVE Facility Type: OPEN DUMP Facility Status: NOT AVAILABLE Permit Status: NOT AVAILABLE VISTA TRANSPORTATION 0!EPARTMEl1IT VISTA! ID#: 1' 52fi77 Address* ISD#834;606 NORTH?MAIN STREET STILLWATER,MN S5082 STATE LUST - State Leaking Underground.Storage Tank / SRC# EPA/Agency ID: N/A 1 5518 Agency Address: SAME AS ABOVE Leak ID#: 2928 Leak Report Date: 7/18/90 Case Closed Date: 9/19/94 Remediation Status: CLOSED Lead Agency: MIKE BRABENDER Contact: MIKE BRABENDER Description / Comment: COUNTY:WASHINGTONOWNER INFO:ISD#834,1875 SOUTH GRELY STREET,STILLWA TER,MN,55082 1 I I I I I ' VISTA address includes enhanced city and ZIP. For more information call VISTA Information Solutions, Inc. at 1 - 800 - 767 - 0403. Report ID: 7735A0KPH Date of Report: May 20, 1999 Version 2.6.1 Page#22 I I NFRAP VISTA conducts a database search to identify all sites within 1/2 mile of your property. SRC#: 5595 The agency release date for CERCLIS-NFRAP was January, 1999. I NFRAP sites may be sites where, following an initial investigation, no contamination was found, contamination was removed quickly, or the contamination was not serious enough to require Federal Superfund action or NPL consideration. I SCL VISTA conducts a database search to identify all sites within 1/2 mile of your property. SRC#: 5437 The agency release date for Voluntary Investigation Cleanup Program (VIC) Database was October, 1998. I This database is provided by the Pollution Control Agency, Site Assessment Unit. The agency may be contacted at: 612-296-8407. I The Minnesota Voluntary Investigation and Cleanup Program Database includes identified hazardous waste sites where the investigation and cleanup activities are completed through Voluntary actions of the responsible party(s). I RCRA-TSD VISTA conducts a database search to identify all sites within 1/2 mile of your property. SRC#: 5596 The agency release date for HWDMS/RCRIS was February, 1999. I The EPA's Resource Conservation and Recovery Act (RCRA) Program identifies and tracks hazardous waste from the point of generation to the point of disposal. The RCRA Facilities database is a compilation by the EPA of facilities which report generation, storage, transportation, treatment or disposal of hazardous waste. RCRA I TSDs are facilities which treat, store and/or dispose of hazardous waste. SWLF VISTA conducts a database search to identify all sites within 1/2 mile of your property. SRC#: 4837 The agency release date for Permitted Solid Waste Disposal Facilities was April, 1998. IThis database is provided by the Pollution Control Agency, Document Center. The agency may be contacted at: 612-296-7276. I SWLF VISTA conducts a database search to identify all sites within 1/2 mile of your property. SRC#: 5694 The agency release date for Open Dump Inventory was March, 1999. I This database is provided by the PW SW Division, PGM Development. The agency may be contacted at: 612-297-1796. LUST VISTA conducts a database search to identify all sites within 1/2 mile of your property. ISRC#: 5518 The agency release date for Spills and Leak Report Log was December, 1998. This database is provided by the Pollution Control Agency, Hazardous Waste IDivision-Tanks and Spills. The agency may be contacted at: 612-297-2552. C) DATABASES SEARCHED TO 1/4 MILE IS 's VISTA conducts a database search to identify all sites within 1/4 mile of your property. SRC#: 5227 The agency release date for Statewide Facilities Tank Information wa s August, 1998. I This database is provided by the Department of Agriculture, Agronomy and Plant Protection. The agency may be contacted at: 612-297-5640. I I vNisavg6,::"'-.‘w4°67—",....—*• , For more information call VISTA Information Solutions, Inc. at 1 - 800 - 767 - 0403. Report ID: 7735A0KPH Date of Report: May 20, 1999 Version 2.6.1 Page#24 I UST's VISTA conducts a database search to identify all sites within 1/4 mile of your property. SRC#: 5693 The agency release date for Underground Storage Tanks was February, 1999. This database is provided by the Print Communications Division. The agency may be contacted at: 612-297-2552; Caution-Many states do not require registration of heating oil tanks, especially those used for residential purposes. AST's VISTA conducts a database search to identify all sites within 1/4 mile of your property. SRC#: 5693 The agency release date for Aboveground Storage Tanks was February, 1999. This database is provided by the Print Communications Division. The agency may be contacted at: 612-297-2552. D) DATABASES SEARCHED T(1 tI8 MILE ERNS VISTA conducts a database search to identify all sites within 1/8 mile of your property. SRC#: 5598 The agency release date for was December, 1998. ' The Emergency Response Notification System (ERNS) is a national database containing records from October 1986 to the release date above and is used to collect information for reported releases of oil and hazardous substances. The database contains information from spill reports made to federal authorities including the EPA, the US Coast Guard, the National Response Center and the Department of Transportation. The ERNS hotline number is (202) 260-2342. RCRA-LgGen VISTA conducts a database search to identify all sites within 1/8 mile of your property. SRC#: 5596 The agency release date for HWDMS/RCRIS was February, 1999. The EPA's Resource Conservation and Recovery Act (RCRA) Program identifies and tracks hazardous waste from the point of generation to the point of disposal. The RCRA Facilities database is a compilation by the EPA of facilities which report generation, storage, transportation, treatment or disposal of hazardous waste. RCRA Large Generators are facilities which generate at least 1000 kg./month of non-acutely hazardous waste ( or 1 kg./month of acutely hazardous waste). RCRA-SmGen VISTA conducts a database search to identify all sites within 1/8 mile of your property. SRC#: 5596 The agency release date for HWDMS/RCRIS was February, 1999. The EPA's Resource Conservation and Recovery Act (RCRA) Program identifies and tracks hazardous waste from the point of generation to the point of disposal. The RCRA Facilities database is a compilation by the EPA of facilities which report generation, storage, transportation, treatment or disposal of hazardous waste. RCRA ' Small and Very Small generators are facilities which generate less than 1000 kg./month of non-acutely hazardous waste. SPILL VISTA conducts a database search to identify all sites within 1/8 mile of your property. ' SRC#: 5638 The agency release date for Spills and Leak Report Log was January, 1999. This database is provided by the Pollution Control Agency, Hazardous Waste Division-Tanks and Spills. The agency may be contacted at: 612-297-8499. I ti For more information call VISTA Information Solutions, Inc. at 1 - 800 - 767 - 0403. Report 1 7735A0KPH Version 2.6.1 Date of Report: May 20, 1999 Page#25 1 1 APPENDIX C ASTM OWNER QUESTIONNAIRE 1 1 I I I 1 1 i 1 ENVIRONMENTAL SITE ASSESSMENT I TRANSACTION SCREEN QUESTIONNAIRE IThis document is an excerpt of Practice E 1528-96:Standard Practice for Environmental Site Assessments:Transaction Screen Process,which is under the jurisdiction of ASTM Committee E-50 on Environmental Assessment and is the direct responsibility of Subcommittee E 50.02 on Commercial Real Estate Transactions. This questionnaire represents only Sections 5 and 6 of Practice I E 1528-96 and should not be construed as being the complete standard. It is necessary to refer to the full standard prior to using this questionnaire. COPYR/GHT©1996 AIMERIC ri SOCIETY FOR IESTLNG AND MATERIALS,West Conshohocken, PA. Prior edition copyrighted 1993. PCN: 13-515280-65. For the complete standard, or to order additional copies of this questionnaire,contact ASTM Customer Service at(610)832-9585. IS. Introduction to Transaction Screen Questionnaire responses,or the questions have been asked in writing sent by certified or registered mail,return receipt requested. red 5.1 Process—The transaction screen process consists of asking questions carrier and no responses o have postage obttain d after by private,ttwo follow-up telephone contained within the transaction screen questionnaire of owners and occupants of calls were made or written request was sent again asking for responses. the property.observing site conditions at the property with direction provided by the transaction screen questionnaire, and, to the extent reasonably ascertainable, 5.53 The transaction screen questionnaire and the transaction screen guide conducting limited research regarding certain government records and certain sometimes include the phrase"to the best of your knowledge." Use of this phrase standard historical sources. The questions asked of owners are the same questions shall not be interpreted as imposing a constructive knowledge standard when it is not I as those asked of occupants. included or as imposing anything other than an actual knowledge standard for the 5.2 Cultic—The transaction screen questionnaire is followed by a person answering tie questions,regardless of whether it is used. It is sometimes designed to assist the person completing the transaction screen questionnaire. The to search out information he or he does nnot questioned have in or she tnot swe the guide to the transaction screen questionnaire is set out in Sections 7 through 10 of particular question. ' this practice.The guide is divided into three sections:Guide for Owner/Occupant Inquiry,Guide to Site Visit,and Guide to Government Records/Historical Sources 5.6 Conclusions Regarding Affirmative or Unknown Answers—If any of the Inquiry. questions set forth in the transaction screen questionnaire are answered in the 5.2.1 To assist the user,its employee or agent.or the environmental professional the questions are not answered document the answer is unk nown user should answer. myent Iin preparing areport,the guide repeats each of the questions set out in the transaction such nonresponse or answer of unknown and evaluate it in light of the ocher screen questionnaire in both the guide for owner/occupant inquiry and the guide to information obtained in the transaction screen process,including, in particular,the sire visit.The questions regarding government records/historical sources inquiry are site visit and the overnment records/historical sources inquiry. If the user decides also repeated in the guide to that section. no further inquiry is warranted after receiving no response,an answer of unknown 5.2.2 The guide also describes the procedures to be followed to determine if sion. affirmative answer,the user must document the masons for any such conclu- 5.2.2 reliance upon the tnrormat.a..ij.a prior.__;^-■•,r.: .:-.. ..at.•�:. Wit"-r c.•r_.__ under this practice. 5.6.1 Upon obtaining an affirmative answer, an answer of unknown or no 5.2.3 A user,his employee or agent,or environmental professional conducting planation o allow a�useruto conclude that no further rinquiry�ispa provide appropriate with the transaction screen process should not use the transaction screen questionnaire respect to the particular question. PP P without reference to.or familiarity from prior usage with,the guide. 5.6.2 If 5.3 User and prepares—The user conducting the transaction screen process conclude that eguide f to is pear question does not,in itself,permit a user to is the parry seeking to perform appropriate inquiry with inquiry a appropriate,n cre then process the user should t relating to this consider oton. user may delegate ry respect to the property.The information obtained from the transaction screen process relating[o this question. Iy gate the preparation of the transaction screen questionnaire to an For example,while on the site performing a site visit,a person may find a storage tank employee or agent of the user or may contract with a third party to prepare the on the property and therefore answer Question 10 of the transaction screen questionnaire on behalf of the user. The person preparing the questionnaire is the questionnaire in the affirmative. However, during or subsequent to the owner/ prepares,who may be either the user or the person to whom the user has delegated occupant inquiry,the owner may produce evidence that substances now or histori- the preparation of the transaction screen questionnaire. cal ly contained in the tank(for example,water)are not likely to cause contamination. I 5.4 Exercise of re—The preparer conducting the transaction screen process 5.63 If either the guide to the question or other information obtained during the should use good faith efforts in determining answers to the questions set forth in the transaction screen process does not permit a user to conclude no further inquiry is transaction screen questionnaire. The user should take time and care to check appropriate with respect to such question, then the user must determine, in the whatever records are in the user's possessicr.. The preparer should ask all persons exercise of the user's reasonable business judgment, based upon the totality of I to whom questions are directed to give answers to the best ffi t of the respondent's unresolved affirmative answers or answers of unknown received during the transac- knowledge. As required by Section 9601(35)(B)of CERCLA,the user or preparer Lion screen process,whether further inquiry may be limited to those specific issues should discuss with a responsible person in authority in the user's organization(if identified as of concern or should proceed with a full Phase I Environmental Site any)any specialized knowledge or experience relating to hazardous substances on Assessment. the property and the preparer should understand such information. 5.5 Knowledge—The owner or occupant of the roe to which 5.7 Presumption—A presumption exists that further inquiry is necessary if an P property rry portions of affirmative answer is given to a question or because the answer was unknown or no the transaction screen questionnaire are directed should have sufficient knowledge response was given. In rebutting this presumption, the user should evaluate and experience with respect to the property or in the owner's oroccupant's particular information obtained from each component of the transaction screen process and business to understand the purpose and use of the transaction screen questionnaire. consider whether sufficient information has been obtained to conclude that no further IAll answers should be given to the best of the owner's or occupant's actual inquiry is necessary. The user must determine, in the exercise of the user's knowledge, reasonable business judgment,the scope of such further inquiry:whether to proceed with a 5.5.1 While the person conducting the transaction screen process has an E 1527 o Phase l lesser inquiry ndrlm Environmental Sire atsspecific issues rairsed by the questionnaire.Practice obligation to ask the questions set forth in the transaction screen questionnaire,in Imany instances the parties to whom the questions are addressed will have no 5.8 Further Inquiry Under Practice E/527—Uponcompleting the transaction obligation to answer them. The user is only required to obtain information to the screen questionnaire, if the user concludes that a Phase I Environmental Site extent it is reasonably ascertainable. Assessment is needed,the user should proceed with such inquiry with the advice and under- 5.5.2 If the guidance of an environmental professional. Such further inquiry should be under- preparer asks the questions set forth in the transaction screen . taken in accordance with Practice 5 1527. Iquestionnaire,but does not receive any response or receives partial responses,the questions will be deemed to have been answered provided the questions have been 5.9 Signature—The user and the preparer of the transaction screen question- asked,or were attempted to be asked,in person or by telephone and written records noire must complete and sign the questionnaire as provided at the end of the have been kept of the person to whom the questions were addressed and their questionnaire. I REPRINTED WITH THE PERM1SSFON DF-ASTM ' I6. Transaction Screen Questionnaire occupant is any occupant using a least 40%of the leasable area of the property or 6.1 Persons to Be Questioned--The following any tenant when the property is a shopping center. In a multifamily property the current owner of the roe gg11estions should be asked of(1) containing both residential and commercial uses,the preparer does not need to ask I P P property.(2)any major occupant of the property or,if the questions of the residential occupants. The preparer Property.does J) addition m to the r ccun o neraea t 10%of the occupanu of the answer all questions to the but of the responenttual knowledge and in person any occupant likely to be using, treating, generating. s identified is(2), faith When completing the ties virlt column,the preparershould be sure to observe anyaoccup rat l ikely ac petroleum produc on gmstthe o disposing ing of the properly and any buildings and other structures on the property. The guide property. l provides further details on the appropriate use of this questionnaire. IDescription of Site: Address: - I Question Owner[ Occupants Observed During Cif applicable) Site Visit Ila.Is the property used for an industrial use? Yes No link Yes No Unk Yes No - lb.is any adjoining property used for an industrial use? Yes No nk Yes No Unk Yes No 2a.Did you observe evidence or do an ou have Y Y prior knowledge that the Yes 1 Io) Unk Yes No link Yes No I property has been used for an industrial use in the past? • 2b.Did you observe evidence or do you have any prior knowledge that any Yes No Unk., Yes No Unk Yes No adjoining property has been used for an industrial use in the past? . I3a. Is the property used as a gasoline station, motor repair facility, Yes 46 Unk commercial printing facility,dry cleaners,photo developing laboratory, Yes No Unk Yes No junkyard or landfill,or as a waste treatment,storage,disposal,processing. or recycling facility(if applicable,identify which)? I 3b. Is any adjoining property used as a gasoline station, motor repair 115, No link facility,commercial printing facility,dry cleaners,photo developing labo- Yes No Unk Yes No ratory,junkyard or landfill, or as a waste treatment, storage, disposal, processing,or recycling facility(if applicable,identify which)? 4a.Did you observe evidence or do you have any prior knowledge that the Yes No Unk property has been used as a gasoline station,motor repair facility,commer- Yes No Unk Yes No cial printing facility,dry cleaners,photo developing laboratory,junkyard Ior landfill, or as a waste treatment, storage, disposal, processing, or recycling facility(if applicable,identify which)? 4b.Did you observe evidence or do you have any prior knowledge that any Yes No Unk Iadjoining property has been used as a gasoline station,motor repair facility, Yes No link Yes No commercial printing facility,dry cleaners,photo developing laboratory, junkyard or landfill,or as a waste treatment,storage,disposal,processing, or recycling facility(if applicable,identify which)? I5a.Are there currently any damaged or discarded automotive or industrial Yes Yes No Unit link Yes No batteries,pesticides,paints,or other chemicals in individual containers of >5 gal(19 L)in volume or 50 gal(190 L)in the aggregate,stored on or used at the property or at the facility? , 5b.Did you observe evidence or do you have any prior knowledge that there Yes No.)' Unk have been previously any damaged or discarded automotive or industrial Yes No Unk Yes No batteries,or pesticides,paints,or other chemicals in individual containers of gal(19 L)in volume or 50 gal(190 L)in the aggregate,stored on or Iused at the property or at the facility? 6a.Are there currently any industrial drums(typically 55 gal(208 L))or Yes No Unk Yes No Unk - Yes No sacks of chemicals located on the property or at the facility? I 6b.Did you observe evidence or do you have any prior knowledge that there Yes ''-057 Link have been previously any industrial drums(typically Yes No Unk Yes No 55 gal(208 L))or sacks of chemicals located on the property or at the facility? _ - . I7a.Did you observe evidence or do you have any prior knowledge thatfll Yes o • Unk Yes No Unk Yes No dirt has been brought onto the property that originated from a contaminated site? 'Unk 'rake..'or'so ' . Copyright C rs+6 AMERICAN SOCIETY roes TESTING AND MATERIAL,.wet Thu document iu aa as of E 152246:Standard Promos tar Environmental Se.Aa esunto a Tranatato.Screen Prom s& (a under the' sod is die is due.,e,ponnbility o(Sre ommisee E 50.02 an Came,eul Real Emus Transaction'.Thu qu aaarm remnant t only Seeuon.3 and 6 of Prmeocs�E 15%red should ea be cansend u being Environmental eom�l�standatd k necessary to rater to do 1.0 sanded prior to amen tW queeenciessaa Par don aampd.o ssedu4 ar o order nddioosi ewer of deia q, .00„sei,a mesa A TNI Cuwomer Somme at(610)&3241M Question Owner Occupants Observed During I (if applicable) Site Visit 7b.Did you observe evidence or do you have any prior knowledge that fill Yes No link Yes , No link Yes No Idirt has been brought onto the property that is of an unknown origin? - 8a.Are there currently any pits,ponds,or lagoons located on the property Yes No link Yes No link Yes No in connection with waste treatment or waste disposal? I 8b.Did you observe evidence or do you have any prior knowledge that there Yes No Unk Yes No Unk Yes No have been previously,any pits,ponds,or lagoons located on the property in connection with waste treatment or waste disposal? 9a.Is there currently any stained soil on the property? Yes No Unk Yes No Unk Yes No 9b.Did you observe evidence or do you have any prior knowledge that there Yes .7--No ' Unk Yes No Unk Yes No has been previously,any stained soil on the property? I10a.Are there currently any registered or unregistered storage tanks(above Yes No link No link Yes No or underground)located on the property? 10b.Did you observe evidence or do you have any prior knowledge that Yes No Unk Yes No Unk Yes No Ithere have been previously,any registered or unregistered storage tanks (above or underground)located on the property? 11 a.Are there currently any vent pipes,fill pipes,or access ways indicating Yes `No Unk Yes No Unk Yes No I a fill pipe protruding from the ground on the property or adjacent to any structure located on the property? 1 lb. Did you observe evidence or do you have any prior knowledge that Yes No Unk Yes No Unk Yes No there have been previously, any vent pipes, fill pipes, or access ways Iindicating a fill pipe protruding from the ground on the property or adjacent to any structure located on the property? 12a. Are there currently any flooring,drains,or walls located within the Yes a Unk Yes No Unk Yes No Ifacility that are stained by substances other than water or are emitting foul odors? 12b. Did you observe evidence or do you have any prior knowledge that Yes No Unk Yes No Unk Yes No there have been previously any flooring,drains,or walls within the facility Ithat were stained by substances other than water or were emitting foul odors? 13a.If the property is served by a private well or non-public water system, Yes • link Yes No link Yes No Iis there evidence or do you have prior knowledge that contaminants have - been identified in the well or system that exceed guidelines applicable to the water system? I13b.If the property is served by a private well or non-public water system, Yes o Unk Yes No link Yes No is there evidence or do you have prior knowledge that the well has been designated as contaminated by any government environmental/health agency? . I14. Does the owner or occupant of the property have any knowledge of Yes No Unk Yes No link environmental liens or governmental notification relating to past or recur- rent violations of environmental laws with respect to the property or any facility located on the property? I1Sa.Has the owner or occupant of the property been informed of the past Yes No Unk Yes No link existence of hazardous substances or petroleum products with respect to the property or any facility located on the property? . ' 15b.Has the owner or occupant of the property been informed of the current Yes link Yes No link existence of hazardous substances or petroleum products with respect to the J property or any facility located on the property? • I1Sc.Has the owner or occupant of the property been informed of the past Yes i 9 Unk Yes No link existence of environmental violations with respect to the property or any facility located on the property? �� 15d.Has the owner or occupant of the property been informed of the current Yes (No )Unk Yes No Unk Iexistence of environmental violations with respect to the property or any `-� facility located on the property? 16.Does the owner or occupant of the property have any knowledge of any Yes No Unk Yes No Unk environmental site assessment of the property or facility that indicated the presence of hazardous substances or petroleum products on,or contamina- tion of,the property or recommended further assessment of the property? • Ca►lrtdtt 0 19.6 AMR2uCAN SOCIETY FOR TRST41C AND MATERIALS,Wet Cn.afo•.dt.,PA I direct dummies is an=ems of t{IS2i96:Slandud Pnaioe rat&wily aul Sir Amassment':Tnraoiw SOIXII Pmtso..Aidi its minder the ja ndicoos of ASTM r„a*lame&30 oe EO.uonmenul Auetmas sad is the 1OP°r+b.b y of Sahcraione C50.02 oe Comatemml Real Star Ttw.ctioe,.Thu s etw..ane teams my Sections 3 aid 6 of Passe 6 1S.r-96 and should sot be consulted u bang the complete standard.II is mower/r tier ie v Ml standard prior m vat thin q.etianaai.Pat the comp=nendasd.of et enter dditlon.t sepia of dm asratiomuito coma AST!"csetma'Scram r(61011.32-9311.1. •1 I . - Question Owner Occupants Observed During (it appUwble) Site Visit 17.Does the owner or occupant of the property know of any past,threat- Yes No Unk Yes No Unk I ened, or pending lawsuits or administrative proceedings concerning a - release oc threatened release of any hazardous substance or petroleum produce involving the property by any owner or occupant of the property? other8a.Dthan oes the stor pm ropwateerty r discharge into a storm waste waterwater ,on sewer or system?adjacent to the property, Yes (Na) Unk Yes No Unk _ Yes No Ii , 186. Does the property discharge waste water, on or adjacent to the Yes No Unk Yes No Unk Yes No property, other than storm water,into a sanitary sewer system? 19.Did you observe evidence or do you have any prior knowledge that any Yes No Unk hazardous substances or petroleum products,unidentified waste materials, Yes No Unk Yes No tires.automotive or industri al batteries,or any other waste materials have ����n� ���/L�� n dumped above grade,buried and/or burned on the property? sauC /fit 20.Is there a transformer,capacitor,or any hydraulic equipment for which /Yes �N l' riikGN Yes No Unk Yes No there are any records indicating the presence of PCBs? Government Records/Historical Sources Inquiry (See guide,Section 10 of ASTM Practice E 1528-96) 21. Do any of the following Federal government record systems list the property or any property within the circumference of the area noted below: INational Priorities List(NPL)—within 1.0 mile(1.6 km)? Yes _ CERCLIS List—within 0.5 mile(0.8 kin)? Yes No IRCRA CORRACTS Facilities—within 1.0 mile(1.6 Ian)? Yes No RCRA non-CORRACTS TSD Facilities—within 1.5 mile(0.8 km)? Yes No I22. within the circumference of the area noted below: List maintained by state environmental agency of hazardous waste sites ' identified for investigation or remediation that is the state agency equivalent to NPL—within approximately 1.0 mile(1.6 Ian)? Yes No List maintained by state environmental agency of sites identified for investigation or remediation that is the state equivalent to CERCLIS I within 0.5 mile(0.8 km)? Yes No Leaking Underground Storage Tank(LUST)List—within 0.5 mile(0.8 lan)? Yes No 1 Solid Waste/Landfill Facilities—within 0.5 mile(0.8 km)? •23. Based upon a review of fire insurance maps or consultation with the local fire department Yes No serving the property, all as specified in the guide,are any buildings or other improvements on the property or on an adjoining property identified as having been used for an industrial use or uses likely to lead to contamination of the property? • Yes No N/A I t • ... • ... • ICopyright O 1996 AMERICAN SOCIETY roR TESTING AND MATERIALS,Won r . Tha document u in escape of E 132496:SurdYd Ptaetice for Enwonmeaul Site AsseumaurC T s Screen Rome.#im is under the din=n ramonsibility al to refer a Subcommittee E 30.02 or Caemaeul Real Elute Toe/actions.Thu questionnaire represent'only Savors I and 6 of Practice a In}.%steed'hand is ee co at Environmental Aeaep®eee standard. 1 u aYdud prior to, the Vueruanaie. For the=s h:u doom sal be unsorted as 63246 the tsmpla4 n4ndYd. to p rWdYd.or b ceder sddttional copes of the Qtr+darartq taauct ASiT1 Comma'Service as(610)102-9383. • I . The preparer of the transaction screen questionnaire must complete and sign the following statement. (For definition of preparer and user,see 5.3 or 3.3.25 of ASTM Practice E 1528-96.) IThis questionnaire was completed by: Name 7M lei FL re 1 Title _CO/4/ Of- C 1, iTe'- Firm • IAddress S SC) 4-,ec# /Yew ,e/ C4/&0>,4 4) pv 5 5-27/7 IPhone number 7/..� .1 q,C— 4� 7/ Date ��/G a_C 'ff 1 IIf the preparer is different than the user, complete the following: Name of user 1 User's address IUsers phone number Preparer's relationship to site IPreparer's relationship to user (for example, principal,employee, agent, consultant) ICopies of the completed questionnaire have Copies of the completed questionnaire have been filed at: . been mailed or delivered to: - • 1 • I Preparer represents that to the best of the preparer's knowledge the above statements and facts are true and correct and to the best of the preparer's actual knowledge, no material facts have been suppressed or misstated. I l-- Signature /-,6'''L-' / � : c.o--" Date 4/ C 7 l 'Signature Date 'Signature Date Copyright 0 19%AMERICAN SOCIETY FOR TESTING AND MATERIALS,West Conshohocken,PA Thu document is an excerpt of E 1526•96:Sundud Practice for Enwwwanul Sc h Aueumenu:Tn+urvm Scrum Proceu..hich it under dhe jar dicum of AVM Committee E-50 on Environmental Aueument ads the direct respotiibdi y of Subcommittee E 50.02 on Commacial Real Estate Trwactions.This gtteationnaire tepresenu only Sections S and 6 of Practice E 1526.96 and should not be construed at being the complete standard It necessary to tda to the fdl nandard prior to using Chia questionnaire.For ate complete standard or to order additional copier of this questionnaire.con=ASTM Cunoma Service at(610)1324M. 1 ti GR1 i I . I 1 I 1 I 1 1 1 I . To order additional copies of this questionnaire, contact ASTM Customer Service. 1 phone: (610) 832-9585 fax: (610) 832-9555 Ie-mail: service@astm.org 1 (IGTO 100 Barr Harbor Drive West Conshohocken, PA 19428-2959 To the best of our knowledge,y knowledge, please summarize the history, ownership, ' and land use of the Property. s. / r /- i 1 1 1 1 1 Please explain any "Yes" responses to the questions. 1 1 1 1 1 1 1 GME CONSULTANTS.INC. I APPENDIX D PROPERTY RECONNAISSANCE PHOTOGRAPHS I I I I I I I I I I 1 I I GME CONSULTANTS , INC. IPHOTOGRAPHIC RECORD I CLIENT: Senior Housing Partners GME PROJECT NO. : 7735-A LOCATION: Senior Housing Addition Oak Park Heights, Minnesota s r r�x# ^,.� '� i ar 8af r s: �3 �t �. ^�. '? € s � , . , � � Rt Photograph No. j , "' z Date: May 19, 1999 Comments : `.' 4fi View of central portion of Property, looking east . Active grading for I .n Y. s "� h w ‘'" --_ ' 58 - Avenue North. r IItit a a + ?► '•� ~.ws.` ee�, a.` "y�"G'�'*'-a,'{ a " `+�'4 1 '1, ,.+��j Photograph No. : 2 iNt " 4r Date: May 19, 1999 No, Comments: ■I ; , �� �. ,r�.•~( ��,�;, View of wetland area on 41:14...... jF ��: :� �,' north-central portion of I ]-� � "� r �,= �4..' Property followed by < All y���, �-� grading for 58th Avenue I `�` '. 't` North looking �� i �. �_�; southwest . .. r . , ( +e•, ' T�! 'iii .... j'. I r., 4 I I GME CONSULTANTS, INC . IPHOTOGRAPHIC RECORD I CLIENT: Senior Housing Partners GME PROJECT NO. : 7735-A LOCATION: Senior Housing Addition Oak Park Heights, Minnesota ...: Photograph No. : 3 °'err Date: May 19, 1999 A Comments : Fill soil pile located kla. west of garage . L� : n,a 1-_jr.:,,,. - t F '4,. •Y ` 2 r �'t r. .c J .. S r, f 1 s,. ,.::;;,...,.'11 ' ri-� .-, a 4-'»'•.1 t r ` Ir 7. ,.. u .4',-17-41 ait1�"� k,{- 4 !` �. �... _ w* oaf o-y y . I • _ �+` t . . Photograph No. :. . 4 h - M _ <: ,_ Date: May 19, 1999 kn' �► �Y t ,s,, , Comments:• �t�- ? s Tank converted to burn ` � _ •_. �,g °1 4.— � hk barrel located in 4,., .' .� _ j•y-,. ;';' �►1'„ vehicle yard, west of ! .- !^ t garage . I 4. r '4 pi`x '4 ..„fit• _.''` -44 .: II , t e�' ., �., / -� "i v 6 ' / . >>Y ,.-a j y / P-` 24 4-".�2 ,It w• ,/ ';11),'V,'. f\, "le``. e 'is124�-- '11' � )• i F ` SKr. ;, ._ ....,;.,* \,-'., .A � � ^'44itir-..-frr,r �' 9 44 R 'M - .�.r ' r t °" y r , - - I I 1 I GME CONSULTANTS , INC . IPHOTOGRAPHIC RECORD IICLIENT: Senior Housing Partners GME PROJECT NO. : 7735-A LOCATION: Senior Housing Addition Oak Park Heights, Minnesota Wit . ' \-;tom 1, - -., 1 6 A-P rte. t.� rte,. ,,;-`=��.j p-..4:- t Y ( p A '� t er ~R 1 s • 4 ,. <.; Photograph No. . 5 :j . �:,'"r,, . e.=y,, _� * Date: May 19, 1999 a, 4 ��: -- , Comments .'� :" , . Partially buried wood I �_ ,• = 1,-"....r4,,'*- --:.. r 9 �`It` ,r �,. jam ' and household waste a `' ° located south of brush a. - " \�� pile and north of ,.• 't. �' �,. r, ... r =..ter � i grading for 58Th Avenue t `� :. __=,-'� ': !- North. Y i 4 0 _.11C40. I � ),,4 i . x,= '^`' ` "-" F r7,'' fi Photograph No. . 6• r -.� �, W },,, ".K'` ;e` • r Date. May 19, 1999 F ey . fiti7 TiS yr o ^ r r. Comments. ',o-"�y f P. "«� .ry 8 :t .Y h,, 'J 4 l._ r.#+'" Z `�-�`y .- , 'r�, z,. ~�' a iv; I III GME CONSULTANTS , INC . 1 PHOTOGRAPHIC RECORD I CLIENT: Senior Housing Partners GME PROJECT NO. : 7735-A LOCATION: Senior Housing Addition Oak Park Heights, Minnesota V. -� .r, i . �i * ' - Photograph No. : 7 h �i"/ r: :4• Y i+a I g Date: May$ 19, 1999 ,, ' ;�s '''— Comments : �A .� f�f ,.Y� '� x q Garage located on the I �' >„ eastern portion of f � ' ` Property, view to * f' p y -_ " southwest I _ . y: I _ S ,�S'1`9 Photograph No. : 8 Date: May 19, 1999 ,t: n.T. -r:r— Comments: Tractor and landscaping !, [ -"%a. equipment located within I the non-enclosed & • portions of garage structure. ` .ae n o of ® I! (a A 16. ,- ._,.... , ,,.„. . ,.: 0 :r., ...._ .14_4.,...,,,:,_..,,f; ., , ,wa,� � r a Ili i, � ' - r r t:'1".',/•I . II' II II - , / 1 'ty ° i r e: ' X1_ ' I .u.�. I I I I GME CONSULTANTS , INC. IPHOTOGRAPHIC RECORD I CLIENT: Senior Housing Partners GME PROJECT NO. : 7735-A LOCATION: Senior Housing Addition Oak Park Heights, Minnesota I ' �. ,, a . lltr n Photograph No. : n _ s, - <,..,., Date: May 19, 9 Y 1999 -.-..x F n Comments I _ -t - _, Gasoline cans in • enclosed space of garage CiK 3=`{ I4.:, s `� structure . a ,-- , , . ,,......., # ....--- , i-^",...:"'le,:...A:,,,..1.___T ......1.r.....,", v.:.: i ..... 1 vri - ' Photograph No. : 10 IDate: May 19, 1999 „4,i, -� a �y , ,r Comments: y-� Refuse and debris • "),,,ii 4 located on floor of t . r , i,• ,,„ • mot, ,' '* garage structure . ,� K'1 r + ! ` ' , '\-- k ; ,,,. _,...„.._ '""r'tir:. i'., - err J f .7R n I I I III GME CONSULTANTS , INC . IIPHOTOGRAPHIC RECORD CLIENT: Senior Housing Partners GME PROJECT NO. : 7735-A I LOCATION: Senior Housing Addition Oak Park Heights, Minnesota 1! : ...?...ity ,_„ :14. -..:,-.. -- , :'Mir: y �" 5,a�� ' Photograph No. : 11 .s� 4a -- � -5" -'\ '3.' _ Date: May 19, 1999 l �. - 4 ,.4. "..., .« ' Comments : 1 1 �� ,, ,� `'-; Fuel Oil AST located on•�y__� 4 �1, the west side of garage -- "( `�) ,�"�1..' (, `._ �, structure. 4 . F a _ J r+� .,c,� �� i� Or-4 '/ , •-.""•••---44. ' !\, , ii . . • -• -1/ Photograph No. : 12 I �• Date: May 19, 1999 • Comments: �' d, �e - , � t Appliances, wire, va. 1, 1, t. .. , ' ,,� , ,,',.'i.1'4.1;-.'s' ',�° er, and other d7 �' 't" r ,f debris located on south �► t � " ' 1° 1 l ' ' side of former• r greenhouse wall . e I J, y'"'4*4 - ' -_iG : r^ .15t r l I 'y r1 , ' r �'� �`,� +! tr A 14 �,t, ; I ,� w'� .der ,,, �.� q' ! -.• 1( ( ', r r. ike, [ ,,�''^ i i0, pl+ ,- "� 76 `,7 �-4-•..tom ,•': j - '+�-mow; •may I .t 1 I 1 I i 1 APPENDIX B PHASE II ESA REPORT OF AUGUST 9, 1999 I I I I I I I I I I I ti OPY 11 I PHASE II ENVIRONMENTAL SITE ASSESSMENT REPORT PROPOSED SENIOR HOUSING ADDITION 58TH AVENUE NORTH AND OAK GREEN AVENUE NORTH OAK PARK HEIGHTS, MINNESOTA GME PROJECT NO. 7735-C August 9, 1999. 1 I I I/ Prepared for: Mr. Greg Collatz Senior Housing Partners 2345 Roy Street, Suite 240 St. Paul, Minnesota 55113 11 I Copyright, 1999 - GME Consultants, Inc. 11 1 1 II I IAugust 9, 1999 1 Mr. Greg Collatz Senior Housing Partners II 2345 Roy Street, Suite 240 St . Paul, Minnesota 55113 GME Project No. 7735-C RE : Phase II Environmental Site Assessment (ESA) Report for the I proposed Senior Housing Addition Property located at 58th Avenue North and Oak Green Avenue North in Oak Park Heights, Minnesota II Dear Mr. Collatz : II In accordance with your authorization on June 11, 1999, we have completed our services for this project . The purposes of this report are to summarize and interpret the results of the field and laboratory work. IIWe appreciate this opportunity to be of service to you. If you have questions regarding this report, please contact us . II Sincerely, GME CONSULTANTS, INC. I/ 44 II Eric P. . ,• es Timothy F. McGlennen Envir e al Scientist Senior Environmental Scientist Proj ct,,, -nager Property Development Assistance IGroup Manager EPS :rma II C:\EPS\7735-C.ESA I I I I TABLE OF CONTENTS PHASE II ENVIRONMENTAL SITE ASSESSMENT REPORT PROPOSED SENIOR HOUSING ADDITION 58TH AVENUE NORTH AND OAK GREEN AVENUE NORTH OAK PARK HEIGHTS, MINNESOTA ' GME PROJECT NO. 7735-C ' SECTION PAGE I . INTRODUCTION 1 A. Background Information 1 B. Purpose and Scope 2 II . SITE LOCATION 3 III . EXPLORATION PROCEDURES 3 A. Environmental Test Pits 3 B. Soil Organic Vapor Measurements 5 C. Laboratory Analyses 5 IV. EXPLORATION RESULTS 6 A. Geology and Groundwater Levels 6 B. Soil Organic Vapor Measurements 7 C. Test Pit Observations 7 1 . Concrete Vessel 7 2 . Parking Yard (East of Garage) 8 3 . Office/Coal Storage Basement 8 4 . Fuel Oil AST 9 5 . Surficial Debris Piles 9 D. Soil Chemistry 10 E. Liquid Chemistry Results 12 ' F. Non-Environmental Issues 12 V. DISCUSSION AND CONCLUSIONS 12 IVI . RECOMMENDATIONS 14 VII . GENERAL QUALIFICATIONS 15 APPENDIX FIGURES Figure 1 : Regional Location Diagram Figure 2 : Test Pit Location Map ' TABLES Table 1 : Soil & Liquid Chemistry Results (DRO, GRO, VOCs) Table 2 : Soil Chemistry Results (Metals & PAHs) APPENDICES EnChem Laboratory Report MVTL Chem Laboratory Report I. INTRODUCTION A. Background Information On May 28, 1999, we completed a Phase I Environmental Site Assessment (ESA) report for the site which revealed potential recognized environmental conditions (RECs) associated with the Property. The site is planned to be developed for senior housing. The approximate 16 acre Property is located in a rural and more recently residential area. Since the 1930' s, a wood-framed garage and a greenhouse have occupied the Property; only one wall of the greenhouse remains . The garage is still used for equipment and ' vehicle maintenance and storage . We also observed solid waste/ debris disposed on the ground surface, scattered in different areas around the buildings . ' The RECs identified in our Phase I ESA report included the ' presence of a tank or dry well south of the garage which reportedly was formerly connected to the basement of the greenhouse office; the presence of a 265-gallon fuel oil aboveground storage tank (AST) without secondary containment next ' to the garage that was used as a fuel source for the heater inside ' the building; the continued activity of vehicle maintenance since the 1930 ' s during which petroleum products and automotive fluids may have been handled and possibly could have been spilled onto the ground surface in and around the garage; the presence of solid waste/debris piles across the site; and, the former presence of a I 1 ' Mr. Greg Collatz 2 August 9, 1999 GME Project No. 7735-C coal-fired heating system. The owner indicated that the coal was ' stored in the basement of a former building adjoining the greenhouse . I IIThe off-site RECs identified in the Phase I ESA included the presence of the Bay Town Township chlorinated solvents 9 roundwater plume to the south and the presence of a salvage yard on the adjacent property to the north. You decided not to assess these ' off-site RECs . B. Purpose and Scope The purpose of this Phase II ESA was to assess for the possible presence of subsurface impacts from petroleum hydrocarbons, metals, volatile organic compounds (VOCs) , and polynuclear aromatic hydrocarbons (PAHs) on the Property. ' The scope of this s project was based on our May 28, 1999 proposal . ' It included conducting test pits on the site, collecting soil samples for field monitoring and laboratory analysis, and ' preparing this report . You authorized us to roceed with this p project on June 28, 1999 . i Mr. Greg Collatz 3 August 9, 1999 GME Project No. 7735-C II . SITE LOCATION The Property is defined as the approximately 16 acre parcel of land located in the southwest quadrant of Oak Green Avenue North and the newly constructed 58th Avenue North in the City of Oak Park Heights, Washington County, Minnesota. The Property' s legal description is "the north one-half of the southeast quarter of the northeast quarter of Section 5, Township 29 North, Range 20 West, ' except the north 100 feet of the east 200 feet, and except the north 218 feet of the south 400 feet of the east 200 feet thereof, Washington County, State of Minnesota, subject to public roads . " ' A Regional Location Diagram is presented as Figure 1 and a Property Diagram is presented as Figure 2 . i III. EXPLORATION PROCEDURES A. Environmental Test Pits 11 On July 2 , 1999, an excavator that you contracted excavated 16 test pits at the site with a backhoe. The test pit locations were 1 selected by our Senior Environmental Scientist, based on the 1 potential RECs identified in our Phase I ESA report and on our discussions with you. The final locations, as shown on Figure 2, ' were determined in the field based on site logistics such as utility locations, buildings, and property lines . 1 I �5 Mr. Greg Collatz 4 August 9, 1999 GME Project No. 7735-C Underground utilities were cleared by Gopher State One Call prior to excavating. We observed the exposed soil profiles for obvious visual or olfactory evidence of petroleum impacts . The depths of the test pits ranged from 1 to 10 feet . The test pits were completed in five distinct areas, as discussed in the proposal and highlighted below. • The first area included the dry well/tank (concrete vessel) on the south side of the 1 garage. • The second area included next to the 265- , gallon fuel oil AST and below the aboveground piping. • The third area included the gravel drive on the east side of the garage to assess for possible petroleum spills . • The fourth area included the five larger piles of concentrated solid waste/debris . • The fifth area included near the former office/coal storage basement . 11 t Mr. Greg Collatz 5 August 9, 1999 GME Project No. 7735-C • We collected one composite soil sample from the earthen floor of the former greenhouse to analyze for agricultural chemicals . I After the test pits were completed, they were located on a site ' map, backfilled with the excavated soil, and compacted by the ' backhoe . Descriptions of the test pits, including our organic vapor measurements, soil classifications, and field observations, are included in Section 4C. B. Soil Organic Vapor Measurements Soil samples collected from each test pit were monitored on-site P P by our Environmental Scientist using an HNU Model PI-101 (HNU) photoionization detector (PID) fitted with an 11 . 7 eV lamp. The ' HNU measures certain organic vapors in parts per million (ppm) range . Headspace analyses were conducted in general accordance with Minnesota Pollution Control Agency (MPCA) guidance documents . C. Laboratory Analyses I The soil samples and one liquid sample were submitted to EnChem and Minnesota Valley Testing Laboratories . The selected samples ' were collected in laboratory-provided jars and placed in a cooler with ice under chain-of-custody procedures . I IMr. Greg Collatz 6 August 9, 1999 GME Project No. 7735-C IINo soil samples were collected near the concrete vessel on the Isouth side of the garage. However, we did collect a liquid sample from the concrete vessel for analysis of gasoline range organics I (GRO) , diesel range organics (DRO) , VOCs and Minnesota Department of Agriculture (MDA) List 1 base/neutral pesticides . II IThe soil sample collected from beneath the 265-gallon fuel oil AST was analyzed for DRO. The soil samples from the test pits on the Ieast side of the garage were analyzed for DRO, GRO, and VOCs . The soil samples from the test pits beneath the larger piles of Iconcentrated solid waste/debris were analyzed for DRO, GRO, and IIVOCs . The soil samples from the test pits near the former office/coal storage basement were analyzed for the eight RCRA Imetals and PAHs . The composite soil sample from the earthen floor of the former greenhouse was analyzed for List 1 base/neutral Ipesticides . A soil trip blank was submitted for VOC analysis . No IIgroundwater samples were collected, as it was not encountered. IIV. EXPLORATION RESULTS IA. Geology and Groundwater Levels IIThe geology encountered in the test pits generally consisted of Idark brown silty sand in the upper 2 feet overlying a brown silty clay with varying amounts of sand from 2 to 10 feet . I 11 Mr. Greg Collatz 7 August 9, 1999 GME Project No. 7735-C Groundwater was not encountered in the test pits . In our Phase I ESA, we estimated groundwater to be 30 to 60 feet below grade. B. Soil Organic Vapor Measurements The headspace measurements conducted on the soil samples collected from the test pits did not indicate significant elevated organic vapor impacts, except from test pit TP-3 (0 to 2 feet) and in test ' pit TP-13 (0 to 4 feet) ; these PID readings were 4 and 2 ppm, respectively. C. Test Pit Observations Below is a description of our observations of the test pits . 1. Concrete Vessel Test pit TP-1 was excavated on the east side of the vertical pipe P P P ' leading down to the concrete vessel . The pipe appeared to be PVC. The top of this vessel was approximately 6 feet below grade. The test pit was excavated an additional 4 feet, where it appeared to ' be the base of the concrete vessel . We did not observe obvious staining or odors in the soil samples collected from this test ' pit . We also did not observe a pipe that was reportedly connected to this vessel from the office/coal storage basement located to rthe east . I r IMr. Greg Collatz 8 August 9, 1999 GME Project No. 7735-C II2 . Parking Yard (East of Garage) II Test pits TP-2 , TP-3 , TP-4 , TP-5, TP-6 and TP-7 were excavated to Ian average depth of about 5 feet . All of these test pits had asphalt and some darker fill material in the upper 1-1/2 feet, Iwhich was underlain by native silty sands and silty clays .s . Test Ipits TP-3 , TP-4 and TP-5 had noticeable staining and low to no PID readings, possibly indicating a weathered heavier petroleum IIproduct (e .g. , perhaps motor oil) . II3 . Office/Coal Storage Basement II Test pits TP-8 and TP-9 were excavated to 8 and 7 feet, IIrespectively. In test pit TP-8, 4 feet of darker fill which contained some concrete pieces was excavated, which was underlain 1 by brown silty sand. Test pit TP-9 consisted of fill with Iconcrete pieces, wood debris, miscellaneous garbage (e.g. , plastic) , and several small pieces of coal . A concrete footing IIwhich was likely from the office/coal storage basement was encountered at about 7 feet below grade; we did not observe Iobvious staining or odors in these fill soils . I II I I t Mr. Greg Collatz 9 August 9, 1999 9 , GME Project No. 7735-C 4 . Fuel Oil AST Test pit TP-10 was excavated adjacent to the fuel oil AST. We did 1 not observe obvious staining or odors, or record elevated PID readings . 5 . Surficial Debris Piles ' In test pits TP-11, TP-12 , TP-15 and TP-16, the surficial debris, which generally consisted of asphalt, brush, rock, concrete and Iwood, was removed and no obvious staining or odors were noted or observed in the native soil beneath this debris . Test pit TP-13 , located in the central portion of the large brush pile west of the garage, had gray-stained soil from 0 to 4 feet . These soils had slightly elevated PID readings . At 4 to 6 feet, we encountered what appeared to be native reddish-brown sand with silt with no obvious stained soil or odors . 1 Test pit TP-14 located adjacent to the burn barrel consisted of ' fill with red chimney brick and one heating duct buried to about 4 feet below grade . No obvious stained soil or odors were noted in or beneath this fill in the native soil to 6 feet . I 1 I tMr. Greg Collatz 10 August 9, 1999 GME Project No. 7735-C D. Soil Chemistry I In test pits TP-2 through TP-7 located on the east side of the 11 garage, DRO was detected in test pit TP-3 (0 to 2 feet) and test pit TP-5 (0 to 2 feet) at 16 ppm and 5 . 6 ppm, respectively (Table 1) . In the deeper soil sample from test pit TP-3 and the shallow soil samples from test pits TP-2, TP-3 , TP-6 and TP-7, there were no detections of the analyzed parameters except for acetone; this acetone detection is likely attributable to laboratory contamination as it is commonly used in the laboratory environment . 11 In test pit TP-9 (4 to 6 feet) located near the former office/coal storage basement, the levels of the eight RCRA metals (arsenic, barium, cadmium, chromium, lead, mercury, selenium, and silver) ■ were either below detection limits or below the MPCA soil reference values (SRVs) . In the PAH analysis, all detected constituents were below their respective SRVs (Table 2) . SRVs are typically the most conservative action levels used by the MPCA for a residential i site . In test pit TP-10 located near the fuel oil AST, DRO was detected at 4 . 9 ppm, which is slightly above the laboratory limit of 11 detection. r tMr. Greg Collatz 11 August 9, 1999 GME Project No. 7735-C In test - st pit TP 12 located underneath the debris pile on the western portion of the study area and test pit TP-14 located adjacent to the burn barrel, there were no detections for the analyzed parameters . We collected two soil samples from test pit TP-13 located on the west side of the garage in the large wood debris pile. In the first soil sample collected from 0 to 4 feet, DRO was detected at 58 ppm with no GRO or VOC detections excluding acetone. In the deeper soil sample from 4 to 6 feet, there were no detections for the same analyzed parameters. In the composite p site soil sample analyzed for MDA List 1 base/neutral pesticides from the earthen floor of the greenhouse, Alachlor (Lasso) was detected at 0 . 13 ppm and Metolachlor (Dual) was detected at 0 . 05 ppm. These levels are below the MDA Preliminary Soil Cleanup Goals using a moderate to low risk to groundwater scenario for these compounds; the goals are 0 . 5 ppm and 1 . 5 ppm, respectively. No other List 1 agricultural compounds were detected in the soil sample . r 1 1 11 1 II IIMr. Greg Collatz 12 August 9, 1999 GME Project No. 7735-C I/ E. Liquid Chemistry Results I 1 II In the liquid sample from the concrete vessel, DRO was detected at 1 490 parts per billion (ppb) . There were no other detections for the other analyzed parameters . II 11 F. Non-Environmental Issues IWhile excavating in the area of the burn barrel, we encountered a significant amount of red chimney brick from the surface to IIapproximately 4 feet . This material appears to be inert; however, IIit (and other debris) will be encountered during site grading. I V. DISCUSSION AND CONCLUSIONS II IIOur Phase I ESA revealed on-site RECs which included the presence of a concrete vessel ; presence of a 265-gallon fuel oil AST; IIpresence of a vehicle maintenance garage; presence of solid waste piles across the site; and, the former presence of a coal-fired 1 heating system. To assess these areas, we excavated test pits Iacross the site to observe soil conditions and to collect samples for field observation and laboratory analysis . II II I I tMr. Greg Collatz 13 August 9, 1999 GME Project No. 7735-C The areas identified with low level petroleum impacts included the gravel drive east of the garage and beneath the large wood debris pile on the west side of the garage . We contacted Mr. Peter Sadjovic, representative of Mr. Greg Collatz, on July 26, 1999, and discussed the results with him and informed him of their possible duty to notify the State per Minnesota Statute 115 . 061, "Duty to Notify and Avoid Water Pollution. " We recommend that you discuss reporting the detections to the MPCA with your legal 11 counsel . Soil vapor readings and analytical data from these test pits suggest that the petroleum impacts are present in the upper 2 feet in the gravel yard east of the garage and in the upper 4 feet in the soils beneath the large wood debris pile west of the garage. The laboratory results and field readings for the other areas either were below detection limits, MPCA SRV levels or MDA preliminary soil clean-up goals, or were within the range of naturally-occurring concentrations in the soil (i .e. , metals) . 11 1 11 I t Mr. Greg Collatz 14 GME Project No. 7735-C August 9, 1999 VI. RECOMMENDATIONS Based on the results of this study, we recommend that the impacted surface soil of the gravel yard east of the garage and the impacted soils beneath the large wood debris pile west of the garage be excavated and disposed of properly. The liquid inside of the concrete vessel should be disposed of properly by a licensed contractor as there were detections of analyzed parameters . r 1 We recommend that you apply to the MPCA Voluntary Petroleum Investigation and Cleanup (VPIC) program to discuss the proposed alternatives to excavating the impacted soil and its disposal or reuse on-site . We recommend that you request issuance of a "Site Closure" letter from the VPIC program and a "No Association" letter regarding the detected impacts on the Property from the Voluntary Investigation and Cleanup (VIC) program, as appropriate. We can assist you with this process . 11 We also recommend that you discuss these issues and our recommendations with your attorney before proceeding. I I I I 11 Mr. Greg Collatz 15 August 9, 1999 GME Project No. 7735-C VII. GENERAL QUALIFICATIONS I The interpretations and conclusions submitted in this report are based on the data produced during this study. This report does inot account for any variations that may occur between or outside ■ of the soil or groundwater sampling locations . The conclusions in this report represent our engineering and hydrogeologic judgement . This report has been prepared in accordance with the local standard of practice for our profession, using the normally available sources of information. No warranty, express or implied, is presented in this report with respect to the environmental conditions on this site. Prepared by: Eric P. St. `iiii . Environ ' dg . Scientist Project wager I Reviewed by: Timothy F. McGlennen Senior Environmental Scientist Property Development Assistance Group Manager t Reviewed by: Mark D. Millsop Principal Hydrogeologist Environmental Division Manager EPS :rma C:\EPS\7735-C.ESA I I/ I I I I FIGURES FIGURE 1 : REGIONAL LOCATION DIAGRAM FIGURE 2 : TEST PIT LOCATION MAP I I I i I l I 1 I 111 1 STILLWATER QUADRANGLE 'i o �`� `° STILLWATER, MINN.—WIS. ii MINNESOTA—WISCONSIN '` -- `\` { `•�e .� Q N4500—W9245/7.5 7.5 MINUTE SERIES (TOPOGRAPHIC) , ,, cam&-.".. -.,. i _ _.I \�®I 1967 i , . V"v U �. ' �s - S� 0/ 4.1- a iS1 PHOTOREVISED 1980 0 (f 1�r Virliprfz :.7:?._-, 4' ;�' a0 ♦ �, I�S \� i x!'11`` ,. o , � � ,� ,� � �� i iii I ® w ��� _- i \ ..1� � 6 iii ��—i..,t,§.r a --. Oil gs. / P *446' 0- ki' •2 '' '1/4-... ■t_ g - '-'91fr eo \‘2 ;if if NA,41,-•-_,' .= 'c2 .,, ...,..4,,, 0 mi \ it====_- Bi �� / )4;1P I ��I\ 1110 Wig t# 1 O 1I� : j y yo . • 1\ �O• �r I -, !Tr- , , , . 90• ^�C f 1 9 ° Q fir` . Og O_�� iti_k/AVArdilikt,4.1<ar: is --"r717e4E -T --. - - - •• • 1• 7,• ' ,H7 4------•-•OL.1-1 -: - -- '� ., PROPERTY f� '. .. 1 `--- �,-' LOCATION : �� -A.---'::- ----.9/.2..r.‘4Ce. e � T g 950 ° . •. •�. 9 (� / C�'�Z1.c u 1::77„,/ 6 I'C1 r o1J � --— - • a i % ,, '31 • ° 9" I � 'o - ____:____= 1 �� O .L , I O of D O . f 1 v y o c re=== O Q C s o tip`.,` f ,, O � � � : o _ - ) 9 4 1 1 _ , r-6,77,11:0 f7..P-, \ ,,,,..:0, ),)Tii I ,d o IL O C�,..t:e �, �' B .'_ . o 0° \:11i..,..,,' 9,p. ( do b, , c ,_,, - . \___4/ k(--;1 1 1 1 i SCALE 1:24 000 1 0 1 MILE 1000 u0 _ 1000 J .000 3000— 4000 5000 6000 7000 FEET // 1 KILOMETER MINN.( CONTOUR INTERVAL 10 FEET NATIONAL GEODETIC VERTICAL DATUM OF 1929 QUADRANGLE LOCATION Figure 1: Regional Location Diagram. GME CONSULTANTS, INC. Senior Housing Addition 14000 21st Avenue North Oak Park Heights, Minnesota Minneapolis, MN 55447' EPS ( TFM IJuly 99 J 7735 -C I ' ■ I OAKGREEN AVENUE N. r___---_- IHOUSE 1 i 1 I HI i 1 1 I I Z I -J 1 i FORMER OFFICE/COAL Ja 0 I I STORAGE BASEMENT 3 1 cc 0 I Z GARAGE I <~/1 1 1 j 1 i W i -..-..--] 1 I = T--8'-' ►�• 1 to I TP-5 TP-7 Co �, 1 �n ® 0 TP 9 TP-15 • TP-6 (SURFICIAL TP-20 ►.• ►S A CONSTRUCTION TP-3 TP-4 I DEBRIS) GARAGE i TP-16® CCONCTP 1 1 'ETE TP-10 VES` L) (AST) TP-14 I (Burn barrel) 1 0 1 ®TP-13 ® TP-11 (Brush pile) (Coast debris)ion m I I 0 I I )-J Q I L` i -Li J TP-12 ® 0 (Buried wood & ? •••••.,....... v7 other debris.) 1 WET LAND 1 I I \ : \ FILL I 1 LEGEND PILES __ PROPERTY i n BOUNDARY i .L.� I TREE LINE �' (APPROXIMATE) APPROXIMATE WETLAND SCALE (APPROXIMATE) I 0 TEST PITS O. FEET IOIO I 7735B.GCD RGURE 2: TEST PIT LOCATION DIAGRAM GME CONSULTANTS. INC. SENIOR HOUSING ADDITION Geotechnical• Materials •Environmental EmirAe OAK PARK FIGHTS. MINNESOTA 21st Avenue N. Msineapolis. Minnesota 55447 ■, (612) 559-1859 Vi_ I EPS I JULY 99 I GME Project No. 7735-B I II II TABLE 2 SOIL CHEMISTRY RESULTS II METALS AND PARS OAK PARK HEIGHTS, MINNESOTA IIGME PROJECT NO. 7735-C IITEST PIT TP-9 (7' ) ANALYTE MPCA SRV VALUE RESULT I/ , 8 RCRA METALS Arsenic 10 1 . 9 I/ Barium 1200 49 Cadmium 35 <0 . 11 Chromium 71 11 IILead 400 18 IIMercury 0 . 7 0 . 035 Selenium 170 <1 . 1 ISilver 170 <0 . 56 II PAHs Benzo (a) pyrene 2 . 0 0 . 066 IIBenzo (b) fluoranthene 2 . 0 0 . 063 II Chrysene NE 0 . 057 Fluoranthene 1080 0 . 100 I/ Pyrene 890 0 . 071 I/ NOTES : All results in mg/kg NE - No SRV established SRV - Soil Reference Value II < - less than detection limits PAH - Polynuclear Aromatic Hydrocarbon I I I I 1 I ' ENCHEM LABORATORY REPORT I I I I r t I 1 I ■ rc): N y g s Q n 1_ a — lam' \ ' / c acco°o'n 3 a I ao N O E x T., o a� C7 �� .a a CC • .Ni O N _, v O .‘N. m „ ¢ v E E Q y � � 3 %� mN a O � � N a °C a Qm d 5 ui ui t Q. .�� c g n . E_ _ _ _ urniaoo o Q ���in dLw2?116' U .ago w ? p ► 0 u' • 1 ts..ON�D Q Q .' .� �.� '^\ �no0o d = �4k ��w • [73 N U d H G a c\I N r•C) 1 k I .x r N Is N c V itil uJ 1/1 .o. II A (P m m t)m m St1 -(:>,: e, I X67 dS'w O y `� N N N N 171 SI kl.1 �� Q . Q Q • z e‹,.. 7C Q I _ Q o hio _ w E E E E F+�1 } °oU ✓7 x t' t�E O ° 3' o"�-0 0 0 z " w ^� '?�- yL f '74 �. 74.- `�� of ,.�^ T (� .).. ..i.. -4 i'' „L..../(.4.= „ ate i� -rjb, • by �- �- -,2- 4L •;L ,c -74 .,� I `, �_ W 54 �y3 C. j at i Q o N L .�L L L 7 cr U Q1 Q 2 Q Q V7 o S Gl ¢ V U ¢ c m o W N C IL.La G r1 H :-' N co rr 1 N h �1�-, ^ �1 o U u1 c16i E c a �, �� GJ cal �,�,�• r 0 H , 0 � Q Ji.i � N J.V L •V 0 67,....., ,g. rn ❑ �.J M £' mlu0 rn � n ,.., , ...T tl) 7 a `o U o Z Z in o a M 1 1 `, t t 1 �� c,. =O r`w m t E c d m d i5 avi E m z O 'LL C,Z.. (a (� �.. Z.S Z c c CC E 2 O O O O !0 m }S1 ���.. Q G V' U m a I°-' a a` a` m b:h l-V a c l' W c Nii g wtin 0 �'� Z E,, I ¢ c a 0 0 _ i-i .. - .c m w. o u N a Q p p 0 t,19 w g n W W'nip ° 22 CC _ te1" M U Q °�..`p' v 0 E E E E('N pp o w , ,.NT p Q ijL' Q \ ... �1 CO CI°":"11. Ire) 4 ca d m N co � � U p 2 O Q c Cpl U. V y 5 M ., h- .......... „c„. � Q��, ti C N 1 g g, A illsoisionion''41114pr . -C,m o ..r 1111 m m � IIIIIIIIIIIIIIIIIIIIIIt w c,w ovensolosion WD x_ o ° °NYS) IIIIIiit13 Z O Z 1- > bib O i eigEIIIIIIIIIIIIIIIIIIr N N .�. �s�d INIEIIIIIIIIIIIIIIIIII w �, d *-4, I iiiiiii ` Q 1131111111111111111111 ONIIII111111111111 \ I A wag : - 10. to y L C k. Q r t II ■ o a ¢c c � Q as R L l0 a x U i';i' i .8 iii a o a V;c x ry ° U c Z z =° m Z U :$ ii m ., id m °m 2 a L °E ' o E 0 z 0 e > >iIIIIIIIIIII ; j Gg S:. ^ zxz> c ■ I ; 1795 Industrial Drive Green Bay,WI 54302 920-469-2436 EHEM 800-7-ENCHEM rrc. FA%: 920-469-8827 I -Analytical Report- Project Name: SENIOR HOUSING ADD. IProject Number: 7735-B Client: GME CONSULTANTS MDH LAB ID: 055-999-334 Collection Collection Sample No. Field ID Date Sample No. Field ID Date I 893755-001 TP-2(0-2') 7/2/99 893755-002 TP-3(0-2') 7/2/99 893755-003 TP-3(4-6') 7/2/99 I893755-004 TP-5(0-2') 7/2/99 893755-005 TP-6(0-2') 7/2/99 893755-006 TP-7(0-2') 7/2/99 I893755-007 TP-9(7') 7/2/99 893755-008 TP-10(2') 7/2/99 I 893755-009 TP-12(6') 7/2/99 893755-010 TP-13(0-4') 7/2/99 893755-011 TP-13(4-6') 7/2/99 I 893755-012 TP-14(6') 7/2/99 893755-013 TB(SOIL) 7/2/99 893755-014 ST-1 7/2/99 I893755-015 TB(WATER) 7/2/99 I I ISoil VOC detects are corrected for the total solids,unless otherwise noted. I certify that the data contained in this Final Report has been generated and reviewed in accordance with approved methods and Laboratory Standard Operating Procedure. Exceptions,if any,are discussed in the accompanying sample narrative. Release of this Ifinal report is authorized by Laboratory management,as is verified by the following signature. 1 0,1/..,),/ 174 /,7 Approval Signature Date I I 1795 Industrial Drive Green Bay, WI 54302 E i HEM 920-469-2436 INC. 800-7-ENCHEM FAX: 920-469-8827 Lab#: TestGrouplD: Comment: 893755- 465 Acetone is present in the laboratory environment.Detects should be considered suspect. 893755-004 DRO-S Hump was present late in chromatogram. TP-5(0-2') , 893755-008 DRO-S Hump was present late in chromatogram. TP-10(2) 893755-010 DRO-S Hump was present late in chromatogram. t TP-I3(0-4') 893755-014 DRO-W Hump was present late in chromatogram. ST-1 I 1 1 1 1 1 1 1795 Industrial Drive Green Bay,WI 54302 { 920-469-2436 �� 800-7-ENCHEM E l H E i No FAX: 920-469-8827 4 I - Analytical Report - Project Name: SENIOR HOUSING ADD. IProject Number: 7735-B Client: GME CONSULTANTS Field ID: TP-2(0-2') Report Date: 7/9/99 I Lab Sample Number: 893755-001 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL IInorganic Results Analysis Prep Analysis Test Result EQL Units Code Date Method Method Solids,percent 82.3 % 7/8/99 SM2540G SM2540G Organic Results IPreservation Date: 7/7/99 DIESEL RANGE ORGANICS-SOIL Prep Method: Wi MOD DRO Prep Date: 7/7/99 Analyst: DJB I Analysis Analysis Analyte Result EQL Units Code Date Method DIESEL RANGE ORGANICS < 4.8 4.8 mg/kg 7/7/99 Wi MOD DRO I Blank spike 88 --- %Recov 7/7/99 Wi MOD DRO Blank spike duplicate 82 --- %Recov 7/7/99 Wi MOD DRO Blank < 5.0 5.0 mg/kg 7/7/99 Wi MOD DRO • Organic Results I GASOLINE RANGE ORGANICS-SOIL/METHANOL Prep Method: Wi MOD GRO Prep Date: 7/8/99 Analyst: MSB Analysis Analysis Analyte Result EQL Units Code Date Method IGasoline Range Organics < 3.0 3.0 mg/kg 7/8/99 Wi MOD GRO Blank Spike 105 — %Recov 7/8/99 Wi MOD GRO ' Blank Spike Duplicate 104 -- %Recov mg/kg 7/8/99 Wi MOD GRO Blank < 2.5 2.5 7/8/99 Wi MOD GRO Organic Results I MDH 465E VOLATILES-SOIL/METHANOL Prep Method: SW846 5030B Prep Date: 7/8/99 Analyst: RJN I Analysis Analysis Analyte Result EQL Units Code Date Method Acetone < 150 150 ug/kg 7/8/99 SW846 8260B I Ally'Chloride < 30 30 ug/kg 7/8/99 SW846 8260B Benzene < 30 30 ug/kg 7/8/99 SW846 8260B IAll soil results are reported on a dry weight basis unless otherwise noted. 1795 Industrial Drive I Green Bay,WI 54302 E' HEM 920-469-2436 I NC. 800-7-ENCHEM FAx 920-469-8827 -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS I Field ID: TP-2(0-2) Report Date: 7/9/99 Lab Sample Number: 893755-001 Collection Date: 7/2/99 I MDH LAB ID: 055-999-334 Matrix Type: SOIL Bromochloromethane < 30 30 ug/kg 7/8/99 ' SW846 82608 Bromodichloromethane < 30 30 ug/kg 7/8/99 SW846 82608 Bromoform < 30 30 ug/kg 7/8/99 SW846 82606 I Bromobenzene < 30 30 ug/kg 7/8/99 SW846 82606 Bromomethane < 30 30 ug/kg 7/8/99 SW846 82608 2-Butanone < 150 150 ug/kg 7/8/99 SW846 82606 I s-Butylbenzene < 30 30 ug/kg 7/8/99 SW846 82606 t-Butylbenzene < 30 30 ug/kg 7/8/99 SW846 82606 n-Butylbenzene < 30 30 ug/kg 7/8/99 SW846 82606 Carbon tetrachloride < 30 30 ug/kg 7/8/99 SW846 82608 Chloroform < 30 30 ug/kg 7/8/99 SW846 82608 I Chlorobenzene < 30 30 ug/kg 7/8/99 SW846 82606 Chlorodibromomethane < 30 30 ug/kg 7/8/99 SW846 82606 Chloroethane < 30 30 ug/kg 7/8/99 SW846 82608 Chloromethane < 30 30 ug/kg 7/8/99 SW846 82608 2-Chiorotoluene < 30 30 ug/kg 7/8/99 SW846 82606 4-Chiorotoluene < 30 30 ug/kg 7/8/99 SW846 82608 1,2-Dibromo-3-chloropropane < 30 30 ug/kg 7/8/99 SW846 82608 1,2-Dibromoethane < 30 30 ug/kg 7/8/99 SW846 82606 I Dibromomethane < 30 30 ug/kg 7/8/99 SW846 82608 1,3-Dichlorobenzene < 30 30 ug/kg 7/8/99 SW846 82608 1,4-Dichlorobenzene < 30 30 ug/kg 7/8/99 SW846 82606 I 1,2-Dichloroethane < 30 30 ug/kg 7/8/99 SW846 82608 1,2-Dichlorobenzene < 30 30 ug/kg 7/8/99 SW846 82606 1,1-Dichloroethene < 30 30 ug/kg 7/8/99 SW846 82606 I cis-1,2-Dichloroethene < 30 30 ug/kg 7/8/99 SW846 82606 Dichlorodifluoromethane < 30 30 ug/kg 7/8/99 SW846 82608 trans-1,2-Dichloroethene < 30 30 ug/kg 7/8/99 ' SW846 82608 Dichlorofluoromethane < 30 30 ug/kg 7/8/99 SW846 82606 1,2-Dichloropropane < 30 30 ug/kg 7/8/99 SW846 82608 I 1,1-Dichloroethane < 30 30 ug/kg 7/8/99 SW846 82608 1,3-Dichloropropane < 30 30 ug/kg 7/8/99 SW846 82608 All soil results are reported on a dry weight basis unless otherwise noted. I I 1795 Industrial Drive Green Bay,WI 54302 920-469-2436 E 1 -H FPM 800-7-ENCHEM rrc FAX: 920-469-8827 I -Analytical Report - Project Name: SENIOR HOUSING ADD. IProject Number: 7735-B Client: GME CONSULTANTS Field ID: TP-2(0-21 Report Date: 7/9/99 ILab Sample Number: 893755-001 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL I2,2-Dichloropropane < 30 30 ug/kg 7/8/99 SW846 8260B 1,1-Dichloropropene < 30 30 ug/kg 7/8/99 SW846 82608 I cis-1,3-Dichloropropene < 30 30 ug/kg 7/8/99 SW846 82608 trans-1,3-Dichloropropene < 30 30 ug/kg 7/8/99 SW846 82606 Ethylbenzene < 30 30 ug/kg 7/8/99 SW846 8260B I Diethyl ether < 150 150 ug/kg 7/8/99 SW846 8260B Fluorotrichloromethane < 30 30 ug/kg 7/8/99 SW846 82608 Hexachlorobutadiene < 30 30 ug/kg 7/8/99 SW846 8260B Ilsopropylbenzene < 30 30 ug/kg 7/8/99 SW846 82608 p-Isopropyltoluene < 30 30 ug/kg 7/8/99 SW846 8260B I Methylene chloride < 30 30 ug/kg 7/8/99 SW846 8260B 4-Methyl-2-pentanone < 150 150 ug/kg 7/8/99 SW846 8260B Methyl-tert-butyl-ether < 30 30 ug/kg 7/8/99 SW846 8260B I Naphthalene < 30 30 ug/kg 7/8/99 SW846 8260B n-Propylbenzene < 30 30 ug/kg 7/8/99 SW846 8260B Styrene < 30 30 ug/kg 7/8/99 SW846 82608 I 1,1,2,2-Tetrachloroethane < 30 30 ug/kg 7/8/99 SW846 8260B 1,1,1,2-Tetrachloroethane < 30 30 ug/kg 7/8/99 SW846 82608 I Tetrachloroethene < 30 30 ug/kg 7/8/99 SW846 8260B Toluene < 30 30 ug/kg 7/8/99 SW846 8260B 1,2,3-Trichlorobenzene < 30 30 ug/kg 7/8/99 SW846 82608 I 1,2,4-Trichlorobenzene < 30 30 ug/kg 7/8/99 SW846 8260B 1,1,1-Trichloroethane < 30 30 ug/kg 7/8/99 SW846 8260B 1,1,2-Trichloroethane < 30 30 ug/kg 7/8/99 SW846 8260B I 1,1,2-Trichlorotrifluoroethane < 30 30 ug/kg 7/8/99 SW846 8260B 1,2,4-Trimethylbenzene < 30 30 ug/kg 7/8/99 SW846 8260B Trichloroethene < 30 30 ug/kg 7/8/99 SW846 8260B I1,2,3-Trichloropropane < 30 30 ug/kg 7/8/99 SW846 8260B Tetrahydrofuran < 150 150 ug/kg 7/8/99 SW846 8260B Ii,3,5-Trimethylbenzene < 30 30 ug/kg 7/8/99 SW846 8260B Vinyl chloride < 30 30 ug/kg 7/8/99 SW846 82608 Xylenes,-m,-p < 30 30 ug/kg 7/8/99 SW846 8260B IAll soil results are reported on a dry weight basis unless otherwise noted. I 1795 Industrial Drive Green Bay,WI 54302 E '� ' �HEM 800-07-ENCHEM INC. FAX: 920-469-8827 -Analytical Report - Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS ' Field ID: TP-2(0-2') Report Date: 7/9/99 Lab Sample Number: 893755-001 Collection Date: 7/2/99 1 MDH LAB ID: 055-999-334 Matrix Type: SOIL Xylene,-o < 30 30 ug/kg 7/8/99 SW846 8260B 4-Bromofluorobenzene 92 --- %Recov 7/8/99 SW846 8260B Dibromofluoromethane 88 — %Recov 7/8/99 SW846 8260B Toluene-d8 95 — %Recov 7/8/99 SW846 8260B I 1 r I All soil results are reported on a dry weight basis unless otherwise noted. ' 1 ■ I 1795 Industrial Drive Green Bay,WI 54302 920-469-2436 E i , H P.M 800-7-ENCHEM INC. Fnx 920469-8827 1 -Analytical Report - Project Name: SENIOR HOUSING ADD. IProject Number: 7735-B Client: GME CONSULTANTS Field ID: TP-3(0-7) Report Date: 7/9/99 ILab Sample Number: 893755-002 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL IInorganic Results Analysis Prep Analysis Test Result EQL Units Code Date Method Method Solids,percent 83.9 % 7/8/99 SM2540G SM2540G Organic Results IPreservation Date: 7/7/99 DIESEL RANGE ORGANICS-SOIL Prep Method: Wi MOD DRO Prep Date: 7/7/99 Analyst: DJB I Analysis Analysis Analyte Result EQL Units Code Date Method DIESEL RANGE ORGANICS 16 4.7 mg/kg 7/7/99 Wi MOD DRO IBlank spike 88 --- %Recov 7/7/99 Wi MOD DRO Blank spike duplicate 82 — %Recov 7/7/99 Wi MOD DRO Blank < 5.0 5.0 mg/kg 7/7/99 Wi MOD DRO IOrganic Results IGASOLINE RANGE ORGANICS-SOIL/METHANOL Prep Method: Wi MOD GRO Prep Date: 7/8/99 Analyst: MSB Analysis Analysis Analyte Result EQL Units Code Date Method IGasoline Range Organics < 3.0 3.0 mg/kg 7/8/99 Wi MOD GRO Blank Spike 105 -- %Recov 7/8/99 Wi MOD GRO I Blank Spike Duplicate Blank 104 -- %Recov mg/kg 7/8/99 Wi MOD GRO < 2.5 2.5 7/8/99 Wi MOD GRO Organic Results I MDH 465E VOLATILES-SOIL/METHANOL Prep Method: SW846 5030B Prep Date: 7/8/99 Analyst: RJN I Analysis Analysis Analyte Result EQL Units Code Date Method Acetone < 150 150 ug/kg 7/8/99 SW846 8260B I Ally!Chloride < 30 30 ug/kg 7/8/99 SW846 8260B Benzene < 30 30 ug/kg 7/8/99 SW846 8260B IAll soil results are reported on a dry weight basis unless otherwise noted. � 1795 Industrial Drive r Green Bay,WI 54302 �11 !^AHEM 920-469-2436 INC. FAX: 920-469C-8827 -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS I Field ID: TP-3(0-21 Report Date: 7/9/99 Lab Sample Number: 893755-002 Collection Date: 7/2/99 I MDH LAB ID: 055-999-334 Matrix Type: SOIL Bromochloromethane < 30 30 ug/kg 7/8/99 SW846 8260B I Bromodichloromethane < 30 30 ug/kg 7/8/99 SW846 8260B Bromoform < 30 30 ug/kg 7/8/99 SW846 8260B Bromobenzene < 30 30 ug/kg 7/8/99 SW846 8260B I Bromomethane < 30 30 ug/kg 7/8/99 SW846 82606 2-Butanone < 150 150 ug/kg 7/8/99 SW846 8260B III s-Butylbenzene < 30 30 ug/kg 7/8/99 SW846 8260B t-Butylbenzene < 30 30 ug/kg 7/8/99 SW846 8260B n-Butylbenzene < 30 30 ug/kg 7/8/99 SW846 8260B I Carbon tetrachloride < 30 30 ug/kg 7/8/99 SW846 8260B Chloroform < 30 30 ug/kg 7/8/99 SW846 8260B Chlorobenzene < 30 30 ug/kg 7/8/99 SW846 8260B I Chiorodibromomethane < 30 30 ug/kg 7/8/99 SW846 8260B Chloroethane < 30 30 ug/kg 7/8/99 SW846 8260B I Chloromethane < 30 30 ug/kg 7/8/99 SW846 8260B 2-Chiorotoluene < 30 30 ug/kg 7/8/99 SW846 8260B 4-Chiorotoluene < 30 30 ug/kg 7/8/99 SW846 8260B I 1,2-Dibromo-3-chioropropane < 30 30 ug/kg 7/8/99 SW846 8260B 1,2-Dibromoethane < 30 30 ug/kg 7/8/99 SW846 8260B Dibromomethane < 30 30 ug/kg 7/8/99 SW846 8260B 1,3-Dichlorobenzene < 30 30 ug/kg 7/8/99 SW846 8260B 1,4-Dichlorobenzene < 30 30 ug/kg 7/8/99 SW846 8260B 1,2-Dichloroethane < 30 30 ug/kg 7/8/99 SW846 8260B I 1,2-Dichlorobenzene < 30 30 ug/kg 7/8/99 SW846 82608 1,1-Dichloroethene < 30 30 ug/kg 7/8/99 SW846 8260B I cis-1,2-Dichloroethene < 30 30 ug/kg 7/8/99 SW846 8260B Dichlorodifluoromethane < 30 30 ug/kg 7/8/99 SW846 8260B trans-1,2-Dichloroethene < 30 30 ug/kg 7/8/99 SW846 82608 I Dichlorofluoromethane < 30 30 ug/kg 7/8/99 SW846 8260B 1,2-Dichloropropane < 30 30 ug/kg 7/8/99 SW846 8260B 1,1-Dichloroethane < 30 30 ug/kg 7/8/99 SW846 8260B 1 1,3-Dichloropropane < 30 30 ug/kg 7/8/99 SW846 8260B All soil results are reported on a dry weight basis unless otherwise noted. I I ' 1795 Industrial Drive Green Bay, WI 54302 920-469-2436 E lit HEM 800-7-ENCHEM I 1 NC, FAX: 920-469-8827 I -Analytical Report - Project Name: SENIOR HOUSING ADD. IProject Number: 7735-B Client: GME CONSULTANTS Field ID: TP-3(0-21 Report Date: 7/9/99 I Lab Sample Number: 893755-002 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL I 2,2-Dichloropropane < 30 30 ug/kg 7/8/99 SW846 8260B 1,1-Dichloropropene < 30 30 ug/kg 7/8/99 SW846 8260B I cis-1,3 Dichloropropene < 30 30 ug/kg 7/8/99 SW846 8260B trans-1,3-Dichloropropene < 30 30 ug/kg 7/8/99 SW8468260B Ethylbenzene < 30 30 ug/kg 7/8/99 SW846 8260B I Diethyl ether < 150 150 ug/kg 7/8/99 SW846 8260B Fluorotrichloromethane < 30 30 ug/kg 7/8/99 SW846 82608 Hexachlorobutadiene < 30 30 ug/kg 7/8/99 SW846 8260B I Isopropylbenzene < 30 30 ug/kg 7/8/99 SW846 8260B p-lsopropyltoluene < 30 30 ug/kg 7/8/99 SW846 8260B Methylene chloride < 30 30 ug/kg 7/8/99 SW846 8260B I4-Methyl-2-pentanone < 150 150 ug/kg 7/8/99 SW846 8260B Methyl-tert-butyl-ether < 30 30 ug/kg 7/8/99 SW846 8260B I Naphthalene < 30 30 ug/kg 7/8/99 SW846 8260B n-Propylbenzene < 30 30 ug/kg 7/8/99 SW846 82606 Styrene < 30 30 ug/kg 7/8/99 SW846 8260B I 1,1,2,2 Tetrachloroethane < 30 30 ug/kg 7/8/99 SW846 8260B 1,1,1,2-Tetrachloroethane < 30 30 ug/kg 7/8/99 SW846 82608 Tetrachloroethene < 30 30 ug/kg 7/8/99 SW846 8260B IToluene < 30 30 ug/kg 7/8/99 SW846 8260B 1,2,3-Trichlorobenzene < 30 30 ug/kg 7/8/99 SW846 8260B I 1,2,4-Trichlorobenzene < 30 30 ug/kg 7/8/99 SW846 8260B 1,1,1-Trichloroethane < 30 30 ug/kg 7/8/99 SW846 82608 •1,1,2-Trichloroethane < 30 30 ug/kg 7/8/99 SW846 82608 I 1,1,2-Trichlorotrifluoroethane < 30 30 ug/kg 7/8/99 SW846 8260B 1,2,4-Trimethylbenzene < 30 30 ug/kg 7/8/99 SW846 82608 Trichloroethene < 30 30 ug/kg 7/8/99 SW846 8260B I 1,2,3 Trichloropropane < 30 30 ug/kg 7/8/99 SW846 8260B Tetrahydrofuran < 150 150 ug/kg 7/8/99 SW846 8260B I 1,3,5-Trimethylbenzene < 30 30 ug/kg 7/8/99 SW846 8260B Vinyl chloride < 30 30 ug/kg 7/8/99 SW846 82606 Xylenes,-m,-p < 30 30 ug/kg 7/8/99 SW846 8260B IAll soil results are reported on a dry weight basis unless otherwise noted. lit 1795 Industrial Drive ill Green Bay, WI 54302 E' HE M 920 469 2436 r ivc. 800-7-ENCHEM FAx 920-469-8827 -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS I Field ID: TP-3(0-2') Report Date: 7/9/99 Lab Sample Number: 893755-002 Collection Date: 7/2/99 1 MDH LAB ID: 055-999-334 Matrix Type: SOIL Xylene,-o < 30 30 ug/kg 7/8/99 SW846 8260B I 4-Bromofluorobenzene 101 — %Recov 7/8/99 SW846 8260B Dibromofluoromethane 97 --- %Recov 7/8/99 SW846 8260B Toluene-d8 101 --- %Recov 7/8/99 SW846 8260B 1 I I I I I I I I I I All soil results are reported on a dry weight basis unless otherwise noted. 1 I 1795 Industrial Drive P Green Bay,WI 54302 920-469-2436 E_ . : HEM 800-7-ENCHEM IINC FAx: 920-469-8827 I -Analytical Report - Project Name: SENIOR HOUSING ADD. IProject Number: 7735-B Client: GME CONSULTANTS Field ID: TP-3(4-6') Report Date: 7/9/99 Lab Sample Number: 893755-003 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL IInorganic Results Test Result EQL Units Code Analysis Prep Analysis I Date Method Method Solids,percent 88.4 % 7/8/99 SM2540G SM2540G Organic Results IPreservation Date: 7/7/99 DIESEL RANGE ORGANICS-SOIL Prep Method: Wi MOD DRO Prep Date: 7/7/99 Analyst: DJB Result Analysis Analysis Analyte EQL Units Code Date Method DIESEL RANGE ORGANICS < 4.3 4.3 mg/kg 7/7/99 Wi MOD DRO Blank spike 88 --- %Recov 7/7/99 Wi MOD DRO Blank spike duplicate 82 -- %Recov 7/7/99 Wi MOD DRO I Blank < 5.0 5.0 mg/kg 7/7/99 Wi MOD DRO Organic Results 1 GASOLINE RANGE ORGANICS-SOIL/METHANOL Prep Method: Wi MOD GRO Prep Date: 7/8/99 Analyst: MSB Result Analysis Analysis Analyte EQL Units Code Date Method IIGasoline Range Organics < 2.8 2.8 mg/kg 7/8/99 Wi MOD GRO Blank Spike 105 --- %Recov 7/8/99 Wi MOD GRO I Blank Spike Duplicate 104 %Recov 7/8/99 Wi MOD GRO Blank < 2.5 2.5 mg/kg 7/8/99 Wi MOD GRO Organic Results I MDH 465E VOLATILES-SOIL/METHANOL Prep Method: SW846 5030B Prep Date: 7/8/99 Analyst: RJN I Result Analysis Analysis Analyte EQL Units Code Date Method Acetone < 140 140 ug/kg 7/8/99 SW846 8260B IAlly!Chloride < 28 28 ug/kg 7/8/99 SW846 8260B Benzene < 28 28 ug/kg 7/8/99 SW846 8260B I All soil results are reported on a dry weight basis unless otherwise noted. • 1795 Industrial Drive Green Bay,WI 54302 920-469-2436 i E HEM, 800-7-ENCHEM FAx 920-469-8827 I -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS I Field ID: TP-3(4-6') Report Date: 7/9/99 Lab Sample Number: 893755-003 Collection Date: 7/2/99 I MDH LAB ID: 055-999-334 Matrix Type: SOIL Bromochloromethane < 28 28 ug/kg 7/8/99 SW846 8260B 111 Bromodichloromethane < 28 28 ug/kg 7/8/99 SW846 8260B Bromoform < 28 28 ug/kg 7/8/99 SW846 8260B I Bromobenzene < 28 28 ug/kg 7/8/99 SW846 82606 Bromomethane < 28 28 ug/kg 7/8/99 SW846 8260B 2-Butanone < 140 140 ug/kg 7/8/99 SW846 8260B I s-Butylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B t-Butylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B n-Butylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B I Carbon tetrachloride < 28 28 ug/kg 7/8/99 SW846 8260B Chloroform < 28 28 ug/kg 7/8/99 SW846 8260B Chlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B I Chlorodibromomethane < 28 28 ug/kg 7/8/99 SW846 8260B Chioroethane < 28 28 ug/kg 7/8/99 SW846 8260B Chloromethane < 28 28 ug/kg 7/8/99 SW846 8260B 2-Chlorotoluene < 28 28 ug/kg 7/8/99 SW846 8260B 4-Chlorotoluene < 28 28 ug/kg 7/8/99 SW846 8260B 1,2-Dibromo-3-chloropropane < 28 28 ug/kg 7/8/99 SW846 8260B 1,2-Dibromoethane < 28 28 ug/kg 7/8/99 SW846 8260B Dibromomethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,3-Dichlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B 1,4-Dichlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B I 1,2-Dichloroethane < 28 28 ug/kg 7/8/99 SW846 82608 1,2-Dichlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B 1,1-Dichloroethene < 28 28 ug/kg 7/8/99 SW846 8260B cis-1,2-Dichloroethene < 28 . 28 ug/kg 7/8/99 SW846 8260B Dichlorodifluoromethane < 28 28 ug/kg 7/8/99 SW846 8260B trans-1,2-Dichloroethene < 28 28 ug/kg 7/8/99 SW846 8260B I Dichlorofluoromethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,2-Dichloropropane < 28 28 ug/kg 7/8/99 SW846 8260B I 1,1-Dichloroethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,3-Dichloropropane < 28 28 ug/kg 7/8/99 SW846 8260B All soil results are reported on a dry weight basis unless otherwise noted. I 1795 Industrial Drive Green Bay,WI 54302 920-469-2436 E HEM 800 7 ENCHEM INC. FAx: 920-469-8827 I -Analytical Report - Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS Field ID: TP-3(4-6') Report Date: 7/9/99 Lab Sample Number: 893755-003 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL 2,2-Dichloropropane < 28 28 ug/kg 7/8/99 SW846 8260B 1,1-Dichloropropene < 28 28 ug/kg 7/8/99 SW846 8260B cis-1,3-Dichloropropene < 28 28 ug/kg 7/8/99 SW846 8260B trans-1,3-Dichloropropene < 28 28 ug/kg 7/8/99 SW846 8260B Ethylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B Diethyl ether < 140 140 ug/kg 7/8/99 SW846 8260B Fluorotrichloromethane < 28 28 ug/kg 7/8/99 SW846 8260B Hexachlorobutadiene < 28 28 ug/kg 7/8/99 SW846 8260B Isopropylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B p-Isopropyltoluene < 28 28 ug/kg 7/8/99 SW846 8260B Methylene chloride < 28 28 ug/kg 7/8/99 SW846 8260B ' 7/8/99 SW846 8260B 4-Methyl-2-pentanone < 140 140 ug/kg Methyl-tert-butyl-ether < 28 28 ug/kg 7/8/99 SW846 8260B Naphthalene < 28 28 ug/kg 7/8/99 SW846 8260B n-Propylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B Styrene < 28 28 ug/kg 7/8/99 SW846 8260B 1 7/8/99 SW846 82608 1,1,2,2-Tetrachloroethane < 28 28 ug/kg 1,1,1,2-Tetrachloroethane < 28 28 ug/kg 7/8/99 SW846 8260B Tetrachloroethene < 28 28 ug/kg 7/8/99 SW846 8260B 1 7/8/99 SW846 8260B Toluene < 28 28 ug/kg 1,2,3-Trichlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B Il,2,4-Trichlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B 1,1,1-Trichloroethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,1,2-Trichloroethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,1,2-Trichlorotrifluoroethane < 28 28 ug/kg 7/8/99 SW846 82606 1,2,4-Trimethylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B Trichloroethene < 28 28 ug/kg 7/8/99 SW846 8260B 1 1,2,3-Trichloropropane < 28 28 ug/kg 7/8/99 SW846 8260B Tetrahydrofuran < 140 140 ug/kg 7/8/99 SW846 8260B 1,3,5-Trimethylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B Vinyl chloride < 28 28 ug/kg 7/8/99 SW846 8260B Xylenes,-m,-p < 28 28 ug/kg 7/8/99 SW846 8260B All soil results are reported on a dry weight basis unless otherwise noted. 1795 Industrial Drive 1 Green Bay, 54302 A E *4 1 • HEM WI 9 2436 INC. 800-7-ENCHEM Fnx 920-469-8827 -Analytical Report- I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS I Field ID: TP-3(4-6') Report Date: 7/9/99 Lab Sample Number: 893755-003 Collection Date: 7/2/99 1 MDH LAB ID: 055-999-334 Matrix Type: SOIL Xylene,-o < 28 28 ug/kg 7/8/99 SW846 8260B 4-Bromofluorobenzene 98 -- %Recov 7/8/99 SW846 8260B Dibromofluoromethane 95 -- %Recov 7/8/99 SW846 8260B Toluene-d8 102 — • %Recov 7/8/99 SW846 8260B 1 I I I I I I I 1 I I All soil results are reported on a dry weight basis unless otherwise noted. I I I 1795 Industrial Drive Green Bay, WI 54302 920-469-2436 E i HEM 800-7-ENCHEM 1 . t Nc. FAx 920-469-8827 I -Analytical Report - Project Name: SENIOR HOUSING ADD. IProject Number: 7735-B Client: GME CONSULTANTS Field ID: TP-5(0-21 Report Date: 7/9/99 ILab Sample Number: 893755-004 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL 1 Inorganic Results Analysis Prep Analysis I Test Result 86.9 EQL Units Code Date Method Method Solids,percent % 7/8/99 SM2540G SM2540G I Organic Results Preservation Date: 7/7/99 DIESEL RANGE ORGANICS-SOIL Prep Method: Wi MOD DRO Prep Date: 7/7/99 Analyst: DJB I Result EQL Units Code Analysis Analysis Analyte Date Method DIESEL RANGE ORGANICS 5.6 4.4 mg/kg 7/7/99 Wi MOD DRO IBlank spike 102 --- %Recov 7/7/99 Wi MOD DRO Blank spike duplicate 89 --- %Recov 7/7/99 Wi MOD DRO Blank < 5.0 5.0 mg/kg 7/7/99 Wi MOD DRO I Organic Results IGASOLINE RANGE ORGANICS-SOIL/METHANOL Prep Method: Wi MOD GRO Prep Date: 7/8/99 Analyst: MSB Result EQL Units Code Analysis Analysis I Analyte Date M Gasoline Range Organics < 2.9 2.9 mg/kg 7/8/99 Wi MOD GRO Blank Spike 105 --- %Recov 7/8/99 Wi MOD GRO I --- %Recov 7/8/99 Wi MOD GRO Blank Spike Duplicate 104 Blank < 2.5 2.5 mg/kg 7/8/99 Wi MOD GRO Organic Results I MDH 465E VOLATILES-SOIL/METHANOL Prep Method: SW846 5030B Prep Date: 7/8/99 Analyst: RJN I Result EQL Units Code Analysis Analysis Analyte Date Method Acetone 220 140 ug/kg 7/8/99 SW846 8260B Ally/Chloride < 29 29 ug/kg 7/8/99 SW846 8260B Benzene < 29 29 ug/kg 7/8/99 SW846 8260B IAll soil results are reported on a dry weight basis unless otherwise noted. 1795 Industrial Drive Green Bay,WI 54302 920-469-2436 E I AHEM INC. 8007 ENCHEM FAx 920-469-8827 I -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS I Field ID: TP-5(0-T) Report Date: 7/9/99 Lab Sample Number: 893755-004 Collection Date: 7/2/99 1 MDH LAB ID: 055-999-334 Matrix Type: SOIL Bromochloromethane < 29 29 ug/kg 7/8/99 SW846 8260B Bromodichloromethane < 29 29 ug/kg 7/8/99 SW846 8260B Bromoform < 29 29 ug/kg 7/8/99 SW846 8260B Bromobenzene < 29 29 ug/kg 7/8/99 SW846 8260B 1 Bromomethane < 29 29 ug/kg 7/8/99 SW846 8260B 2-Butanone < 140 140 ug/kg 7/8/99 SW846 8260B s-Butylbenzene < 29 29 ug/kg 7/8/99 SW846 8260B t-Butylbenzene < 29 29 ug/kg 7/8/99 SW846 8260B n-Butylbenzene < 29 29 ug/kg 7/8/99 SW846 8260B I Carbon tetrachloride < 29 29 ug/kg 7/8/99 SW846 8260B Chloroform < 29 29 ug/kg 7/8/99 SW846 8260B Chlorobenzene < 29 29 ug/kg 7/8/99 SW846 8260B I Chlorodibromomethane < 29 29 ug/kg 7/8/99 SW846 8260B Chloroethane < 29 29 ug/kg 7/8/99 SW846 8260B I Chloromethane < 29 29 ug/kg 7/8/99 SW846 8260B 2-Chlorotoluene < 29 29 ug/kg 7/8/99 SW846 8260B 4-Chlorotoluene < 29 29 ug/kg 7/8/99 SW846 8260B I 1,2-Dibromo-3-chloropropane < 29 29 ug/kg 7/8/99 SW846 8260B 1,2-Dibromoethane < 29 29 ug/kg 7/8/99 SW846 8260B Dibromomethane < 29 29 ug/kg 7/8/99 SW846 8260B 111 1,3-Dichlorobenzene < 29 29 ug/kg 7/8/99 SW846 8260B 1,4-Dichlorobenzene < 29 29 ug/kg 7/8/99 SW846 8260B I1,2-Dichloroethane < 29 29 ug/kg 7/8/99 SW846 8260B 1,2-Dichlorobenzene < 29 29 ug/kg 7/8/99 SW846 8260B 1,1-Dichloroethene < 29 29 ug/kg 7/8/99 SW846 8260B cis-1,2-Dichloroethene < 29 29 ug/kg 7/8/99 SW846 8260B Dichlorodifluoromethane < 29 29 ug/kg 7/8/99 SW846 8260B trans-1,2-Dichloroethene < 29 29 ug/kg 7/8/99 SW846 8260B Dichlorofluoromethane < 29 29 ug/kg 7/8/99 SW846 8260B 1,2-Dichloropropane < 29 29 ug/kg 7/8/99 SW846 8260B I 1,1-Dichloroethane < 29 29 ug/kg 7/8/99 SW846 8260B 1,3-Dichloropropane < 29 29 ug/kg 7/8/99 SW846 8260B All soil results are reported on a dry weight basis unless otherwise noted. I 1795 Industrial Drive �_ Green Bay, WI 54302 ' 920-469-2436 E I a HEM 800-7-ENCHEM i NC • FAX: 920-469-8827 I -Analytical Report - Project Name: SENIOR HOUSING ADD. IProject Number: 7735-B Client: GME CONSULTANTS Field ID: TP-5(0-2') Report Date: 7/9/99 ILab Sample Number: 893755-004 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL 1 2,2-Dichloropropane < 29 29 ug/kg 7/8/99 SW846 8260B 1,1-Dichloropropene < 29 29 ug/kg 7/8/99 SW846 8260B I cis-1,3-Dichloropropene < 29 29 ug/kg 7/8/99 SW846 8260B trans-1,3-Dichloropropene < 29 29 ug/kg 7/8/99 SW846 8260B Ethylbenzene < 29 29 ug/kg 7/8/99 SW846 82608 I Diethyl ether < 140 140 ug/kg 7/8/99 SW846 8260B Fluorotrichloromethane < 29 29 ug/kg 7/8/99 SW846 8260B Hexachlorobutadiene < 29 29 ug/kg 7/8/99 SW846 8260B IIsopropylbenzene < 29 29 ug/kg 7/8/99 SW846 8260B p-Isopropyltoluene < 29 29 ug/kg 7/8/99 SW846 8260B I Methylene chloride < 29 29 ug/kg 7/8/99 SW846 82606 4-Methyl-2-pentanone < 140 140 ug/kg 7/8/99 SW846 8260B Methyl-tert-butyl-ether < 29 29 ug/kg 7/8/99 SW846 8260B I Naphthalene < 29 29 ug/kg 7/8/99 SW846 8260B n-Propylbenzene < 29 29 ug/kg 7/8/99 SW846 8260B Styrene < 29 29 ug/kg 7/8/99 SW846 8260B I1,1,2,2-Tetrachloroethane < 29 29 ug/kg 7/8/99 SW846 82608 1,1,1,2-Tetrachloroethane < 29 29 ug/kg 7/8/99 SW846 8260B Tetrachloroethene < 29 29 ug/kg 7/8/99 SW846 8260B IToluene < 29 29 ug/kg 7/8/99 SW846 8260B 1,2,3-Trichlorobenzene < 29 29 ug/kg 7/8/99 SW846 8260B I 1,2,4-Trichlorobenzene < 29 29 ug/kg 7/8/99 SW846 82606 1,1,1-Trichloroethane < 29 29 ug/kg 7/8/99 SW846 82608 1,1,2-Trichloroethane < 29 29 ug/kg 7/8/99 SW846 8260B I1,1,2-Trichlorotrifluoroethane < 29 29 ug/kg 7/8/99 SW846 82608 1,2,4-Trimethylbenzene < 29 29 ug/kg 7/8/99 SW846 8260B Trichloroethene < 29 29 ug/kg 7/8/99 SW846 8260B I1,2,3-Trichloropropane < 29 29 ug/kg 7/8/99 SW846 8260B Tetrahydrofuran < 140 140 ug/kg 7/8/99 SW846 8260B Il,3,5-Trimethylbenzene < 29 29 ug/kg 7/8/99 SW846 82608 Vinyl chloride < 29 29 ug/kg 7/8/99 SW846 8260B Xylenes,-m,-p < 29 29 ug/kg 7/8/99 SW846 8260B IAll soil results are reported on a dry weight basis unless otherwise noted. 1795 Industrial Drive Green Bay,WI 54302 E Atii.HE1%/ 920-469-2436 800-7-ENCHEM 1 -4 r, xc FAx: 92069-8827 -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS I Field ID: TP-5(0-2) Report Date: 7/9/99 Lab Sample Number: 893755-004 Collection Date: 7/2/99 1 MDH LAB ID: 055-999-334 Matrix Type: SOIL Xylene,-o < 29 29 ug/kg 7/8/99 SW846 8260B t 4-Bromofluorobenzene 132 -- %Recov 7/8/99 SW846 8260B Dibromofluoromethane 122 — %Recov 7/8/99 SW846 8260B Toluene-d8 129 -- %Recov 7/8/99 SW846 82608 I I I 1 I I I I I I All soil results are reported on a dry weight basis unless otherwise noted. I I � A �_ 1795 Industrial Drive Green Bay,WI 54302 920-469-2436 Fi' HEM 800-7-ENCHEM sig INC. FAx 920469-8827 I -Analytical Report- Project Name: SENIOR HOUSING ADD. IProject Number: 7735-B Client: GME CONSULTANTS Field ID: TP-6(0-2') Report Date: 7/9/99 ILab Sample Number: 893755-005 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL IInorganic Results Test Result EQL Units Code Analysis Prep Analysis Date Method Method Solids,percent 81.7 % 7/8/99 SM2540G SM2540G Organic Results IPreservation Date: 7/7/99 DIESEL RANGE ORGANICS-SOIL Prep Method: Wi MOD DRO Prep Date: 7/7/99 Analyst: DJB I Result Analysis Analysis Analyte EQL Units Code Date Method DIESEL RANGE ORGANICS < 4.8 4.8 mg/kg 7/7/99 Wi MOD DRO 1 Blank spike 102 --- %Recov 7/7/99 Wi MOD DRO Blank spike duplicate 89 -- %Recov 7/7/99 Wi MOD DRO I Blank < 5.0 5.0 mg/kg 7/7/99 Wi MOD DRO Organic Results GASOLINE RANGE ORGANICS-SOIL/METHANOL Prep Method: Wi MOD GRO Prep Date: 7/8/99 Analyst: MSB Analysis Analysis Analyte Result EQL Units Code Date Method IGasoline Range Organics < 3.1 3.1 mg/kg 7/8/99 Wi MOD GRO Blank Spike 105 -- %Recov 7/8/99 Wi MOD GRO 1 Blank Spike Duplicate 104 %Recov 7/8/99 Wi MOD GRO Blank < 2.5 2.5 mg/kg 7/8/99 Wi MOD GRO Organic Results I MDH 465E VOLATILES-SOIL/METHANOL Prep Method: SW846 5030B Prep Date: 7/8/99 Analyst: RJN I Result Analysis Analysis Analyte EQL Units Code Date Method Acetone < 150 150 ug/kg 7/8/99 SW846 8260B I Allyl Chloride < 31 31 ug/kg 7/8/99 SW846 8260B Benzene < 31 31 ug/kg 7/8/99 SW846 8260B IAll soil results are reported on a dry weight basis unless otherwise noted. 1795 Industrial Drive Akk Green Bay,WI 54302 EHEM 920-469-2436 INC. 800-7 ENCHEM FAx 920-469-8827 I -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS I Field ID: TP-6(0-2') Report Date: 7/9/99 Lab Sample Number: 893755-005 Collection Date: 7/2/99 I MDH LAB ID: 055-999-334 Matrix Type: SOIL Bromochloromethane < 31 31 ug/kg 7/8/99 SW846 8260B III Bromodichloromethane < 31 31 ug/kg 7/8/99 SW846 8260B Bromoform < 31 31 ug/kg 7/8/99 SW846 8260B Bromobenzene < 31 31 ug/kg 7/8/99 SW846 8260B Bromomethane < 31 31 ug/kg 7/8/99 SW846 8260B 2-Butanone < 150 150 ug/kg 7/8/99 SW846 82606 s-Butylbenzene < 31 31 ug/kg 7/8/99 SW846 8260B t-Butylbenzene < 31 31 ug/kg 7/8/99 SW846 8260B n-Butylbenzene < 31 31 ug/kg 7/8/99 SW846 8260B Carbon tetrachloride < 31 31 ug/kg 7/8/99 SW846 8260B Chloroform < 31 31 ug/kg 7/8/99 SW846 8260B Chlorobenzene < 31 31 ug/kg 7/8/99 SW846 8260B t Chlorodibromomethane < 31 31 ug/kg 7/8/99 SW846 8260B Chloroethane < 31 31 ug/kg 7/8/99 SW846 8260B Chloromethane < 31 31 ug/kg 7/8/99 SW846 8260B 2-Chlorotoluene < 31 31 ug/kg 7/8/99 SW846 8260B 4-Chlorotoluene < 31 31 ug/kg 7/8/99 SW846 8260B 1,2-Dibromo-3-chloropropane < 31 31 ug/kg 7/8/99 SW846 8260B 1,2-Dibromoethane < 31 31 ug/kg 7/8/99 SW846 8260B Dibromomethane < 31 31 ug/kg 7/8/99 SW846 8260B 1,3-Dichlorobenzene < 31 31 ug/kg 7/8/99 SW846 8260B 1,4-Dichlorobenzene < 31 31 ug/kg 7/8/99 SW846 8260B 1,2-Dichloroethane < 31 31 ug/kg 7/8/99 SW846 8260B 1,2-Dichlorobenzene < 31 31 ug/kg 7/8/99 SW846 8260B 1,1-Dich loroethene < 31 31 ug/kg 7/8/99 SW846 8260B cis-1,2-Dichloroethene < 31 31 ug/kg 7/8/99 SW846 8260B Dichlorodifluoromethane < 31 31 ug/kg 7/8/99 SW846 8260B trans-1,2-Dichloroethene < 31 31 ug/kg 7/8/99 SW846 8260B Dichlorofluoromethane < 31 31 ug/kg 7/8/99 SW846 8260B 1,2-Dichloropropane < 31 31 ug/kg 7/8/99 SW846 8260B 1,1-Dichloroethane < 31 31 ug/kg 7/8/99 SW846 8260B 1,3-Dichloropropane < 31 31 ug/kg 7/8/99 SW846 8260B All soil results are reported on a dry weight basis unless otherwise noted. I I 1795 Industrial Drive Green Bay,WI 54302 920-469-2436 E HEM 800-7-ENCHEM IINC. FAX: 920-469-8827 I -Analytical Report - Project Name: SENIOR HOUSING ADD. IIProject Number: 7735-B Client: GME CONSULTANTS Field ID: TP-6(0-21 Report Date: 7/9/99 1 Lab Sample Number: 893755-005 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL I2,2-Dichloropropane < 31 31 ug/kg 7/8/99 SW846 8260B 1,1-Dichloropropene < 31 31 ug/kg 7/8/99 SW846 8260B I cis-1,3-Dichloropropene < 31 31 ug/kg 7/8/99 SW846 8260B trans-1,3-Dichloropropene < 31 31 ug/kg 7/8/99 SW846 8260B Ethylbenzene < 31 31 ug/kg 7/8/99 SW846 82608 I Diethyl ether < 150 150 ug/kg 7/8/99 SW846 8260B Fluorotrichloromethane < 31 31 ug/kg 7/8/99 SW846 82608 Hexachlorobutadiene < 31 31 ug/kg 7/8/99 SW846 8260B I Isopropylbenzene < 31 31 ug/kg 7/8/99 SW846 8260B p-lsopropyltoluene < 31 31 ug/kg 7/8/99 SW846 8260B Methylene chloride < 31 31 ug/kg 7/8/99 SW846 8260B I4-Methyl-2-pentanone < 150 150 ug/kg 7/8/99 SW846 8260B Methyl-tert-butyl-ether < 31 31 ug/kg 7/8/99 SW846 8260B I Naphthalene < 31 31 ug/kg 7/8/99 SW846 8260B n-Propylbenzene < 31 31 ug/kg 7/8/99 SW846 82608 Styrene < 31 31 ug/kg 7/8/99 SW846 82608 I 1,1,2,2-Tetrachioroethane < 31 31 ug/kg 7/8/99 SW846 82606 1,1,1,2-Tetrachioroethane < 31 31 ug/kg 7/8/99 SW846 82608 Tetrachloroethene < 31 31 ug/kg 7/8/99 SW846 8260B IToluene < 31 31 ug/kg 7/8/99 SW846 82606 1,2,3-Trichlorobenzene < 31 31 ug/kg 7/8/99 SW846 8260B I 1,2,4-Trichlorobenzene < 31 31 ug/kg 7/8/99 SW846 8260B 1,1,1-Trichloroethane < 31 31 ug/kg 7/8/99 SW846 8260B 1,1,2-Trichloroethane < 31 31 ug/kg 7/8/99 SW846 8260B I 1,1,2-Trichlorotrifluoroethane < 31 31 ug/kg 7/8/99 SW846 8260B 1,2,4-Trimethylbenzene < 31 31 ug/kg 7/8/99 SW846 8260B Trichloroethene < 31 31 ug/kg 7/8/99 SW846 8260B Il 2,3-Trichloropropane < 31 31 ug/kg 7/8/99 SW846 8260B Tetrahydrofuran < 150 150 ug/kg 7/8/99 SW846 8260B I 1,3,5-Trimethylbenzene < 31 31 ug/kg 7/8/99 SW846 82608 Vinyl chloride < 31 31 ug/kg 7/8/99 SW846 82608 Xylenes,-m,-p < 31 31 ug/kg 7/8/99 SW846 8260B IAll soil results are reported on a dry weight basis unless otherwise noted. I 1795 Industrial Drive Green Bay.WI 54302 E# 920-469-2436 ! HEWN 1 ii 800 7 ENCHEM FAx 920-469-8827 I -Analytical Report - III Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS I Field ID: TP-6(0-2) Report Date: 7/9/99 Lab Sample Number: 893755-005 Collection Date: 7/2/99 I MDH LAB ID: 055-999-334 Matrix Type: SOIL Xylene,-o < 31 31 ug/kg 7/8/99 SW846 8260B 4-Bromofluorobenzene 97 — %Recov 7/8/99 SW846 8260B Dibromofluoromethane 93 -- %Recov 7/8/99 SW846 8260B Toluene-d8 100 -- %Recov 7/8/99 SW846 8260B I I I I I I I I I I I All soil results are reported on a dry weight basis unless otherwise noted. I I 1795 Industrial Drive Green Bay, WI 54302 E i H■ M 800-07-ENCHEM INC. FAX 920-469-8827 I -Analytical Report - Project Name: SENIOR HOUSING ADD. 1 Project Number: 7735-B Client: GME CONSULTANTS Field ID: TP-7(0-2') Report Date: 7/9/99 ILab Sample Number: 893755-006 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL IInorganic Results Test Result EQL Units Code Analysis Prep Analysis I Date Method Method Solids,percent 83.1 % 7/8/99 SM2540G SM2540G I Organic Results Preservation Date: 7/7/99 DIESEL RANGE ORGANICS-SOIL Prep Method: Wi MOD DRO Prep Date: 7/7/99 Analyst: DJB IAnalysis Analysis Analyte Result EQL Units Code Date Method DIESEL RANGE ORGANICS < 4.7 4.7 mg/kg 7/7/99 Wi MOD DRO IBlank spike 102 --- %Recov 7/7/99 Wi MOD DRO Blank spike duplicate 89 -- %Recov 7/7/99 Wi MOD DRO I Blank < 5.0 5.0 mg/kg 7/7/99 Wi MOD DRO Organic Results GASOLINE RANGE ORGANICS-SOIL/METHANOL Prep Method: Wi MOD GRO Prep Date: 7/8/99 Analyst: MSB Analyte Result EQL Units Analysis Analysis Code Date Method Gasoline Range Organics < 3.0 3.0 mg/kg 7/8/99 Wi MOD GRO Blank Spike 105 --- %Recov 7/8/99 Wi MOD GRO IBlank Spike Duplicate 104 _ %Recov 7/8/99 Wi MOD GRO Blank < 2.5 2.5 mg/kg 7/8/99 Wi MOD GRO IOrganic Results MDH 465E VOLATILES-SOIL/METHANOL Prep Method: SW846 5030B Prep Date: 7/8/99 Analyst: RJN I Analyte Result EQL Units Analysis Analysis Code Date Method Acetone 180 150 ug/kg 7/8/99 SW846 82608 IAlly'Chloride < 30 30 ug/kg 7/8/99 SW846 8260B Benzene < 30 30 ug/kg 7/8/99 SW846 8260B IAll soil results are reported on a dry weight basis unless otherwise noted. • I 1795 Industrial Drive Green Bay,WI 54302 ` 920-469-2436 E' c:HEM 800-7-ENCHEM NC. Fnx 920-469-8827 y ux� >mce.......:.......,.,.,.,-.�.a m..............r ., ....�..».,» .,,. eAa ..vw.v,:...,,.,..b�..- «..,...,..., ,.-.-,..,.-.P..,,m.,«» �.. ,e...a.r.. ,..._�, ®..4-.......e.._o,. ,..,..A..., , .... -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS I/ Field ID: TP-7(0-T) Report Date: 7/9/99 Lab Sample Number: 893755-006 Collection Date: 7/2/99 1 MDH LAB ID: 055-999-334 Matrix Type: SOIL Bromochloromethane < 30 30 ug/kg 7/8/99 SW846 8260B Bromodichloromethane < 30 30 ug/kg 7/8/99 SW846 8260B Bromoform < 30 30 ug/kg 7/8/99 SW846 8260B Bromobenzene < 30 30 ug/kg 7/8/99 SW846 8260B Bromomethane < 30 30 ug/kg 7/8/99 SW846 8260B 2-Butanone < 150 150 ug/kg 7/8/99 SW846 8260B s-Butylbenzene < 30 30 ug/kg 7/8/99 SW846 8260B t-Butylbenzene < 30 30 ug/kg 7/8/99 SW846 8260B n-Butylbenzene < 30 30 ug/kg 7/8/99 SW846 8260B Carbon tetrachloride < 30 30 ug/kg 7/8/99 SW846 8260B Chloroform < 30 30 ug/kg 7/8/99 SW846 8260B Chlorobenzene < 30 30 ug/kg 7/8/99 SW846 8260B Chlorodibromomethane < 30 30 ug/kg 7/8/99 SW846 8260B Chloroethane < 30 30 ug/kg 7/8/99 SW846 8260B Chloromethane < 30 30 ug/kg 7/8/99 SW846 8260B 2-Chlorotoluene < 30 30 ug/kg 7/8/99 SW846 8260B 4-Chlorotoluene < 30 30 ug/kg 7/8/99 SW846 8260B I 1,2-Dibromo-3-chloropropane < 30 30 ug/kg 7/8/99 SW846 8260B 1,2-Dibromoethane < 30 30 ug/kg 7/8/99 SW846 8260B Dibromomethane < 30 30 ug/kg 7/8/99 SW846 8260B 1,3-Dichlorobenzene < 30 30 ug/kg 7/8/99 SW846 8260B 1,4-Dichlorobenzene < 30 30 ug/kg 7/8/99 SW846 8260B I 1,2-Dichloroethane < 30 30 ug/kg 7/8/99 SW846 8260B 1,2-Dichlorobenzene < 30 30 ug/kg 7/8/99 SW846 8260B 1,1-Dichloroethene < 30 30 ug/kg 7/8/99 SW846 8260B cis-1,2-Dichloroethene < 30 30 ug/kg 7/8/99 SW846 8260B Dichlorodifluoromethane < 30 30 ug/kg 7/8/99 SW846 8260B trans-1,2-Dichloroethene < 30 30 ug/kg 7/8/99 SW846 8260B Dichlorofluoromethane < 30 30 ug/kg 7/8/99 SW846 8260B 1,2-Dichloropropane < 30 30 ug/kg 7/8/99 SW846 8260B 1,1-Dichloroethane < 30 30 ug/kg 7/8/99 SW846 8260B 1,3-Dichloropropane < 30 30 ug/kg 7/8/99 SW846 8260B All soil results are reported on a dry weight basis unless otherwise noted. I I 1795 Industrial Drive ', Green Bay,WI 54302 R H FiM 800-7-ENCHEM IINC FAx 920-469-8827 I -Analytical Report - Project Name: SENIOR HOUSING ADD. 1 Project Number: 7735-B Client: GME CONSULTANTS Field ID: TP-7(0-2') Report Date: 7/9/99 ILab Sample Number: 893755-006 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL I2,2-Dichloropropane < 30 30 ug/kg 7/8/99 SW846 8260B 1,1-Dichloropropene < 30 30 ug/kg 7/8/99 SW846 8260B I cis-1,3-Dichloropropene < 30 30 ug/kg 7/8/99 SW846 82606 trans-1,3-Dichloropropene < 30 30 ug/kg 7/8/99 SW846 8260B Ethylbenzene < 30 30 ug/kg 7/8/99 SW846 8260B I Diethyl ether < 150 150 ug/kg 7/8/99 SW846 82608 Fluorotrichloromethane < 30 30 ug/kg 7/8/99 SW846 82608 Hexachlorobutadiene < 30 30 ug/kg 7/8/99 SW846 8260B 1 Isopropylbenzene < 30 30 ug/kg 7/8/99 SW846 8260B p-Isopropyltoluene < 30 30 ug/kg 7/8/99 SW846 8260B I Methylene chloride < 30 30 ug/kg 7/8/99 SW846 82608 4-Methyl-2-pentanone < 150 150 ug/kg 7/8/99 SW846 8260B Methyl-tert-butyl-ether < 30 30 ug/kg 7/8/99 SW846 8260B I Naphthalene < 30 30 ug/kg 7/8/99 SW846 82608 n-Propylbenzene < 30 30 ug/kg 7/8/99 SW846 8260B Styrene < 30 30 ug/kg 7/8/99 SW846 8260B I1,1,2,2-Tetrachloroethane < 30 30 ug/kg 7/8/99 SW846 8260B 1,1,1,2-Tetrachloroethane < 30 30 ug/kg 7/8/99 SW846 8260B Tetrachloroethene < 30 30 ug/kg 7/8/99 SW846 8260B IToluene < 30 30 ug/kg 7/8/99 SW846 82608 1,2,3-Trichlorobenzene < 30 30 ug/kg 7/8/99 SW846 8260B Ii,2,4-Trichlorobenzene < 30 30 ug/kg 7/8/99 SW846 82606 1,1,1-Trichloroethane < 30 30 ug/kg 7/8/99 SW846 8260B 1,1,2-Trichloroethane < 30 30 ug/kg 7/8/99 SW846 82608 I1,1,2-Trichlorotrifluoroethane < 30 30 ug/kg 7/8/99 SW846 82608 1,2,4-Trimethylbenzene < 30 30 ug/kg 7/8/99 SW846 8260B Trichloroethene < 30 30 ug/kg 7/8/99 SW846 8260B I1,2,3-Trichloropropane < 30 30 ug/kg 7/8/99 SW846 8260B Tetrahydrofuran < 150 150 ug/kg 7/8/99 SW846 8260B I 1,3,5-Trimethylbenzene < 30 30 ug/kg 7/8/99 SW846 82608 Vinyl chloride < 30 30 ug/kg 7/8/99 SW846 8260B Xylenes,-m,-p < 30 30 ug/kg 7/8/99 SW846 82608 IAll soil results are reported on a dry weight basis unless otherwise noted. I 1795 Industrial Drive Green Bay,WI 54302 920-469-2436 Ei -HEM 800-7-ENCHEM I NC. FAX: 920-469-8827 1 -Analytical Report - Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS 1 Field ID: TP-7(0-21 Report Date: 7/9/99 Lab Sample Number: 893755-006 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL Xylene,-o < 30 30 ug/kg 7/8/99 SW846 8260B 4-Bromofluorobenzene 109 -- %Recov 7/8/99 SW846 8260B Dibromofluoromethane 104 --- %Recov 7/8/99 SW846 8260B Toluene-d8 112 --- %Recov 7/8/99 SW846 8260B 1 1 1 1 1 1 1 i 1 1 All soil results are reported on a dry weight basis unless otherwise noted. 1 1 1795 Industrial Drive Green Bay, WI 54302 920-469-2436 E I H FiM 800-7-ENCHEM 1 NC. FAX: 920-469-8827 I'I I -Analytical Report - II Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS Field ID: TP-9(7') Report Date: 7/22/99 ILab Sample Number: 893755-007 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL IInorganic Results I Analysis Prep Analysis Test Result EQL Units Code Date Method Method Arsenic 1.9 1.1 mg/kg 7/14/99 SW846 3051 SW846 6010 Barium 49 0.56 mg/kg 7/14/99 SW846 3051 SW846 6010 I Cadmium < 0.11 0.11 mg/kg 7/14/99 SW846 3051 SW846 6010 Chromium 11 0.33 mg/kg 7/14/99 SW846 3051 SW846 6010 Lead 18 0.56 mg/kg 7/14/99 SW846 3051 SW846 6010 I Mercury 0.022 mg/kg 7/21/99 SW846 7471A SW846 7471 Selenium < 1.1 1.1 mg/kg 7/14/99 SW846 3051 SW846 6010 Silver < 0.56 0.56 mg/kg 7/13/99 SW846 3050B SW846 6010 ISolids,percent 89.9 % 7/8/99 SM2540G SM2540G Organic Results 1 PAH-SEMIVOLATILES Prep Method: SW846 3550 Prep Date: 7/8/99 Analyst: NJS Result Analysis Analysis I Analyte EQL Units Code Date Method Acenaphthene < 56 56 ug/kg 7/9/99 SW846 8270 Acenaphthylene < 56 56 ug/kg 7/9/99 SW846 8270 IAnthracene < 56 56 ug/kg 7/9/99 SW846 8270 Benzo(a)anthracene < 56 56 ug/kg 7/9/99 SW846 8270 I Benzo(a)pyrene 66 56 ug/kg 7/9/99 SW846 8270 Benzo(b)fluoranthene 63 56 ug/kg 7/9/99 SW846 8270 Benzo(g,h,i)perylene < 56 56 ug/kg 7/9/99 SW846 8270 I Benzo(k)fluoranthene < 56 56 ug/kg 7/9/99 SW846 8270 Chrysene 57 56 ug/kg 7/9/99 SW846 8270 Dibenzo(a,h)anthracene < 56 56 ug/kg 7/9/99 SW846 8270 IFluoranthene 100 56 ug/kg 7/9/99 SW846 8270 Fluorene < 56 56 ug/kg 7/9/99 SW846 8270 Indeno(1,2,3-cd)pyrene < 56 56 ug/kg 7/9/99 SW846 8270 I1-Methylnaphthalene < 56 56 ug/kg 7/9/99 SW846 8270 2-Methylnaphthalene < 56 56 ug/kg 7/9/99 SW846 8270 All soil results are reported on a dry weight basis unless otherwise noted. 1795 Industrial Gre n Bays WI Drive 4302 920 469 2436 E i� 4, °HEM 800 7 ENCHEM INC. FAx 920-469-8827 -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS Field ID : TP-9(T) Report Date: 7/22/99 Lab Sample Number: 893755-007 Collection Date: 7/2/99 I MDH LAB ID : 055-999-334 Matrix Type: SOIL Naphthalene < 56 56 ug/kg 7/9/99 SW846 8270 I Phenanthrene < 56 56 ug/kg 7/9/99 SW846 8270 Pyrene 94 56 ug/kg 7/9/99 SW846 8270 I Nitrobenzene-d5 71 --- %Recov 7/9/99 SW846 8270 2-Fluorobiphenyl 82 -- %Recov 7/9/99 SW846 8270 Terphenyl-d14 87 -- %Recov 7/9/99 SW846 8270 I I I I I III I I I All soil results are reported on a dry weight basis unless otherwise noted. I A I 1795 Industrial Drive Green Bay,WI 54302 920-469-2436 Ei HEM 800-7-ENCHEM INC FAx 920-469 8827 I -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS Field ID: TP-10(2') Report Date: 7/8/99 ILab Sample Number: 893755-008 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL llInorganic Results I Analysis Prep Analysis Test Result EQL Units Code Date Method Method Solids,percent 88.9 % 7/8/99 SM2540G SM2540G I Organic Results Preservation Date: 7/7/99 DIESEL RANGE ORGANICS-SOIL Prep Method: Wi MOD DRO Prep Date: 7/7/99 Analyst: DJB IAnalyte Result EQL Units Code Analysis Analysis Date Method I DIESEL RANGE ORGANICS 4.9 4.4 mg/kg 7/7/99 Wi MOD DRO Blank spike 102 %Recov 7/7/99 Wi MOD DRO Blank spike duplicate 89 --- %Recov 7/7/99 Wi MOD DRO IBlank < 5.0 5.0 mg/kg 7/7/99 Wi MOD DRO I I I I I I All soil results are reported on a dry weight basis unless otherwise noted. I 1795 Industrial Drive Green Bay,WI 54302 92y0,Z -2436 E HEM 800 7 ENCHEM '"'" I N C Fnx 920-469-8827 -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS Field ID: TP-12(6') Report Date: 7/9/99 Lab Sample Number: 893755-009 Collection Date: 7/2/99 I MDH LAB ID: 055-999-334 Matrix Type: SOIL Inorganic Results I Analysis Prep Analysis I Test Result EQL Units Code Date Method Method Solids,percent 85.8 % 7/8/99 SM2540G SM2540G Organic Results I Preservation Date: 7/7/99 DIESEL RANGE ORGANICS-SOIL Prep Method: Wi MOD DRO Prep Date: 7/7/99 Analyst: DJB Result Analysis Analysis 111 Analyte EQL Units Code Date Method DIESEL RANGE ORGANICS < 4.9 4.9 mg/kg 7/7/99 Wi MOD DRO IBlank spike 102 -- %Recov 7/7/99 Wi MOD DRO Blank spike duplicate 89 -- %Recov 7/7/99 Wi MOD DRO Blank < 5.0 5.0 mg/kg 7/7/99 Wi MOD DRO I Organic Results GASOLINE RANGE ORGANICS-SOIL/METHANOL Prep Method: Wi MOD GRO Prep Date: 7/8/99 Analyst: MSB I Result Analysis Analysis Analyte EQL Units Code Date Method I Gasoline Range Organics < 2.9 2.9 mg/kg 7/8/99 Wi MOD GRO Blank Spike 105 — %Recov 7/8/99 Wi MOD GRO Blank Spike Duplicate 104 --- %Recov 7/8/99 Wi MOD GRO I Blank < 2.5 2.5 mg/kg 7/8/99 Wi MOD GRO Organic Results I MDH 465E VOLATILES-SOIL/METHANOL Prep Method: SW846 5030B Prep Date: 7/8/99 Analyst: RJN Analysis Analysis I Analyte Result EQL Units Code Date Method Acetone < 150 150 ug/kg 7/8/99 SW846 8260B Ally!Chloride < 29 29 ug/kg 7/8/99 SW846 8260B I Benzene < 29 29 ug/kg 7/8/99 SW846 8260B All soil results are reported on a dry weight basis unless otherwise noted. I I1795 Industrial Drive Green Bay,WI 54302 920-469-2436 E A HFiM 800-7-ENCHEM �o Frvc: 920-469-8827 __":L___________._____ I -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-8 Client: GME CONSULTANTS Field ID: TP-12(6') Report Date: 7/9/99 ILab Sample Number: 893755-009 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL 1 Bromochloromethane < 29 29 ug/kg 7/8/99 SW846 8260B Bromodichloromethane < 29 29 ug/kg 7/8/99 SW846 8260B I Bromoform < 29 29 ug/kg 7/8/99 SW846 82608 Bromobenzene < 29 29 ug/kg 7/8/99 SW846 8260B Bromomethane < 29 29 ug/kg 7/8/99 SW846 8260B I2-Butanone < 150 150 ug/kg 7/8/99 SW846 82606 s-Butylbenzene < 29 29 ug/kg 7/8/99 SW846 8260B t-Butylbenzene < 29 29 ug/kg 7/8/99 SW846 8260B In-Butylbenzene < 29 29 ug/kg 7/8/99 SW846 8260B Carbon tetrachloride < 29 29 ug/kg 7/8/99 SW846 8260B Chloroform < 29 29 ug/kg 7/8/99 SW846 82606 Chlorobenzene < 29 29 ug/kg 7/8/99 SW846 8260B Chlorodibromomethane < 29 29 ug/kg 7/8/99 SW846 8260B ' Chloroethane < 29 29 ug/kg 7/8/99 SW846 82608 Chloromethane < 29 29 ug/kg 7/8/99 SW846 8260B 2-Chlorotoluene < 29 29 ug/kg 7/8/99 SW846 8260B I4-Chlorotoluene < 29 29 ug/kg 7/8/99 SW846 8260B 1,2-Dibromo-3-chloropropane < 29 29 ug/kg 7/8/99 SW846 8260B Ii 2-Dibromoethane < 29 29 ug/kg 7/8/99 SW846 82608 Dibromomethane < 29 29 ug/kg 7/8/99 SW846 8260B 1,3-Dichlorobenzene < 29 29 ug/kg 7/8/99 SW846 8260B Il,4-Dichlorobenzene < 29 29 ug/kg 7/8/99 SW846 82606 1,2-Dichloroethane < 29 29 ug/kg 7/8/99 SW846 8260B 1,2-Dichlorobenzene < 29 29 ug/kg 7/8/99 SW846 8260B I1,1-Dichloroethene < 29 29 ug/kg 7/8/99 SW846 8260B cis-1,2-Dichloroethene < 29 29 ug/kg 7/8/99 SW846 8260B I Dichlorodifluoromethane < 29 29 ug/kg 7/8/99 SW846 8260B trans-1,2-Dichloroethene < 29 29 ug/kg 7/8/99 SW846 82608 Dichlorofluoromethane < 29 29 ug/kg 7/8/99 SW846 8260B Il 2-Dichloropropane < 29 29 ug/kg 7/8/99 SW846 82606 1,1-Dichloroethane < 29 29 ug/kg 7/8/99 SW846 8260B 1,3-Dichloropropane < 29 29 ug/kg 7/8/99 SW846 8260B IAll soil results are reported on a dry weight basis unless otherwise noted. 1795 Industrial Drive I Green Bay,WI 54302 920-469-2436 E' -HEM A A 800 7 ENCHEM �rrc. FAx 920-469-8827 m -Analytical Report- I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS Field ID: TP-12(6') Report Date: 7/9/99 Lab Sample Number: 893755-009 Collection Date: 7/2/99 I MDH LAB ID: 055-999-334 Matrix Type: SOIL 2,2-Dichloropropane < 29 29 ug/kg 7/8/99 SW846 8260B t 1 1-Dichloro ro ene < 29 29 ug/kg 7/8/99 SW846 P P 9 9 8 6 82608 cis-1,3-Dichloropropene < 29 29 ug/kg 7/8/99 SW846 8260B trans-1,3-Dichloropropene < 29 29 ug/kg 7/8/99 SW846 8260B Ethylbenzene < 29 29 ug/kg 7/8/99 SW846 8260B Diethyl ether < 150 150 ug/kg 7/8/99 SW846 8260B I Fluorotrichloromethane < 29 29 ug/kg 7/8/99 SW846 8260B Hexachlorobutadiene < 29 29 ug/kg 7/8/99 SW846 8260B Isopropylbenzene < 29 29 ug/kg 7/8/99 SW846 8260B I p-Isopropyltoluene < 29 29 ug/kg 7/8/99 SW846 8260B Methylene chloride < 29 29 ug/kg 7/8/99 SW846 8260B I 4-Methyl-2-pentanone < 150 150 ug/kg 7/8/99 SW846 8260B Meth l-tert-but l-ether < 29 7/ / 29 ug/kg 8 99 SW846 8260B Y Y 9 9 Naphthalene < 29 29 ug/kg 7/8/99 SW846 8260B I n-Propylbenzene < 29 29 ug/kg 7/8/99 SW846 8260B Styrene < 29 29 ug/kg 7/8/99 SW846 8260B 1,1,2,2-Tetrachloroethane < 29 29 ug/kg 7/8/99 SW846 8260B 1,1,1,2-Tetrachloroethane < 29 29 ug/kg 7/8/99 SW846 8260B Tetrachloroethene < 29 29 ug/kg 7/8/99 SW846 8260B I Toluene < 29 29 ug/kg 7/8/99 SW846 8260B 1,2,3-Trichlorobenzene < 29 29 ug/kg 7/8/99 SW846 8260B 1,2,4-Trichlorobenzene < 29 29 ug/kg 7/8/99 SW846 82606 1,1,1-Trichloroethane < 29 29 ug/kg 7/8/99 SW846 8260B 1,1,2-Trichloroethane < 29 29 ug/kg 7/8/99 SW846 82606 1,1,2-Trichlorotrifluoroethane < 29 29 ug/kg 7/8/99 SW846 8260B 1,2,4-Trimethylbenzene < 29 29 ug/kg 7/8/99 SW846 8260B Trichloroethene < 29 29 ug/kg 7/8/99 SW846 8260B 1,2,3-Trichloropropane < 29 29 ug/kg 7/8/99 SW846 8260B Tetrahydrofuran < 150 150 ug/kg 7/8/99 SW846 82606 1,3,5-Trimethylbenzene < 29 29 ug/kg 7/8/99 SW846 8260B I Vinyl chloride < 29 29 ug/kg 7/8/99 SW846 8260B Xylenes,-m,-p < 29 29 ug/kg 7/8/99 SW846 8260B All soil results are reported on a dry weight basis unless otherwise noted. I I1795 Industrial Drive Green Bay,WI 54302 �_E HEM 920-469-2436 800-7-ENCHEM INC. Fex: 920-469-8827 I -Analytical Report- Project Name: SENIOR HOUSING ADD. IProject Number: 7735-B Client: GME CONSULTANTS Field ID: TP-12(6) Report Date: 7/9/99 ILab Sample Number: 893755-009 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL Xylene,-o < 29 29 ug/kg 7/8/99 SW846 8260B 4-Bromofluorobenzene 93 --- %Recov 7/8/99 SW846 8260B I Dibromofluoromethane 92 %Recov 7/8/99 SW846 8260B Toluene-d8 98 %Recov 7/8/99 SW846 8260B I I I I I I I I I I IAll soil results are reported on a dry weight basis unless otherwise noted. 1795 Industrial Drive Green Bay, WI 54302 920-469-2436 1 E� AHEM 800 7 ENCHEM INC FAx 920-469-8827 III 024 315131,(9101.ADA8M -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS 1 Field ID: TP-13(0-4') Report Date: 7/9/99 Lab Sample Number: 893755-010 Collection Date: 7/2/99 1 MDH LAB ID: 055-999-334 Matrix Type: SOIL Inorganic Results I Analysis Prep Analysis Test Result EQL Units Code Date Method Method Solids,percent 90.6 % 7/8/99 SM2540G SM2540G Organic Results ' Preservation Date: 7/7/99 DIESEL RANGE ORGANICS-SOIL Prep Method: Wi MOD DRO Prep Date: 7/7/99 Analyst: DJB Result Analysis Analysis I Analyte EQL Units Code Date Method DIESEL RANGE ORGANICS 58 4.2 mg/kg 7/7/99 Wi MOD DRO Blank spike 102 — %Recov 7/7/99 Wi MOD DRO I Blank spike duplicate 89 — %Recov 7/7/99 Wi MOD DRO Blank < 5.0 5.0 mg/kg 7/7/99 Wi MOD DRO Organic Results GASOLINE RANGE ORGANICS-SOIL/METHANOL Prep Method: Wi MOD GRO Prep Date: 7/8/99 Analyst: MSB I Analyte Result EQL Units Code Analysis Analysis Date Method I Gasoline Range Organics < 2.8 2.8 mg/kg 7/8/99 Wi MOD GRO Blank Spike 105 — %Recov 7/8/99 Wi MOD GRO Blank Spike Duplicate 104 — %Recov 7/8/99 Wi MOD GRO I Blank < 2.5 2.5 mg/kg 7/8/99 Wi MOD GRO Organic Results MDH 465E VOLATILES-SOIL/METHANOL Prep Method: SW846 5030B Prep Date: 7/8/99 Analyst: RJN Analyte Result EQL Units Code Analysis Analysis I Date Method d Acetone 170 140 ug/kg 7/8/99 SW846 8260B Ally!Chloride < 28 28 ug/kg 7/8/99 SW846 8260B I Benzene < 28 28 ug/kg 7/8/99 SW846 8260B All soil results are reported on a dry weight basis unless otherwise noted. I I I1795 Industrial Drive ilk �� Green Bay, WI 54302 920 469 2436 Fil HEM 800-7-ENCHEM a NC. FAx 920-469-8827 I -Analytical Report - Project Name: SENIOR HOUSING ADD. IProject Number: 7735-B Client: GME CONSULTANTS Field ID: TP-13(0-4') Report Date: 7/9/99 ILab Sample Number: 893755-010 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL 1 Bromochloromethane < 28 28 ug/kg 7/8/99 SW846 8260B Bromodichloromethane < 28 28 ug/kg 7/8/99 SW846 8260B I Bromoform < 28 28 ug/kg 7/8/99 SW846 8260B Bromobenzene < 28 28 ug/kg 7/8/99 SW846 8260B Bromomethane < 28 28 ug/kg 7/8/99 SW846 8260B I2-Butanone < 140 140 ug/kg 7/8/99 SW846 8260B s-Butylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B t-Butylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B In-Butylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B Carbon tetrachloride < 28 28 ug/kg 7/8/99 SW846 8260B I Chloroform < 28 28 ug/kg 7/8/99 SW846 82606 Chlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B Chlorodibromomethane < 28 28 ug/kg 7/8/99 SW846 8260B I Chloroethane < 28 28 ug/kg 7/8/99 SW846 8260B Chloromethane < 28 28 ug/kg 7/8/99 SW846 8260B 2-Chlorotoluene < 28 28 ug/kg 7/8/99 SW846 8260B I4-Chlorotoluene < 28 28 ug/kg 7/8/99 SW846 8260B 1,2-Dibromo-3-chloropropane < 28 28 ug/kg 7/8/99 SW846 8260B Il,2-Dibromoethane < 28 28 ug/kg 7/8/99 SW846 8260B Dibromomethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,3-Dichlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B Il,4-Dichlorobenzene < 28 28 ug/kg 7/8/99 SW846 82606 1,2-Dichloroethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,2-Dichlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B I1,1-Dichloroethene < 28 28 ug/kg 7/8/99 SW846 8260B cis-1,2-Dichloroethene < 28 28 ug/kg 7/8/99 SW846 8260B Dichlorodifluoromethane < 28 28 ug/kg 7/8/99 SW846 8260B Itrans-1,2-Dichloroethene < 28 28 ug/kg 7/8/99 SW846 8260B Dichlorofluoromethane < 28 28 ug/kg 7/8/99 SW846 8260B Ii,2-Dichloropropane < 28 28 ug/kg 7/8/99 SW846 8260B 1,1-Dichloroethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,3-Dichloropropane < 28 28 ug/kg 7/8/99 SW846 8260B IAll soil results are reported on a dry weight basis unless otherwise noted. 1795 Industrial Drive Green Bay,WI 54302 Ss 920-469-2436 E H EM 800 7 ENCHEM INC. I Fnx 920-469-8827 . -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS I Field ID: TP-13(0-4') Report Date: 7/9/99 I Lab Sample Number: 893755-010 Collection Date: 7/2/99 1 MDH LAB ID: 055-999-334 Matrix Type: SOIL 2,2-Dichloropropane < 28 28 ug/kg 7/8/99 SW846 8260B I 1,1-Dichloropropene < 28 28 ug/kg 7/8/99 SW846 8260B cis-1,3-Dichloropropene < 28 28 ug/kg 7/8/99 SW846 8260B trans-1,3-Dichloropropene < 28 28 ug/kg 7/8/99 SW846 8260B Ethylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B Diethyl ether < 140 140 ug/kg 7/8/99 SW846 8260B ' Fluorotrichloromethane < 28 28 ug/kg 7/8/99 SW846 8260B Hexachlorobutadiene < 28 28 ug/kg 7/8/99 SW846 8260B lsopropylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B I p-lsopropyltoluene < 28 28 ug/kg 7/8/99 SW846 8260B Methylene chloride < 28 28 ug/kg 7/8/99 SW846 8260B 4-Methyl-2-pentanone < 140 140 ug/kg 7/8/99 SW846 8260B I Methyl-tert-butyl-ether < 28 28 ug/kg 7/8/99 SW846 8260B Naphthalene < 28 28 ug/kg 7/8/99 SW846 8260B n-Propylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B Styrene < 28 28 ug/kg 7/8/99 SW846 8260B 1,1,2,2-Tetrachloroethane < 28 28 ug/kg 7/8/99 SW846 8260B , 1,1,1,2-Tetrachloroethane < 28 28 ug/kg 7/8/99 SW846 8260B Tetrachloroethene < 28 28 ug/kg 7/8/99 SW846 8260B IToluene < 28 28 ug/kg 7/8/99 SW846 8260B 1,2,3-Trichlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B 1,2,4-Trichlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B 1,1,1-Trichloroethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,1,2-Trichloroethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,1,2-Trichlorotrifluoroethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,2,4-Trimethylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B Trichloroethene < 28 28 ug/kg 7/8/99 SW846 8260B 1,2,3-Trichloropropane < 28 28 ug/kg 7/8/99 SW846 8260B I Tetrahydrofuran < 140 140 ug/kg 7/8/99 SW846 8260B 1,3,5-Trimethylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B 111 Vinyl chloride < 28 28 ug/kg 7/8/99 SW846 8260B Xylenes,-m,-p < 28 28 ug/kg 7/8/99 SW846 8260B All soil results are reported on a dry weight basis unless otherwise noted. I I � 1795 Industrial Drive °� Green Bay,WI 54302 Fi HEM 920-469-2436 I I 800-7-ENCHEM 11111 ' NC. FAx: 920-469-8827 I -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS Field ID: TP-13(0-4') Report Date: 7/9/99 Lab Sample Number: 893755-010 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL IXylene,-o < 28 28 ug/kg 7/8/99 SW846 8260B 4-Bromofluorobenzene 108 --- %Recov 7/8/99 SW846 8260B I Dibromofluoromethane 103 %Recov 7/8/99 SW846 8260B Toluene-d8 110 %Recov 7/8/99 SW846 82608 I I I I I I I I I I IAll soil results are reported on a dry weight basis unless otherwise noted. 1795 Industrial Drive Green Bay,WI 54302 920-469-2436 E 4 '. HEM 800-7-ENCHEM INC Fnx 920-469-8827 -Analytical Report- I Project Name: SENIOR HOUSING ADD. I Project Number: 7735-B Client: GME CONSULTANTS Field ID: TP-13(4-6') Report Date: 7/9/99 Lab Sample Number: 893755-011 Collection Date: 7/2/99 1 MDH LAB ID: 055-999-334 Matrix Type: SOIL Inorganic Results I Analysis Prep Analysis Test Result EQL Units Code Date Method Method I Solids,percent 88.4 % 7/8/99 SM2540G SM2540G Organic Results I Preservation Date: 7/7/99 DIESEL RANGE ORGANICS-SOIL Prep Method: Wi MOD DRO Prep Date: 7/7/99 Analyst: DJB Analysis Analysis I Analyte Result EQL Units Code Date Method DIESEL RANGE ORGANICS < 4.4 4.4 mg/kg 7/7/99 Wi MOD DRO IBlank spike 102 -- %Recov 7/7/99 Wi MOD DRO Blank spike duplicate 89 — %Recov 7/7/99 Wi MOD DRO Blank < 5.0 5.0 mg/kg 7/7/99 Wi MOD DRO Organic Results GASOLINE RANGE ORGANICS-SOIL/METHANOL Prep Method: Wi MOD GRO Prep Date: 7/8/99 Analyst: MSB I Result Analysis Analysis Analyte EQL Units Code Date Method Gasoline Range Organics < 2.8 2.8 mg/kg 7/8/99 Wi MOD GRO I Blank Spike 105 --- %Recov 7/8/99 Wi MOD GRO Blank Spike Duplicate 104 -- %Recov 7/8/99 Wi MOD GRO Blank < 2.5 2.5 mg/kg 7/8/99 Wi MOD GRO Organic Results MDH 465E VOLATILES-SOIL/METHANOL Prep Method: SW846 5030B Prep Date: 7/8/99 Analyst: RJN Analysis Analysis Analyte Result EQL Units Code Date Method / I Acetone < 140 140 ug/kg 7/8/99 SW846 8260B Allyl Chloride < 28 28 ug/kg 7/8/99 SW846 8260B I Benzene < 28 28 ug/kg 7/8/99 SW846 8260B All soil results are reported on a dry weight basis unless otherwise noted. I I I I "r 1795 Industrial Drive• 1, Green Bay, WI 54302 �j l l�� l��T 920-469-2436 1 1 l�l 800-7-ENCHEM .. INC. FAX 920-469-8827 I -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS Field ID: TP-13(4-61 Report Date: 7/9/99 ILab Sample Number: 893755-011 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL IBromochloromethane < 28 28 ug/kg 7/8/99 SW846 8260B Bromodichloromethane < 28 28 ug/kg 7/8/99 SW846 8260B I Bromoform < 28 28 ug/kg 7/8/99 SW846 82608 Bromobenzene < 28 28 ug/kg 7/8/99 SW846 8260B Bromomethane < 28 28 ug/kg 7/8/99 SW846 82608 I2-Butanone < 140 140 ug/kg 7/8/99 SW846 82606 s-Butylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B t-Butylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B I n-Butylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B Carbon tetrachloride < 28 28 ug/kg 7/8/99 SW846 8260B I Chloroform < 28 28 ug/kg 7/8/99 SW846 82606 Chlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B Chlorodibromomethane < 28 28 ug/kg 7/8/99 SW846 8260B IChloroethane < 28 28 ug/kg 7/8/99 SW846 82606 Chloromethane < 28 28 ug/kg 7/8/99 SW846 8260B 2-Chlorotoluene < 28 28 ug/kg 7/8/99 SW846 8260B I4-Chlorotoluene < 28 28 ug/kg 7/8/99 SW846 8260B 1,2-Dibromo-3-chloropropane < 28 28 ug/kg 7/8/99 SW846 8260B Il,2-Dibromoethane < 28 28 ug/kg 7/8/99 SW846 82608 Dibromomethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,3-Dichlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B 1,4-Dichlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B 1,2-Dichloroethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,2-Dichlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B I1,1-Dichloroethene < 28 28 ug/kg 7/8/99 SW846 82606 cis-1,2-Dichloroethene < 28 28 ug/kg 7/8/99 SW8468260B I Dichlorodifluoromethane < 28 28 ug/kg 7/8/99 SW846 8260B trans-1,2-Dichloroethene < 28 28 ug/kg 7/8/99 SW846 8260B Dichlorofluoromethane < 28 28 ug/kg 7/8/99 SW846 8260B Ii,2-Dichloropropane < 28 28 ug/kg 7/8/99 SW846 82608 1,1-Dichloroethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,3-Dichloropropane < 28 28 ug/kg 7/8/99 SW846 8260B 1 All soil results are reported on a dry weight basis unless otherwise noted. I 1795 Industrial Drive Green Bay, WI 54302 920-469-2436 EIL, 9 HE,M 800 7 ENCHEM � I NC FAx 92069-8827 4 -Analytical Report- I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS I Field ID: TP-13(4-6') Report Date: 7/9/99 Lab Sample Number: 893755-011 Collection Date: 7/2/99 1 MDH LAB ID: 055-999-334 Matrix Type: SOIL 2,2-Dichloropropane < 28 28 ug/kg 7/8/99 SW846 8260B I 1,1-Dichloropropene < 28 28 ug/kg 7/8/99 SW846 8260B cis-1,3-Dichloropropene < 28 28 ug/kg 7/8/99 SW846 8260B trans-1,3-Dichloropropene < 28 28 ug/kg 7/8/99 SW846 8260B Ethylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B Diethyl ether < 140 140 ug/kg 7/8/99 SW846 8260B I Fluorotrichloromethane < 28 28 ug/kg 7/8/99 SW846 8260B Hexachlorobutadiene < 28 28 ug/kg 7/8/99 SW846 8260B Isopropylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B I p-Isopropyltoluene < 28 28 ug/kg 7/8/99 SW846 8260B Methylene chloride < 28 28 ug/kg 7/8/99 SW846 8260B 4-Methyl-2-pentanone < 140 140 ug/kg 7/8/99 SW846 8260B Methyl-tert-butyl-ether < 28 28 ug/kg 7/8/99 SW846 8260B Naphthalene < 28 28 ug/kg 7/8/99 SW846 8260B I n-Propylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B Styrene < 28 28 ug/kg 7/8/99 SW846 8260B II1,1,2,2-Tetrachloroethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,1,1,2-Tetrachloroethane < 28 28 ug/kg 7/8/99 SW846 8260B Tetrachloroethene < 28 28 ug/kg 7/8/99 SW846 8260B Toluene < 28 28 ug/kg 7/8/99 SW846 8260B 1,2,3-Trichlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B 1,2,4-Trichlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B I 1,1,1-Trichloroethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,1,2-Trichloroethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,1,2-Trichiorotrifluoroethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,2,4-Trimethylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B Trichloroethene < 28 28 ug/kg 7/8/99 SW846 8260B 111 1,2,3-Trichloropropane < 28 28 ug/kg 7/8/99 SW846 8260B Tetrahydrofuran < 140 140 ug/kg 7/8/99 SW846 8260B 1,3,5-Trimethylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B Vinyl chloride < 28 28 ug/kg 7/8/99 SW846 8260B Xylenes,-m,-p < 28 28 ug/kg 7/8/99 SW846 8260B All soil results are reported on a dry weight basis unless otherwise noted. I I 1 5 : 1795 Industrial Drive Green Bay,WI 54302 1 E o H FPM 920-469-2436 800-7-ENCHEM irrc. FAx: 920-469-8827 I -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS Field ID: TP-13(4-6') Report Date: 7/9/99 iLab Sample Number: 893755-011 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL Xylene,-o < 28 28 ug/kg 7/8/99 SW846 8260B 4-Bromofluorobenzene 98 -- %Recov 7/8/99 SW846 8260B I Dibromofluoromethane 96 -- %Recov 7/8/99 SW846 8260B— Toluene-d8 102 %Recov 7/8/99 SW846 8260B I I I I I I I 1 I I IAll soil results are reported on a dry weight basis unless otherwise noted. 1795 Industrial Drive Green Bay, WI 54302 E1 ,HEM 800-07-ENCHEM i NC FAx 920 469 8827 -Analytical Report - I Project Name: SENIOR HOUSING ADD. I Project Number: 7735-B Client: GME CONSULTANTS Field ID: TP-14(6') Report Date: 7/9/99 Lab Sample Number: 893755-012 Collection Date: 7/2/99 1 MDH LAB ID: 055-999-334 Matrix Type: SOIL Inorganic Results I Analysis Prep Analysis ITest Result EQL Units Code Date Method Method Solids,percent 87.9 % 7/8/99 SM2540G SM2540G Organic Results Preservation Date: 7/7/99 DIESEL RANGE ORGANICS-SOIL Prep Method: Wi MOD DRO Prep Date: 7/7/99 Analyst: DJB Analysis Analysis Analyte Result EQL Units Code Date Method DIESEL RANGE ORGANICS < 4.4 4.4 mg/kg 7/7/99 Wi MOD DRO Blank spike 102 — %Recov 7/7/99 Wi MOD DRO I Blank spike duplicate 89 — %Recov 7/7/99 Wi MOD DRO Blank < 5.0 5.0 mg/kg 7/7/99 Wi MOD DRO I Organic Results GASOLINE RANGE ORGANICS-SOIUMETHANOL Prep Method: Wi MOD GRO Prep Date: 7/8/99 Analyst: MSB I Analysis Analysis Result EQL Units Code Analyte Date Method Gasoline Range Organics < 2.8 2.8 mg/kg 7/9/99 Wi MOD GRO Blank Spike 105 --- %Recov 7/9/99 Wi MOD GRO Blank Spike Duplicate 104 -- %Recov 7/9/99 Wi MOD GRO Blank < 2.5 2.5 mg/kg 7/9/99 Wi MOD GRO Organic Results I MDH 465E VOLATILES-SOIUMETHANOL Prep Method: SW846 5030B Prep Date: 7/8/99 Analyst: RJN Analysis Analysis I Analyte Result EQL Units Code Date Method Acetone < 140 140 ug/kg 7/8/99 SW846 8260B Ally!Chloride < 28 28 ug/kg 7/8/99 SW846 8260B Benzene < 28 28 ug/kg 7/8/99 SW846 8260B All soil results are reported on a dry weight basis unless otherwise noted. I I1795 Industrial Drive Green Bay,WI 54302 EHEM 920-469-2436 INC. 800-7-ENCHEM FAx: 920-469-8827 I -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS Field ID: TP-14(6') Report Date: 7/9/99 ILab Sample Number: 893755-012 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL IBromochloromethane < 28 28 ug/kg 7/8/99 SW846 8260B Bromodichloromethane < 28 28 ug/kg 7/8/99 SW846 8260B I Bromoform < 28 28 ug/kg 7/8/99 SW846 82608 Bromobenzene < 28 28 ug/kg 7/8/99 SW846 8260B Bromomethane < 28 28 ug/kg 7/8/99 SW846 8260B 2-Butanone < 140 140 ug/kg 7/8/99 SW846 8260B s-Butylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B I t-Butylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B n-Butylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B Carbon tetrachloride < 28 28 ug/kg 7/8/99 SW846 8260B I Chloroform < 28 28 ug/kg 7/8/99 SW846 8260B Chlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B Chlorodibromomethane < 28 28 ug/kg 7/8/99 SW846 8260B IChloroethane < 28 28 ug/kg 7/8/99 SW846 8260B Chloromethane < 28 28 ug/kg 7/8/99 SW846 8260B 2-Chlorotoluene < 28 28 ug/kg 7/8/99 SW846 8260B I4-Chlorotoluene < 28 28 ug/kg 7/8/99 SW846 8260B 1,2-Dibromo-3-chloropropane < 28 28 ug/kg 7/8/99 SW846 8260B I 1,2-Dibromoethane < 28 28 ug/kg 7/8/99 SW846 8260B Dibromomethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,3-Dichlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B Il,4-Dichlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B 1,2-Dichloroethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,2-Dichlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B I1,1-Dichloroethene < 28 28 ug/kg 7/8/99 SW8468260B cis-1,2-Dichloroethene < 28 28 ug/kg 7/8/99 SW846 8260B I Dichlorodifluoromethane < 28 28 ug/kg 7/8/99 SW846 8260B trans-1,2-Dichloroethene < 28 28 ug/kg 7/8/99 SW846 8260B Dichlorofluoromethane < 28 28 ug/kg 7/8/99 SW846 8260B I 1,2-Dichloropropane < 28 28 ug/kg 7/8/99 SW846 8260B 1,1-Dichloroethane < 28 28 ug/kg 7/8/99 SW846 8260B 1 1,3-Dichloropropane < 28 28 ug/kg 7/8/99 SW846 8260B All soil results are reported on a dry weight basis unless otherwise noted. 1795 Industrial Drive Green Bay,WI 54302 920-469-2436 � E{ HEM 800-7-ENCHEM INC FAX 920 469 8827 I -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS Field ID: TP-14(61 Report Date: 7/9/99 Lab Sample Number: 893755-012 Collection Date: 7/2/99 I MDH LAB ID: 055-999-334 Matrix Type: SOIL 2,2-Dichloropropane < 28 28 ug/kg 7/8/99 SW846 8260B 1 1,1-Dichloropropene < 28 28 ug/kg 7/8/99 SW846 8260B cis-1,3-Dichloropropene < 28 28 ug/kg 7/8/99 SW846 8260B trans-1,3-Dichloropropene < 28 28 ug/kg 7/8/99 SW846 82608 Ethylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B Diethyl ether < 140 140 ug/kg 7/8/99 SW846 8260B I Fluorotrichloromethane < 28 28 ug/kg 7/8/99 SW846 8260B Hexachlorobutadiene < 28 28 ug/kg 7/8/99 SW846 8260B Isopropylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B III p-lsopropyltoluene < 28 28 ug/kg 7/8/99 SW846 8260B Methylene chloride < 28 28 ug/kg 7/8/99 SW846 8260B 4-Methyl-2-pentanone < 140 140 ug/kg 7/8/99 SW846 8260B Methyl-tert-butyl-ether < 28 28 ug/kg 7/8/99 SW846 8260B Naphthalene < 28 28 ug/kg 7/8/99 SW846 8260B n-Propylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B Styrene < 28 28 ug/kg 7/8/99 SW846 82606 1,1,2,2-Tetrachloroethane < 28 28 ug/kg 7/8/99 SW846 8260B I 1,1,1,2-Tetrachloroethane < 28 28 ug/kg 7/8/99 SW846 8260f3 Tetrachloroethene < 28 28 ug/kg 7/8/99 SW846 8260B Toluene < 28 28 ug/kg 7/8/99 SW846 8260B 1,2,3-Trichlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B 1,2,4-Trichlorobenzene < 28 28 ug/kg 7/8/99 SW846 8260B II 1,1,1-Trichloroethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,1,2-Trichloroethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,1,2-Trichlorotrifluoroethane < 28 28 ug/kg 7/8/99 SW846 8260B 1,2,4-Trimethylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B Trichloroethene < 28 28 ug/kg 7/8/99 SW846 8260B 111 1,2,3-Trichloropropane < 28 28 ug/kg 7/8/99 SW846 8260B Tetrahydrofuran < 140 140 ug/kg 7/8/99 SW846 8260B 1,3,5-Trimethylbenzene < 28 28 ug/kg 7/8/99 SW846 8260B Vinyl chloride < 28 28 ug/kg 7/8/99 SW846 8260B Xylenes,-m,-p < 28 28 ug/kg 7/8/99 SW846 8260B All soil results are reported on a dry weight basis unless otherwise noted. I I 1795 Industrial Drive Green Bay,WI 54302 E�. HEM 920-469-2436 I 0-7-ENCHEM INC. ,,.,ro \ � INC.NC. FAX: 920-469-8827 I -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS Field ID: TP-14(6') Report Date: 7/9/99 iLab Sample Number: 893755-012 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: SOIL iXylene,-o < 28 28 ug/kg 7/8/99 SW846 82606 4-Bromofluorobenzene 104 -- %Recov 7/8/99 SW846 8260B I Dibromofluoromethane 99.9 --- %Recov 7/8/99 SW846 8260B Toluene-d8 107 %Recov 7/8/99 SW846 8260B I I I I I i I I I I 1 All soil results are reported on a dry weight basis unless otherwise noted. i 1795 Industrial Drive Green Bay,WI 54302 920-469-2436 E AHEM 800 7 ENCHEM , INC. FAx: 920-469-8827 - Analytical Report- I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS Field ID: TB(SOIL) Report Date: 7/9/99 Lab Sample Number: 893755-013 Collection Date: 7/2/99 1 MDH LAB ID: 055-999-334 Matrix Type: METHANOL I Organic Results GASOLINE RANGE ORGANICS-METHANOL Prep Method: Wi MOD GRO Prep Date: 7/8/99 Analyst: MSB 1 Analysis Analysis Analyte Result EQL Units Code Date Method 1 Gasoline Range Organics < 2500 2500 ug/L 7/9/99 Wi MOD GRO Blank Spike 105 -- %Recov 7/9/99 Wi MOD GRO I Blank Spike Duplicate 104 — %Recov 7/9/99 Wi MOD GRO Blank < 50 50 ug/L 7/9/99 Wi MOD GRO Organic Results 1 MDH 465E VOLATILES-METHANOL Prep Method: SW846 5030B Prep Date: 7/8/99 Analyst: RJN Analysis Analysis Analyte Result EQL Units Code Date Method Acetone < 130 130 ug/L 7/8/99 SW846 8260B Allyl Chloride < 25 25 ug/L 7/8/99 SW846 8260B Benzene < 25 25 ug/L 7/8/99 SW846 8260B Bromochloromethane < 25 25 ug/L 7/8/99 SW846 8260B Bromodichloromethane < 25 25 ug/L 7/8/99 SW846 8260B Bromoform < 25 25 ug/L 7/8/99 SW846 8260B IBromobenzene < 25 25 ug/L 7/8/99 SW846 8260B Bromomethane < 25 25 ug/L 7/8/99 SW846 8260B 2-Butanone < 130 130 ug/L 7/8/99 SW846 8260B s-Butylbenzene < 25 25 ug/L 7/8/99 SW846 82608 t-Butylbenzene < 25 25 ug/L 7/8/99 SW846 8260B n-Butylbenzene < 25 25 ug/L 7/8/99 SW846 8260B II Carbon tetrachloride < 25 25 ug/L 7/8/99 SW846 8260B Chloroform < 25 25 ug/L 7/8/99 SW846 8260B Chlorobenzene < 25 25 ug/L 7/8/99 SW846 8260B I Chlorodibromomethane < 25 25 ug/L 7/8/99 SW846 8260B I I 1795 Industrial Drive Green Bay, WI 54302 E HEM 920-469-2436 INC. 800-7-ENCHEM II Fnx: 920-469 8827 I -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS Field ID: TB(SOIL) Report Date: 7/9/99 ILab Sample Number: 893755-013 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: METHANOL 1 Chloroethane < 25 25 ug/L 7/8/99 SW846 8260B Chloromethane < 25 25 ug/L 7/8/99 SW846 8260B I 2-Chlorotoluene < 25 25 ug/L 7/8/99 SW846 82608 4-Chlorotoluene < 25 25 ug/L 7/8/99 SW846 8260B 1,2-Dibromo-3-chloropropane < 25 25 ug/L 7/8/99 SW846 8260B II,2-Dibromoethane < 25 25 ug/L 7/8/99 SW846 82606 Dibromomethane < 25 25 ug/L 7/8/99 SW846 82608 I 1,3-Dichlorobenzene < 25 25 ug/L 7/8/99 SW846 8260B 1,4-Dichlorobenzene < 25 25 ug/L 7/8/99 SW846 8260B 1,2-Dichioroethane < 25 25 ug/L 7/8/99 SW846 8260B I 1,2-Dichlorobenzene < 25 25 ug/L 7/8/99 SW846 82606 1,1-Dichloroethene < 25 25 ug/L 7/8/99 SW846 8260B cis-1,2-Dichloroethene < 25 25 ug/L 7/8/99 SW846 8260B IDichlorodifluoromethane < 25 25 ug/L 7/8/99 SW846 82606 trans-1,2-Dichloroethene < 25 25 ug/L 7/8/99 SW846 8260B Dichlorofluoromethane < 25 25 ug/L 7/8/99 SW846 8260B I1,2-Dichloropropane < 25 25 ug/L 7/8/99 SW846 8260B 1,1-Dichioroethane < 25 25 ug/L 7/8/99 SW846 8260B Il,3-Dichloropropane < 25 25 ug/L 7/8/99 SW846 8260B 2,2-Dichloropropane < 25 25 ug/L 7/8/99 SW846 8260B 1,1-Dichloropropene < 25 25 ug/L 7/8/99 SW846 8260B Icis-1,3-Dichloropropene < 25 25 ug/L 7/8/99 SW846 82606 trans-1,3-Dichloropropene < 25 25 ug/L 7/8/99 SW846 8260B Ethylbenzene < 25 25 ug/L 7/8/99 SW846 8260B IDiethyl ether < 130 130 ug/L 7/8/99 SW846 8260B Fluorotrichloromethane < 25 25 ug/L 7/8/99 SW846 82608 I Hexachlorobutadiene < 25 25 ug/L 7/8/99 SW846 8260B Isopropylbenzene < 25 25 ug/L 7/8/99 SW846 8260B p-Isopropyltoluene < 25 25 ug/L 7/8/99 SW846 82608 I Methylene chloride < 25 25 ug/L 7/8/99 SW846 82608 4-Methyl-2-pentanone < 130 130 ug/L 7/8/99 SW846 8260B Methyl-tert-butyl-ether < 25 25 ug/L 7/8/99 SW846 8260B I 1795 Industrial Drive Green Bay, WI 54302 920-469-2436 E ri AHEM 800-7-ENCHEM INC. FAX: I920-469-8827 -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS Field ID: TB(SOIL) Report Date: 7/9/99 Lab Sample Number: 893755-013 Collection Date: 7/2/99 1 MDH LAB ID: 055-999-334 Matrix Type: METHANOL Naphthalene < 25 25 ug/L 7/8/99 SW846 8260B t n-Propylbenzene < 25 25 ug/L 7/8/99 SW846 8260B Styrene < 25 25 ug/L 7/8/99 SW846 8260B 1,1,2,2-Tetrachioroethane < 25 25 ug/L 7/8/99 SW846 8260B 1,1,1,2-Tetrachioroethane < 25 25 ug/L 7/8/99 SW846 8260B Tetrachloroethene < 25 25 ug/L 7/8/99 SW846 8260B Toluene < 25 25 ug/L 7/8/99 SW846 8260B 1,2,3-Trichlorobenzene < 25 25 ug/L 7/8/99 SW846 8260B I1,2,4-Trichlorobenzene < 25 25 ug/L 7/8/99 SW846 8260B 1,1,1-Trichloroethane < 25 25 ug/L 7/8/99 SW846 8260B 1,1,2-Trichloroethane < 25 25 ug/L 7/8/99 SW846 8260B 1,1,2-Trichlorotrifluoroethane < 25 25 ug/L 7/8/99 SW846 8260B 1,2,4-Trimethylbenzene < 25 25 ug/L 7/8/99 SW846 8260B Trichloroethene < 25 25 ug/L 7/8/99 SW846 8260B I 1,2,3-Trichloropropane < 25 25 ug/L 7/8/99 SW846 8260B Tetrahydrofuran < 130 130 ug/L 7/8/99 SW846 8260B 1,3,5-Trimethylbenzene < 25 25 ug/L 7/8/99 SW846 8260B I Vinyl chloride < 25 25 ug/L 7/8/99 SW846 8260B Xylenes,-m,-p < 25 25 ug/L 7/8/99 SW846 8260B Xylene,-o < 25 25 ug/L 7/8/99 SW846 8260B 4-Bromofluorobenzene 99 — %Recov 7/8/99 SW846 8260B Dibromofluoromethane 97 -- %Recov 7/8/99 SW846 8260B I Toluene-d8 97 -- %Recov 7/8/99 SW846 8260B I I 1 I I 1795 Industrial Drive Green Bay, WI 54302 E HE M 920-469-2436 I 800-7-ENCHEM ' t NC*.' FAX: 920-469-8827 I -Analytical Report - Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS Field ID: ST-1 Report Date: 7/14/99 ILab Sample Number: 893755-014 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: WATER 1 Organic Results IDIESEL RANGE ORGANICS-WATER Prep Method: Wi MOD DRO Prep Date: 7/7/99 Analyst: DJB i Analyte Result EQL Units Analysis Analysis Method Code Date DIESEL RANGE ORGANICS 490 100 ug/I 7/7/99 Wi MOD DRO I Blank spike 87 �- %Recov 7/7/99 Wi MOD DRO Blank spike duplicate 95 %Recov 7/7/99 Wi MOD DRO Blank < 50 50 ug/I 7/7/99 Wi MOD DRO IOrganic Results IGASOLINE RANGE ORGANICS-WATER Prep Method: Wi MOD GRO Prep Date: 7/9/99 Analyst: EGS EQL Analysis Analysis Analyte Result E Q Units Code Date Method I GASOLINE RANGE ORGANICS < 50 50 ug/I 7/13/99 Wi MOD GRO Blank Spike 97 %Recov 7/13/99 Wi MOD GRO Blank Spike Duplicate 98 --- %Recov 7/13/99 Wi MOD GRO IBlank < 50 50 ug/I 7/13/99 Wi MOD GRO Organic Results 1 MDH 465E VOLATILES-WATER Prep Method: SW846 5030B Prep Date: 7/12/99 Analyst: 11W Analyte Result EQL Units Analysis Analysis Code Date Method Acetone < 10 10 ug/L 7/12/99 SW846 8260B Allyl Chloride < 1.0 1.0 ug/L 7/12/99 SW846 8260B IBenzene < 1.0 1.0 ug/L 7/12/99 SW846 8260B Bromochloromethane < 1.0 1.0 ug/L 7/12/99 SW846 8260B I Bromodichloromethane < 1.0 1.0 ug/L 7/12/99 SW846 8260B Bromoform < 1.0 1.0 ug/L 7/12/99 SW846 8260B Bromobenzene < 1.0 1.0 ug/L 7/12/99 SW846 8260B I 1 1795 Industrial Drive Green Bay,WI 54302 920-469-2436 E � �HEM 800 7 ENCHEM iivc. FAx 920-469-8827 �M.� .. . ��.u,, � ���..��., a�.�a e.��a .� �,�. -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS I Field ID: ST-1 Report Date: 7/14/99 Lab Sample Number: 893755-014 Collection Date: 7/2/99 1 MDH LAB ID: 055-999-334 Matrix Type: WATER Bromomethane < 1.0 1.0 ug/L 7/12/99 SW846 8260B I 2-Butanone < 5.0 5.0 ug/L 7/12/99 SW846 8260B s-Butylbenzene < 1.0 1.0 ug/L 7/12/99 SW846 8260B t-Butylbenzene < 1.0 1.0 ug/L 7/12/99 SW846 8260B n-Butylbenzene < 1.0 1.0 ug/L 7/12/99 SW846 8260B Carbon tetrachloride < 1.0 1.0 ug/L 7/12/99 SW846 8260B Chloroform < 1.0 1.0 ug/L 7/12/99 SW846 8260B Chlorobenzene < 1.0 1.0 ug/L 7/12/99 SW846 8260B Chlorodibromomethane < 1.0 1.0 ug/L 7/12/99 SW846 8260B I Chloroethane < 1.0 1.0 ug/L 7/12/99 SW846 8260B Chloromethane < 1.0 1.0 ug/L 7/12/99 SW846 82606 2-Chlorotoluene < 1.0 1.0 ug/L 7/12/99 SW846 82608 4-Chlorotoluene < 1.0 1.0 ug/L 7/12/99 SW846 8260B 1,2-Dibromo-3-chloropropane < 1.0 1.0 ug/L 7/12/99 SW846 8260B II 1,2-Dibromoethane < 1.0 1.0 ug/L 7/12/99 SW846 8260B Dibromomethane < 1.0 1.0 ug/L 7/12/99 SW846 8260B 1,3-Dichlorobenzene < 1.0 1.0 ug/L 7/12/99 SW846 82606 1,4-Dichlorobenzene < 1.0 1.0 ug/L 7/12/99 SW846 82608 1,2-Dichloroethane < 1.0 1.0 ug/L 7/12/99 SW846 82608 1,2-Dichlorobenzene < 1.0 1.0 ug/L 7/12/99 SW846 8260B 1,1-Dichloroethene < 1.0 1.0 ug/L 7/12/99 SW846 82608 cis-1,2-Dichloroethene < 1.0 1.0 ug/L 7/12/99 SW846 8260B Dichlorodifluoromethane < 1.0 1.0 ug/L 7/12/99 SW846 8260B trans-1,2-Dichloroethene < 1.0 1.0 ug/L 7/12/99 SW846 8260B Dichlorofluoromethane < 1.0 1.0 ug/L 7/12/99 SW846 82608 1,2-Dichloropropane < 1.0 1.0 ug/L 7/12/99 SW846 8260B 1,1-Dichloroethane < 1.0 1.0 ug/L 7/12/99 SW846 8260B 1,3-Dichloropropane < 1.0 1.0 ug/L 7/12/99 SW846 82606 I 2,2-Dichloropropane < 1.0 1.0 ug/L 7/12/99 SW846 8260B 1,1-Dichloropropene < 1.0 1.0 ug/L 7/12/99 SW846 82606 cis-1,3-Dichloropropene < 1.0 1.0 ug/L 7/12/99 SW846 82606 trans-1,3-Dichloropropene < 1.0 1.0 ug/L 7/12/99 SW846 8260B I I 1795 Industrial Drive x Vi Green Bay, WI 54302 � 920-469-2436 • E V AHEM 800 7 ENCHEM ., INC. FAX: 920-469-8827 N I -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS Field ID: ST-1 Report Date: 7/14/99 Lab Sample Number: 893755-014 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: WATER IEthylbenzene < 1.0 1.0 ug/L 7/12/99 SW846 82608 Diethyl ether < 1.0 1.0 ug/L 7/12/99 SW846 8260B I Fluorotrichloromethane < 1.0 1.0 ug/L 7/12/99 SW846 82606 Hexachlorobutadiene < 1.0 1.0 ug/L 7/12/99 SW846 82608 Isopropylbenzene < 1.0 1.0 ug/L 7/12/99 SW846 8260B Ip-Isopropyltoluene < 1.0 1.0 ug/L 7/12/99 SW846 8260B Methylene chloride < 1.0 1.0 ug/L 7/12/99 SW846 8260B 4-Methyl-2-pentanone < 5.0 5.0 ug/L 7/12/99 SW846 8260B I Methyl-tert-butyl-ether < 1.0 1.0 ug/L 7/12/99 SW846 8260B Naphthalene < 1.0 1.0 ug/L 7/12/99 SW846 8260B I n-Propylbenzene < 1.0 1.0 ug/L 7/12/99 SW846 8260B Styrene < 1.0 1.0 ug/L 7/12/99 SW846 8260B 1,1,2,2-Tetrachloroethane < 1.0 1.0 ug/L 7/12/99 SW846 8260B I1,1,1,2-Tetrachloroethane < 1.0 1.0 ug/L 7/12/99 SW846 82608 Tetrachloroethene < 1.0 1.0 ug/L 7/12/99 SW846 8260B Toluene < 1.0 1.0 ug/L 7/12/99 SW846 8260B Il,2,3-Trichlorobenzene < 1.0 1.0 ug/L 7/12/99 SW846 8260B 1,2,4-Trichlorobenzene < 1.0 1.0 ug/L 7/12/99 SW846 8260B I 1,1,1-Trichloroethane < 1.0 1.0 ug/L 7/12/99 SW846 8260B 1,1,2-Trichloroethane < 1.0 1.0 ug/L 7/12/99 SW846 8260B 1,1,2-Trichlorotrifluoroethane < 1.0 1.0 ug/L 7/12/99 SW846 82608 I 1,2,4-Trimethylbenzene < 1.0 1.0 ug/L 7/12/99 SW846 82606 Trichloroethene < 1.0 1.0 ug/L 7/12/99 SW846 82608 1,2,3-Trichloropropane < 1.0 1.0 ug/L 7/12/99 SW846 8260B ITetrahydrofuran < 5.0 5.0 ug/L 7/12/99 SW846 82608 1,3,5-Trimethylbenzene < 1.0 1.0 ug/L 7/12/99 SW846 82608 Vinyl chloride < 1.0 1.0 ug/L 7/12/99 SW846 8260B Xylenes,-m,-p < 1.0 1.0 ug/L 7/12/99 SW846 8260B Xylene,-o < 1.0 1.0 ug/L 7/12/99 SW846 8260B $ 4-Bromofluorobenzene 78 _ %Recov 7/12/99 SW846 82606- Dibromofluoromethane 83 %Recov 7/12/99 SW846 8260B Toluene-d8 91 - %Recov 7/12/99 SW846 8260B I 1795 Industrial Drive Green Bay,WI 54302 920-469-2436 Elk.�' � EM 800 7 ENCHEM � iivc FAx: 920-469-8827 I -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS I Field ID: TB(WATER) Report Date: 7/14/99 Lab Sample Number: 893755-015 Collection Date: 7/2/99 1 MDH LAB ID: 055-999-334 Matrix Type: WATER 1 Organic Results GASOLINE RANGE ORGANICS-WATER Prep Method: Wi MOD GRO Prep Date: 7/9/99 Analyst: EGS I Analysis Analysis Analyte Result EQL Units Code Date Method GASOLINE RANGE ORGANICS < 50 50 ug/I 7/13/99 Wi MOD GRO Blank Spike 97 — %Recov 7/13/99 Wi MOD GRO Blank Spike Duplicate 98 -- %Recov 7/13/99 Wi MOD GRO Blank < 50 50 ug/I 7/13/99 Wi MOD GRO Organic Results I MDH 465E VOLATILES-WATER Prep Method: SW846 5030B Prep Date: 7/9/99 Analyst: HW Analysis Analysis Analyte Result EQL Units Code Date Method Acetone < 10 10 ug/L 7/9/99 SW846 8260B Ally/Chloride < 1.0 1.0 ug/L 7/9/99 SW846 8260B Benzene < 1.0 1.0 ug/L 7/9/99 SW846 8260B Bromochloromethane < 1.0 1.0 ug/L 7/9/99 SW846 8260B Bromodichloromethane < 1.0 1.0 ug/L 7/9/99 SW846 8260B Bromoform < 1.0 1.0 ug/L 7/9/99 SW846 8260B Bromobenzene < 1.0 1.0 ug/L 7/9/99 SW846 8260B Bromomethane < 1.0 1.0 ug/L 7/9/99 SW846 8260B 2-Butanone < 5.0 5.0 ug/L 7/9/99 SW846 8260B s-Butylbenzene < 1.0 1.0 ug/L 7/9/99 SW846 8260B t-Butylbenzene < 1.0 1.0 ug/L 7/9/99 SW846 8260B n-Butylbenzene < 1.0 1.0 ug/L 7/9/99 SW846 8260B Carbon tetrachloride < 1.0 1.0 ug/L 7/9/99 SW846 8260B Chloroform < 1.0 1.0 ug/L 7/9/99 SW846 8260B Chlorobenzene < 1.0 1.0 ug/L 7/9/99 SW846 8260B Chlorodibromomethane < 1.0 1.0 ug/L 7/9/99 SW846 8260B I I1795 Industrial Drive -x Green Bay,WI 54302 lit E I HEM 920-469-2436 INC. 800 7 ENCHEM FAX: 920-469-8827 n .�. ....... .. a e... I -Analytical Report - Project Name: SENIOR HOUSING ADD. IProject Number: 7735-B Client: GME CONSULTANTS Field ID: TB(WATER) Report Date: 7/14/99 ILab Sample Number: 893755-015 Collection Date: 7/2/99 MDH LAB ID: 055-999-334 Matrix Type: WATER IChloroethane < 1.0 1.0 ug/L 7/9/99 SW846 8260B Chioromethane < 1.0 1.0 ug/L 7/9/99 SW846 8260B I 2-Chlorotoluene < 1.0 1.0 ug/L 7/9/99 SW846 8260B 4-Chlorotoluene < 1.0 1.0 ug/L 7/9/99 SW846 82608 1,2-Dibromo-3-chloropropane < 1.0 1.0 ug/L 7/9/99 SW846 8260B Ii 2-Dibromoethane < 1.0 1.0 ug/L 7/9/99 SW846 8260B Dibromomethane < 1.0 1.0 ug/L 7/9/99 SW846 8260B , < 1.0 1.0 ug/L 7/9/99 SW846 8260B Ii 1,4-Dichlorobenzene < 1.0 1.0 ug/L 7/9/99 SW846 8260B 1,2-Dichioroethane < 1.0 1.0 ug/L 7/9/99 SW846 8260B I 1,2-Dichlorobenzene < 1.0 1.0 ug/L 7/9/99 SW846 82606 1,1-Dichloroethene < 1.0 1.0 ug/L 7/9/99 SW846 8260B cis-1,2-Dichloroethene < 1.0 1.0 ug/L 7/9/99 SW846 8260B I Dichlorodifluoromethane < 1.0 1.0 ug/L 7/9/99 SW846 8260B trans-1,2-Dichloroethene < 1.0 1.0 ug/L 7/9/99 SW846 8260B Dichlorofluoromethane < 1.0 1.0 ug/L 7/9/99 SW846 8260B Ii,2-Dichloropropane < 1.0 1.0 ug/L 7/9/99 SW846 8260B 1,1-Dichioroethane < 1.0 1.0 ug/L 7/9/99 SW846 8260B 1,3-Dichloropropane < 1.0 1.0 ug/L 7/9/99 SW846 8260B I2,2-Dichloropropane < 1.0 1.0 ug/L 7/9/99 SW846 8260B 1,1-Dichloropropene < 1.0 1.0 ug/L 7/9/99 SW846 8260B I cis-1,3-Dichloropropene < 1.0 1.0 ug/L 7/9/99 SW846 8260B trans-1,3 Dichloropropene < 1.0 1.0 ug/L 7/9/99 SW846 8260B Ethylbenzene < 1.0 1.0 ug/L 7/9/99 SW846 8260B IDiethyl ether < 1.0 1.0 ug/L 7/9/99 SW846 8260B Fluorotrichloromethane < 1.0 1.0 ug/L 7/9/99 SW846 8260B Hexachlorobutadiene < 1.0 1.0 ug/L 7/9/99 SW846 8260B IIsopropylbenzene < 1.0 1.0 ug/L 7/9/99 SW846 8260B p-lsopropyltoluene < 1.0 1.0 ug/L 7/9/99 SW846 8260B I Methylene chloride 1.2 1.0 ug/L 7/9/99 SW846 8260B 4-Methyl-2-pentanone < 5.0 5.0 ug/L 7/9/99 SW846 8260B Methyl-tert-butyl-ether < 1.0 1.0 ug/L I 7/9/99 SW846 8260B I r 1795 Industrial Drive ' - Green Bay,WI 54302 920-469-2436 E /; V HEM 800 7 ENCHEM INC. FAx 920-469-8827 I -Analytical Report - I Project Name: SENIOR HOUSING ADD. Project Number: 7735-B Client: GME CONSULTANTS I Field ID: TB(WATER) Report Date: 7/14/99 Lab Sample Number: 893755-015 Collection Date: 7/2/99 1 MDH LAB ID: 055-999-334 Matrix Type: WATER Naphthalene < 1.0 1.0 ug/L 7/9/99 SW846 8260B n-Propylbenzene < 1.0 1.0 ug/L 7/9/99 SW846 8260B Styrene < 1.0 1.0 ug/L 7/9/99 SW846 8260B I 1,1,2,2-Tetrachloroethane < 1.0 1.0 ug/L 7/9/99 SW846 8260B 1,1,1,2-Tetrachloroethane < 1.0 1.0 ug/L 7/9/99 SW846 8260B Tetrachloroethene < 1.0 1.0 ug/L 7/9/99 SW846 8260B Toluene < 1.0 1.0 ug/L 7/9/99 SW846 8260B 1,2,3-Trichlorobenzene < 1.0 1.0 ug/L 7/9/99 SW846 8260B 1,2,4-Trichlorobenzene < 1.0 1.0 ug/L 7/9/99 SW846 8260B 1,1,1-Trichloroethane < 1.0 1.0 ug/L 7/9/99 SW846 8260B 1,1,2-Trichloroethane < 1.0 1.0 ug/L 7/9/99 SW846 8260B 1,1,2-Trichlorotrifluoroethane < 1.0 1.0 ug/L 7/9/99 SW846 8260B 1,2,4-Trimethylbenzene < 1.0 1.0 ug/L 7/9/99 SW846 8260B Trichloroethene < 1.0 1.0 ug/L 7/9/99 SW846 8260B 1,2,3-Trichloropropane < 1.0 1.0 ug/L 7/9/99 SW846 8260B Tetrahydrofuran < 5.0 5.0 ug/L 7/9/99 SW846 8260B 1,3,5-Trimethylbenzene < 1.0 1.0 ug/L 7/9/99 SW846 8260B I Vinyl chloride < 1.0 1.0 ug/L 7/9/99 SW846 8260B Xylenes,-m,-p < 1.0 1.0 ug/L 7/9/99 SW846 8260B Xylene,-o < 1.0 1.0 ug/L 7/9/99 SW846 8260B 4-Bromofluorobenzene 106 - %Recov 7/9/99 SW846 8260B Dibromofluoromethane 97 - %Recov 7/9/99 SW846 8260B Toluene-d8 103 -- %Recov 7/9/99 SW846 8260B I I I I I 1 5 I I MVTL LABORATORY REPORT 1 I I I I I I I I I I I 1 I • MEMBER LABORATORIES, Inc. l L iii P.O.BOX 249, 1126 N. FRONT STREET NEW ULM, MN 56073-0249 PHONE (507) 354-8517 WATS (800)782-3557 FAX (507)359-2890 I WE ARE AN.e OPPORTUNITY EMPLOYER "` '_x Report Date: 27 Jul. 1999 II ilia_ )' 1999 Lab Number: 99-L17573 J Work Order 4: 21-214 ERIC STOMMES Account #: 013009 II GME CONSULTANTS 14000 21ST AVE N MINNEAPOLIS MN 55447-4047 11 r Date Received: 8 Jul. 1999. Date Sampled: 2 Jul 1999 Project Name: OAK PART HEIGHTS, MN Project Number: 7735-C Method 3510 Date Extracted: 12 Jul 1999 IIMethod 8081, 8141A Date Analyzed: 17 Jul. 1999 IISample Description: ST-1 Analyte Result Units RL jAcetochlor < 0.5 ug/L 0.5 Alachlor (Lasso) < 0.5 ug/L 0.5 Atrazine (Aatrex) < 0.5 ug/L 0.5 IIChlorpyrifos (Lorsban) < 0.5 ug/L 0.5 Cyanazine (Bladex) < 0.2 ug/L 0.2 Deethylatrazine '�. < 0.5 ug/L 0.5 IIDeisopropylatrazine < 0.5 ug/L 0.5 EPTC (Eradicane) < 0.5 ug/L 0.5 Ethal.fluralin (Sonolan) < 0.5 ug/L 0.5 Fonofos (Dyphonate) < 0.5 ug/L 0.5 IIMetolachlor (Dual) < 0.5 ug/L 0.5 Metribuzin (Sencor, Lexone) < 0.5 ug/L 0.5 Pendimethalin (Prowl) < 0.5 ug/I., 0.5 IPhorate (Thimet) < 0.3 ug/L 0.3 Prometon (Pramitol) < 0.5 ug/L 0.5 Propachlor (Ramrod) < 0.5 ug/L 0.5 Propazine (Milogard) < 0.5 ug/L 0.5 Simazine (Princep) < 0.5 ug/L 0.5 Terbufos (Counter) < 0.2 ug/L 0.2 Tri-Allate (Far-Go) < 0.5 ug/L 0.5 IITriflurali.n (Treflan) < 0.5 ug/L 0.5 II RL = Reporting Limits 11 All data for this report has been approved by MVTL Laboratory Management. II MVTL guarantees the accuracy of the analysis done on the sample submitted for testing.It is not possible for MVTL to guarantee that a teat result obtained on a particular sample will be the same on any other I sample unless all conditions affecting the sample are the same,including sampling by MVTL.As a mutual protection to clients,the public and ourselves,all reports are submitted as the confidential property of clients,and authorization for publication of statements,conclusions or extracts from or regarding our reports is reserved pending our written approval. C MEMBER LABORATORIES, Inc. I L P.O. BOX 249, 1126 N. FRONT STREET NEW ULM, MN 56073-0249 I PHONE (507) 354-8517 WATS (800) 782-3557 FAX (507) 359-2890 WE ARE AN EQUAL OPPORTUNITY EMPLOYER Report Date: 27 Jul 1999 I/ Lab Number: 99-S2451 Work Order 4: 21-214 ERIC STOMMES Account 4: 013009 II GME CONSULTANTS 14000 21ST AVE N MINNEAPOLIS MN 55447-4647 Date Received: 8 Jul. 1999 Date Sampled: 2 Jul 1999 Project Name: OAK PART HEIGHTS, MN Project Number: 7735-C Method SW846 3545, 3550 Date Extracted: 14 Jul 1999 IIMethod SW846 8081, 81.41A Date Analyzed: 20 Jul 1999 ISample Description: GRNHSE COMP Analyte Result Units RI IIAcetochlor --- < 0.05 mg/Kg 0.05 Alachlor (Lasso) 0.13 mg/Kg 0.05 Atrazine (Aatrex) < 0.05 mg/Kg 0.05 IChlorpyr:ifos (Lorsban) < 0.05 mg/Kg 0.05 Cyanaz.ine (Bladex) < 0.05 mg/Kg 0.05 Deethylatrazine < 0.05 mg/Kg 0.05 IIDeisopropylatrazine < 0.05 mg/Kg 0.05 EPTC (Eradicane) < 0.03 mg/Kg 0.03 Ethalfluralin (Sonolan) < 0.05 mg/Kg 0.05 IIFonofos (Dyphonate) < 0.05 mg/Kg 0.05 Metolachlor (Dual) 0.05 mg/Kg 0.05 Metribuzin (Sensor, Lexone) < 0.05 mg/Kg 0.05 Pendimethalin (Prowl) < 0.05 mg/Kg 0.05 IIPhorate (Thimet) < 0.05 mg/Kg 0.05 Prometon (Pramitol ) < 0.05 mg/Kg 0.05 Propachlor (Ramrod) < 0.05 mg/Kg 0.05 Propazine (Milogard) < 0.05 mg/Kg 0.05 Simazin.e (.Pr.incep) < 0.05 mg/Kg 0.05 Terbufos (Counter) < 0.05 mg/Kg 0.05 Tri-Allate (Far-Go) < 0.05 mg/Kg 0.05 ITrifluralin (Tref.lan) < 0.05 mg/Kg 0.05 II EL = Reporting Limits IIAll data for this report has been approved by .MVTL Laboratory Management. 11 MVTL guarantees the accuracy of the analysis done on the sample submitted for testing.It is not possible for MVTL to guarantee that a teat result obtained on a particular sample will be the same on any other l sample unless all conditions affecting the sample are the same,including sampling by MVTL.As a mutual protection to clients,the public and ourselves,all reports are submitted as the confidential property of clients,and authorization for publication of statements,conclusions or extracts from or regarding our reports is reserved pending our written approval. IMEMBER 4, LABORATORIES Inc. AC I L P.O. BOX 249, 1126 N. FRONT STREET NEW ULM, MN 56073-0249 I PHONE (507) 354-8517 WATS (800) 782-3557 FAX(507) 359-2890 WE ARE AN EQUAL OPPORTUNITY EMPLOYER I MVTL I QUALITY CONTROL REPORT I Work Order#: 199921-214 Lab #: 99-L17573 Date Reported: 27 July 1999 I Analyte Spike Recovered % Recovery QC Blank Analyte I (ppb) (ppb) Concentrations Acetochlor 0.585 0.581 99 ND Alachlor 0.495 0.472 95 ND Atrazine 0.494 0.468 95 ND ICyanazine 0.484 0.526 109 ND De-ethyl Atrazine 0.486 0.478 98 ND De-isopropyl Atrazine 0.471 0.409 86 ND IEPTC 0.495 0.471 95 ND Metalochlor 0.582 0.551 95 ND IMetribuzin 0.495 0.500 101 ND Pramitol 0.495 0.522 105 ND ISimazine 0.487 0.492 101 ND IND= None Detected I MVTL METHOD I.D. REVISION REFERENCE METHOD I B15323 1.5 US EPA SW 846-8081- 8041A-3510 I Quality control data reviewed and approved by R.Dan O'Connell, Organics Laboratory Manager By and for Minnesota Valley Testing Laboratories,Inc. I MVTL guarantees the accuracy of the analysis done on the sample submitted for testing.It is not possible for MVTL to guarantee that a test result obtained on a particular sample will be the same on any other sample unless all conditions affecting the sample are the same,including sampling by MVTL.As a mutual protection to clients,the public and ourselves,all reports are submitted as the confidential property of clients,and authorization for publication of statements,conclusions or extracts from or regarding our reports is reserved pending our written approval. I .. MEMBER LABORATORIES, Inc. I L P.O. BOX 249, 1126 N. FRONT STREET AC NEW ULM, MN 56073-0249 I PHONE (507)354-8517 WATS (800) 782-3557 FAX(507)359-2890 WE ARE AN EQUAL OPPORTUNITY EMPLOYER I I MVTL QUALITY CONTROL REPORT I I Work Order#: 199921-214 Lab #: 99-S2451 Date Reported: 27 July 1999 I S Analyte Spike Recovered % Recovery QC Blank Analyte Y P (ppb) (ppb) Concentrations IAlachlor 66.40 65.89 99 ND IAtrazine 66.77 60.86 91 ND Cyanazine 69.89 71.05 102 ND IEPTC 68.97 57.66 84 ND Ethalfluralin 67.71 69.73 103 ND IMetalochlor 71.20 64.06 90 ND iTrifluralin 70.53 66.54 94 ND ND= None Detected I IMVTL METHOD I.D. REVISION REFERENCE METHOD B15311 1.7 US EPA SW 846-3545- '1 3550-8081A-8141A I R . ,C1.3,_CC.,,,i4 Quality control data reviewed and approved by R. Dan O'Connell, Organics Laboratory Manager By and for Minnesota Valley Testing Laboratories,Inc. I I MVTL guarantees the accuracy of the analysis done on the sample submitted for testing.U is not possible for MVTL to guarantee that a test result obtained on a particular sample will be the same on any other sample unless all conditions affecting the sample are the same,including sampling by MVTL.As a mutual protection to clients,the public and ourselves,all reports are submitted as the confidential property of clients,and authorization for publication of statements,conclusions or extracts from or regarding our reports is reserved pending our written approval. I . U . 0 :.......:......-:.:..:......... ho "�,, b m E N *,_:.4, -!- N 3 C a 0 T H o__ - 5 Q d: ^l 2 H \ . >mi o d v\ V l 1 a.+-a 1 ® �� E Q �. 1 :::.•I'':iiiii:: ‘de.) U a a •3 m CO I "e%)i 2 (1) :.....'''''. •O° m o Iac 00 a E 0 '' ai E Q o a o� z mO 5. O Q m W I CC I p ' E Q N O d Lys c L Q �\� ~ a L .11,1::":„,0,...,..(01..!:::::.........,:1::.:....,....,..,::-...,--.:-.: .ri �- F- Z 1 _ � 2 s 1 a. �J'^ w (p,4)._:.,,./) -. m 'yi � +� �// f' .m. m m H tq c`� a> d OC aim E oSly, „le,. f d a LL o r Op� II co Z N =, i c c � zQo Y N �� • N CT a a) co v m o oM ry c O O v su c c.a o d o I/ 0- a .O 'O O W•U m i6 m • I C. cQ � m WF- 3 oa p F ° V V co O ~ 1, 0 M Is C 141 4C12) N �` Q c o v, Z can X -.-.-0, N V -p d 'Q V� .co E °`' 14.4 h CD L13 LL m = . t' C In S• j O Y J N %kr co co Z u�� {� 8 I fh p ++ M a°vo 1 . I I 1 APPENDIX C ' LEGEND TECHNICAL SERVICES, INC. LABORATORY REPORT i i I 1 i 1 1 1 r 1 111L. D '. 775 Vandalia Street St. Paul, MN 55114 ' Technical Services, Inc . Tel: 651.642.1150 Fax: 651.642.1239 www.legend-group.com INovember 30, 2004 Mr. Eric Stommes GME Consultants, Inc I14000 21st Ave N Minneapolis, MN 55447 IWork Order Number: 0404059 RE: Senior Housing Partners I Enclosed are the results of analyses for samples received by the laboratory on 11/19/04. If you have any questions concerning this report, please feel free to contact me. I All samples will be retained by LEGEND for 30 days from the date of this report and then discarded unless other arrangements are made. Minnesota Certification #027-123-295 IPrepared by, LEGEND TECHNICAL SERVICES, INC 1 , - (7? Karla Reps Chris Bremer Client Representative Laboratory Director 1 I 1 LEGEND Technical Services, Inc The results in this report apply to the samples • analyzed in accordance with the chain of custody ' document. This analytical report must be reproduced in its entirety. I L E E 775 Vandalic Street I St Paul,MN 55114 Technical Services, inc, 651.642.1150 I GME Consultants, Inc Project: Senior Housing Partners I 14000 21st Ave N Project Number: 7735-E Date Reported: Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 I ANALYTICAL REPORT FOR SAMPLES Sample ID Laboratory ID Matrix Date Sampled Date Received SP-1 0404059-01 Soil 11/17/04 00:00 11/19/04 14:40 SP-2 0404059-02 Soil 11/17/04 00:00 11/19/04 14:40 1 SP-3 0404059-03 Soil 11/17/04 00:00 11/19/04 14:40 Shipping container information Default Cooler Temperature: 7.5 Received on ice: Yes Temperature blank was present Received on blue ice: No Received on melt water: No Ambient: No Acceptable (IH/ISO only): No Custody seals: No Case Narrative: The%RPD for the DRO LCS/LCSD exceeded 20.0%. Recoveries were within limits. The herbicide analysis was performed by a certified sub-contract laboratory. I • I I I I I I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance I with the chain of custody document. This analytical report must be reproduced in its entirety. Page 2 of 33' IL E G " D 775 Vandalia Street St Paul,MN 55114 ITechnical Services, Inc. 651.642.1150 IGME Consultants, Inc Project: Senior Housing Partners 14000 21st Ave N Project Number: 7735-E Date Reported: 1 Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 DRO/8015B ILEGEND Technical Services, Inc Reporting Analyte Result Limit MDL Units Dilution Batch Prepared Analyzed Method Notes ISP-2(0404059-02)Soil Sampled: 11/17/04 00:00 Received: 11/19/04 14:40 Diesel Range Organics 49 6.8 1.4 mg/kg dry 1 B4K1916 11/19/04 11/22/04 Wisc Mod A,L1 DRO ISurrogate:C-30 86.8 60-130 I I I I 1 I I I I I I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 3 of 33 II LEGEND 775 Vandalic Street I St Paul,MN 55114 Technical Services, Inc. 651.642.1150 I GME Consultants, Inc Project: Senior Housing Partners 14000 21st Ave N Project Number: 7735-E Date Reported: Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 GRO/8021B LEGEND Technical Services, Inc Reporting Analyte Result Limit MDL Units Dilution Batch Prepared Analyzed Method Notes 0 SP-2(0404059-02)Soil Sampled: 11/17/04 00:00 Received: 11/19/04 14:40 I Gasoline range organics <5.7 5.7 1.4 mg/kg dry 1 B4K1902 11/19/04 11/19/04 Wisc Mod GRO Surrogate:4-Fluorochlorobenzene 94.8 80-120 % ,, u I I I I I 1 I I I I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance I with the chain of custody document. This analytical report must be reproduced in its entirety. Page 4 of 31 IL E G E N D 775 Vandalia Street St Paul,MN 55114 ITechnical Services, Inc . 651.642.1150 IGME Consultants, Inc Project: Senior Housing Partners 14000 21st Ave N Project Number: 7735-E Date Reported: I Minneapolis MN, 55447 Project Manager: Mr. Eric Stommes November 30,2004 TOTAL METALS ANALYSIS LEGEND Technical Services, Inc IReporting Analyte Result Limit MDL Units Dilutlfon Batch Prepared Analyzed Method Notes ISP-2(0404059-02)Soil Sampled: 11/17/04 00:00 Received: 11/19/04 14:40 Mercury <0.11 0.11 0.0039 mg/kg dry 1 B4K2307 11/23/04 11/23/04 EPA 7471A Arsenic 3.2 0.57 0.13 mg/kg dry I B4K2201 11/22/04 11/22/04 EPA 6010B IBarium 86 1.1 0.16 mg/kg dry 1 " " ,,Cadmium 0.79 0.29 0.0054 mg/kg dry 1 Chromium 13 0.57 0.010 mg/kg dry 1 " " " " ILead 64 1.1 0.026 mg/kg dry 1 " " " II <0.57 0.57 0.15 mg/kg dry 1 Silver <0.29 0.29 0.024 mg/kg dry 1 " " " " ISP-3 (0404059-03)Soil Sampled: 11/17/04 00:00 Received: 11/19/04 14:40 Mercury <0.12 0.12 0.0040 mg/kg dry 1 B4K2307 11/23/04 11/23/04 EPA 7471A IArsenic 4.1 0.58 0.13 mg/kg dry 1 B4K2201 11/22/04 11/22/04 EPA 6010B Barium 73 1.2 0.16 mg/kg dry 1 Cadmium 0.32 0.29 0.0055 mg/kg dry 1 " " " II IChromium 15 0.58 0.010 mg/kg dry 1 " " " Lead 88 1.2 0.027 mg/kg dry 1 Selenium <0.58 0.58 0.15 mg/kg dry 1 " " " " Silver <0.29 0.29 0.024 mg/kg dry 1 " " I I I I I I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 5 of 33 LE E N D 775 Vandalia Street I St Paul,MN 55114 Technical Services, Inc. 651.642.1150 1 GME Consultants, Inc Project: Senior Housing Partners 1 14000 21st Ave N Project Number: 7735-E Date Reported: Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 PAH 8270C LEGEND Technical Services, Inc Reporting Analyte Result Limit MDL Units Dilution Batch Prepared Analyzed Method Notes SP-2(0404059-02)Soil Sampled: 11/17/04 00:00 Received: 11/19/04 14:40 ' 2-Chloronaphthalene <0.38 038 0.095 mg/kg dry 1 B4K2216 11/22/04 11/22/04 8270C 2-Methylnaphthalene <0.38 0.38 0.11 mg/kg dry 1 " Acenaphthene <0.38 0.38 0.094 mg/kg dry 1 " " I Acenaphthylene 0.43 0.38 0.095 mg/kg dry 1 " " Anthracene <0.38 0.38 0.10 mg/kg dry 1 " Benzo(a)anthracene 1.5 0.38 0.10 mg/kg dry 1 " " ., I I. Benzo(a)pyrene 1.6 0.38 0.098 mg/kg dry 1 11 Benzo(b)fluoranthene 1.9 0.38 0.091 mg/kg dry 1 " " " Benzo(g,h,i)perylene 1.0 0.38 0.094 mg/kg dry 1 " " " I Benzo(k)fluoranthene 0.91 0.38 0.11 mg/kg dry 1 " " " Chrysene 1.8 0.38 0.10 mg/kg dry 1 " Dibenz(a,h)anthracene <0.38 0.38 0.099 mg/kg dry 1 " I II Fluoranthene 2.9 0.38 0.10 mg/kg dry 1 " " " Fluorene <0.38 0.38 0.090 mg/kg dry 1 " "Indeno(1,2,3-cd)pyrene 1.0 0.38 0.085 mg/kg dry 1 " " I Naphthalene <0.38 0,38 0.095 mg/kg dry 1 " " " Phenanthrene 0.89 0.38 0.10 mg/kg dry 1 " " I Pyrene 2.3 0.38 0.10 mg/kg dry 1 " " " Surrogate:2-Fluorobiphenyl 85.5 38.1-1/5 % " " " " Surrogate:Nitrobenzene-d5 69.5 39.4-115 % " " " " I Surrogate:Terphenyl-dl4 88.2 36.1-115 % " " " SP-3(0404059-03)Soil Sampled: 11/17/04 00:00 Received: 11/19/04 14:40 2-Chloronaphthalene <0.38 0,38 0.097 mg/kg dry 1 B4K2216 11/22/04 11/22/04 8270C I 2-Methylnaphthalene <0.38 0.38 0.11 mg/kg dry 1 Acenaphthene <0.38 0,38 0.095 mg/kg dry 1 " 1 Acenaphthylene 0.38 0.38 0.097 mg/kg dry 1 " " " Anthracene <0.38 mg/kg dry 1 38 0 38 0 10 " " " II Benzo(a)anthracene 1.4 0.38 0.10 mg/kg dry 1 " " I Benzo(a)pyrene 1.5 0.38 0.099 mg/kg dry 1 " " Benzo(b)fluoranthene 1.8 0.38 0.092 mg/kg dry 1 " " " Benzo(g,h,i)perylene 0.97 0.38 0.095 mg/kg dry 1 " I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance I with the chain of custody document. This analytical report must be reproduced in its entirety. • Page 6 of 3J IL "" G '"" D 775 Vendalia Street St Paul,MN 55114 ITechnical Services, Inc. 651.642.1150 IGME Consultants, Inc Project: Senior Housing Partners 14000 21st Ave N Project Number: 7735-E Date Reported: I Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 . PAH 8270C LEGEND Technical Services, Inc IReporting Analyte Result Limit MDL Units Dilution Batch Prepared Analyzed Method Notes I SP-3 (0404059-03)Soil Sampled: 11/17/04 00:00 Received: 11/19/04 14:40 Benzo(k)fluoranthene 0.78 0.38 0.11 mg/kg dry 1 B4K2216 11/22/04 11/22/04 8270C Chrysene 1.7 0.38 0.10 mg/kg dry 1 IDibenz(a,h)anthracene <0.38 0.38 0.10 mg/kg dry 1 " " Fluoranthene 3.0 0.38 0.10 mg/kg dry 1 Fluorene <0.38 0.38 0.091 mg/kg dry 1 " IIndeno(1,2,3-cd)pyrene 0.76 0.38 0.086 mg/kg dry I " " " Naphthalene <0.38 0.38 0.097 mg/kg dry 1 Phenanthrene 1.4 0.38 0.10 mg/kg dry 1 .1 " t. IPyrene 2.4 0.38 0.11 mg/kg dry 1 " " " " Surrogate:2-Fluorobiphenyl 90.7 38.1-115 Surrogate:Nitrobenzene-d5 74.6 39.4-115 % " " " Surrogate:Terphenyl-d14 81.1 36.1-115 I I I I I I I I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. IPage 7 of 33 LE "'""" N D 775 Vandalia Street I St Paul,MN 55114 Technical Services, Inc. 651.642.1150 I i GME Consultants, Inc Project: Senior Housing Partners I 14000 21st Ave N Project Number: 7735-E Date Reported: Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 I PCB 8082 LEGEND Technical Services, Inc Reporting I Analyte Result Limit MDL Units Dilution Batch Prepared Analyzed Method Notes SP-1 (0404059-01)Soil Sampled: 11/17/04 00:00 Received: 11/19/04 14:40 I PCB-1016 <0.24 0.24 0.042 mg/kg dry 1 B4K1922 11/19/04 11/23/04 EPA 8082 PCB-1221 <0.24 0.24 0.036 mg/kg dry 1 PCB-1232 <0.24 0.24 0.041 mg/kg dry 1 " " II PCB-1242 <0.24 0.24 0.041 mg/kg dry 1 " II PCB-1248 <0.24 0.24 0.020 mg/kg dry 1 ., " PCB-1254 <0.24 0.24 0.026 mg/kg dry 1 I PCB-1260 <0.24 0.24 0.041 mg/kg dry 1 " " " II Surrogate:Decachlorobiphenyl 74.4 62.8-130 % " " " " ISurrogate:Tetrachloro-meta-xylene 97.5 72.3-130 % " " " " SP-2(0404059-02)Soil Sampled: 11/17/04 00:00 Received: 11/19/04 14:40 PCB-1016 <0.23 0.23 0.041 mg/kg dry 1 B4K1922 11/19/04 11/23/04 EPA 8082 I PCB-1221 <0.23 0.23 0.036 mg/kg dry 1 PCB-1232 <0.23 0.23 0.040 mg/kg dry 1 " II PCB-1242 <0.23 0.23 0.040 mg/kg dry 1 " I PCB-1248 <0.23 0.23 0.020 mg/kg dry 1 " " PCB-1254 <0.23 0.23 0.025 mg/kg dry 1 " PCB-1260 <0.23 0.23 0.040 mg/kg dry 1 " Surrogate:Decachlorobiphenyl 78.0 62.8-130 % " a " " Surrogate:Tetrachloro-meta-xylene 111 72.3-130 % " " " " ISP-3 (0404059-03)Soil Sampled: 11/17/04 00:00 Received: 11/19/04 14:40 PCB-1016 <0.23 0.23 0.042 mg/kg dry 1 B4K1922 11/19/04 11/23/04 EPA 8082 IPCB-1221 <0.23 0.23 0.036 mg/kg dry 1 PCB-1232 <0.23 0.23 0.041 mg/kg dry 1 " " II PCB-1242 <0.23 0.23 0.041 mg/kg dry 1 " " " I PCB-1248 <0.23 0.23 0.020 mg/kg dry 1 .. " " PCB-1254 <0.23 0.23 0.026 mg/kg dry 1 " .. ., ,. PCB-1260 <0.23 0.23 0.041 mg/kg dry 1 " " " i Surrogate:Decachlorobiphenyl 79.0 62.8-130 % " " " Surrogate: Tetrachloro-meta-xylene 106 72.3-130 % " " " " I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance I with the chain of custody document. This analytical report must be reproduced in its entirety. Page 8 of 331 t 775 Vandalic Street St Paul,MN 55114 I 651.642.1150 Technical Services, Inc. IGME Consultants, Inc Project: Senior Housing Partners 14000 21st Ave N Project Number: 7735-E Date Reported: I Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 PERCENT SOLIDS LEGEND Technical Services, Inc IReporting Analyte Result Limit MDL Units Dilution Batch Prepared Analyzed Method Notes 2 SP-1 (0404059-01)Soil Sampled: 11/17/04 00:00 Received: 11/19/04 14:40 Solids 85 % 1 B4K2218 11/22/04 11/23/04 %calculation SP-2(0404059-02)Soil Sampled: 11/17/04 00:00 Received: 11/19/04 14:40 I %Solids 87 % 1 B4K2218 11/22/04 11/23/04 %calculation SP-3(0404059-03)Soil Sampled: 11/17/04 00:00 Received: 11/19/04 14:40 %Solids 86 % 1 B4K2218 11/22/04 11/23/04 %calculation I I 1 I I I I I I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. IIPage 9 of 33 ILEGEND 775 Vandalia Street 1 St Paul,MN 55114 Technical Services, Inc. 651.642.1150 I GME Consultants, Inc Project: Senior Housing Partners • I 14000 21st Ave N Project Number: 7735-E Date Reported: Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 PESTICIDES SOIL 8081A LEGEND Technical Services, Inc Reporting Analyte Result Limit MDL Units Dilution Batch Prepared Analyzed Method Notes II SP-1 (0404059-01)Soil Sampled: 11/17/04 00:00 Received: 11/19/04 14:40 1 4,4"-DDD <0.047 0.047 0.0016 mg/kg dry 1 B4K1922 11/19/04 11/23/04 EPA 8081A 4,4'-DDE 0.084 0.047 0.0014 mg/kg dry 1 " 4,4"-DDT 0.22 0.047 0.0015 mg/kg dry 1 " " " "a-Chlordane 0.23 0.047 0.0013 mg/kg dry 1 I Aldrin <0.047 0.047 0.0013 m " .•g/kg dry 1 alpha-BHC <0.047 0.047 0.0011 mg/kg dry 1 " " I beta-BHC <0.047 0.047 0.00099 mg/kg ,,"g dry 1 delta-BHC <0.047 0.047 0.0014 mg/kg dry 1 " " " Dieldrin <0.047 0.047 0.0038 m " I g/kg dry 1 Endosulfan I <0.047 0.047 0.0024 m " ..g/kg dry 1 Endosulfan II <0.047 0.047 0.0019 mg/kg dry 1 -Endosulfan sulfate <0.047 0.047 0.0019 mg/kg dry 1 " 1 Endrin <0.047 0.047 0.0015 mg/kg dry 1 " " Endrin aldehyde <0.047 0.047 0.0025 mg/kg dry 1 " " Endrin ketone <0.047 0.047 0.0016 mg/kg dry 1 " " I gamma-BHC(Lindane) <0.047 0.047 0.0012 mg/kg dry 1 " " gamma-Chlordane 0.23 0.047 0.0019 mg/kg dry 1 " Heptachlor <0.047 0.047 0.0012 mg/kg dry 1 ' I" Heptachlor epoxide 0.061 0.047 0.0013 mg/kg dry 1 " Methoxychlor <0.047 0.047 0.0021 m "g/kg dry 1 I Toxaphene <0.047. 0.047 0.013 mg/kg dry 1 II Surrogate:Decachlorobiphenyl 73.0 60-141 % " ., " " Surrogate:Tetrachloro-meta-xylene 102 70-133 % " .. " " 1 SP-2(0404059-02)Soil Sampled: 11/17/04 00:00 Received: 11/19/04 14:40 4,4'-DDD <0.046 0.046 0.0016 mg/kg dry 1 B4K1922 11/19/04 11/23/04 EPA 8081A I 4,4'-DDE <0.046 0.046 0.0014 mg/kg dry 1 4,4"-DDT <0.046 0.046 0.0015 mg/kg dry 1 ,. " a-Chlordane <0.046 0.046 0.0013 mg/kg dry 1 "" 1 Aldrin <0.046 0.046 0.0013 m "g/kg dry 1 alpha-BHC <0.046 0.046 0.0011 mg/kg dry 1 " " " " beta-BHC <0.046 0.046 0.00097 mg/kg dry 1 " " I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 10 of 33 I IE "" D 775 Vandalia Street St Paul,MN 55114 651.642.1150 ITechnical Services, Inc. 1 GME Consultants, Inc Project: Senior Housing Partners 14000 21st Ave N Project Number: 7735-E Date Reported: I Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 PESTICIDES SOIL 8081A LEGEND Technical Services, Inc IReporting Analyte Result Limit MDL Units Dilution Batch Prepared Analyzed Method Notes IISP-2(0404059-02)Soil Sampled: 11/17/04 00:00 Received: 11/19/04 14:40 delta-BHC <0.046 0.046 0.0014 mg/kg dry 1 B4K1922 11/19/04 11/23/04 EPA 8081A Dieldrin <0.046 0.046 0.0037 mg/kg dry 1 " II IIII II Endosulfan I <0.046 0.046 0.0023 mg/kg dry 1 II II Endosulfan II <0.046 0.046 0.0018 mg/kg dry 1 II Endosulfan sulfate <0.046 0.046 0.0018 mg/kg dry 1 " " IEndrin <0.046 0.046 0.0015 mg/kg dry 1 p " Endrin aldehyde <0.046 0.046 0.0024 mg/kg dry 1 Endrin ketone <0.046 0.046 0.0016 mg/kg dry 1 " " lgamma-BHC(Lindane) <0.046 0.046 0.0011 mg/kg dry 1 gamma-Chlordane <0.046 0.046 0.0018 mg/kg dry 1 I Heptachlor <0.046 0.046 0.0011 mg/kg dry 1 " " " .. II II Heptachlor epoxide <0.046 0.046 0.0013 mg/kg dry 1 " „ Methoxychlor <0.046 0.046 0.0021 mg/kg dry 1 II Toxaphene <0.046 0.046 0.013 mg/kg dry 1 " " " " Surrogate:Decachlorobiphenyl 76.5 60-141 % " " " " Surrogate:Tetrachloro-meta-xylene 113 70-133 % " " " " ISP-3(0404059-03)Soil Sampled: 11/17/04 00:00 Received: 11/19/04 14:40 4,4"-DDD <0.047 0.047 0.0016 mg/kg dry 1 B4K1922 11/19/04 11/23/04 EPA 8081A 4,4"-DDE <0.047 0.047 0.0014 mg/kg dry 1 " " " 14,4"-DDT <0.047 0.047 0.0015 mg/kg dry 1 " " " a-Chlordane 0.24 0.047 0.0013 mg/kg dry 1 II II II IAldrin <0.047 0.047 0.0013 mg/kg dry 1 .. .• .. ., alpha-BHC <0.047 0.047 0.0011 mg/kg dry 1 II beta-BHC <0.047 0.047 0.00098 mg/kg dry 1 ,. " .. ' delta-BHC <0.047 0.047 0.0014 mg/kg dry 1 Dieldrin <0.047 0.047 0.0037 mg/kg dry 1 " " ,, Endosulfan I <0.047 0.047 0.0023 mg/kg dry 1 " " " II ' Endosulfan II <0.047 0.047 0.0019 mg/kg dry 1 N " Endosulfan sulfate <0.047 0.047 0.0019 mg/kg dry 1 Endrin <0.047 0.047 0.0015 mg/kg dry 1 II II II 111 Endrin aldehyde <0.047 0.047 0.0024 mg/kg dry 1 " " " LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. IPage 11 of 33 L E E D 775 Vandalia Street I St Paul,MN 55114 Technical Services, Inc. 651.642.1150 I GME Consultants, Inc Project: Senior Housing Partners I 14000 21st Ave N Project Number: 7735-E Date Reported: Minneapolis MN, 55447 Project Manager: Mr. Eric Stommes November 30,2004 PESTICIDES SOIL 8081A LEGEND Technical Services, Inc Reporting Analyte Result Limit MDL Units Dilution Batch Prepared Analyzed Method Notes SP-3 (0404059-03)Soil Sampled: 11/17/04 00:00 Received: 11/19/04 14:40 Endrin ketone <0.047 0.047 0.0016 mg/kg dry 1 B4K1922 11/19/04 11/23/04 EPA 8081A I gamma-BHC(Lindane) <0.047 0.047 0.0012 mg/kg dry 1 " gamma-Chlordane 0.28 0.047 0.0019 mg/kg dry 1 " " " " Heptachlor <0.047 0.047 0.0012 mg/kg dry 1 " " " " Heptachlor epoxide <0.047 0.047 0.0013 mg/kg dry I " " " If Methoxychlor <0.047 0.047 0.0021 mg/kg dry 1 " " " " 111 Toxaphene <0.047 0.047 0.013 mg/kg dry I " " Surrogate:Decachlorobiphenyl 79.9 60-141 % " " " " Surrogate:Tetrachloro-meta-xylene 110 70-133 % " " " I I I I I I I I I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 12 of 331 1 L E '" D 775 Vandalia Street St Paul,MN 55114 1 Technical Services, Inc. 651.642.1150 IGME Consultants, Inc Project: Senior Housing Partners 14000 21st Ave N Project Number: 7735-E Date Reported: I Minneapolis MN, 55447 Project Manager: Mr. Eric Stommes November 30,2004 VOC GCMS 8260B LEGEND Technical Services, Inc IReporting Analyte Result Limit MDL Units Dilution Batch Prepared Analyzed Method Notes SP-2(0404059-02)Soil Sampled: 11/17/04 00:00 Received: 11/19/04 14:40 II 1,1,1,2-Tetrachloroethane <0.57 0.57 0.034 mg/kg dry 1 B4K1909 11/19/04 11/19/04 EPA 8260B 1,1,1-Trichloroethane <0.29 0.29 0.043 mg/kg dry 1 I IIII 1,1,2,2-Tetrachloroethane <0.29 0.29 0.045 mg/kg dry 1 1,1,2-Trichloroethane <0.29 0.29 0.054 mg/kg dry 1 1,1,2-Trichlorotrifluoroethane <0.29 0.29 0.059 mg/kg dry 1 n I 11 1,1-Dichloroethane <0.29 40.29 0.043 mg/kg dry 1 " 1,1-Dichloroethene <0.29 0.29 0.022 mg/kg dry 1 1,1-Dichloropropene <0.29 0.29 0.036 mg/kg dry 1 SI 1,2,3-Trichlorobenzene <0.57 0.57 0.079 mg/kg dry 1 1,2,3-Trichloropropane <0.57 0.57 0.061 mg/kg dry 1 1,2,4-Trichlorobenzene <0.57 0.57 0.044 mg/kg dry 1 1,2,4-Trimethylbenzene <0.29 0.29 0.030 mg/kg dry 1 II 19 le 1,2-Dibromo-3-chloropropane <0.57 0.57 0.16 mg/kg dry 1 1,2-Dibromoethane(EDB) <0.29 0.29 0.060 mg/kg dry 1 1,2-Dichlorobenzene <0.29 0.29 0.033 mg/kg dry 1 II II II IS IS II 1,2-Dichloroethane <0.29 0.29 0.032 mg/kg dry 1 1,2-Dichloropropane <0.29 0.29 0.041 mg/kg dry 1 ". 1,3,5-Trimethylbenzene <0.29 0.29 0.026 mg/kg dry 1 1,3-Dichlorobenzene <0.29 0.29 . 0.023 mg/kg dry 1 111 It1,3-Dichloropropane <0.29 0.29 0.026 mg/kg dry 1 SO 1,4-Dichlorobenzene <0.29 0.29 0.023 mg/kg dry 1 2,2-Dichloropropane <0.57 0.57 0.026 mg/kg dry 1 II II 2-Butanone <2.3 2.3 0.18 mg/kg dry 1 2-Chlorotoluene <0.29 0.29 0.021 mg/kg dry 1 „ 4-Chlorotoluene <0.29 0.29 0.023 mg/kg dry 1 I II II Acetone <2.3 2.3 0.23 mg/kg dry 1 Ally/chloride <0.57 0.57 0.040 mg/kg dry 1 Benzene <0.29 0.29 0.031 mg/kg dry 1 p I Bromobenzene <0.29 0.29 0.053 mg/kg dry 1 II Bromochloromethane <0.29 0.29 0.066 mg/kg dry 1 IS It IS Bromodichloromethane <0.29 0.29 0.068 mg/kg dry 1 n II IS I Bromoform <0.57 0.57 0.084 mg/kg dry 1 LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance I with the chain of custody document. This analytical report must be reproduced in its entirety. IPage 13 of 33 'LEGEND 775 Vandalia Street I St Paul,MN 55114 Technical Services, Inc. 651.642.1150 I GME Consultants, Inc Project: Senior Housing Partners I 14000 21st Ave N Project Number: 7735-E Date Reported: Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 I VOC GCMS 82608 LEGEND Technical Services, Inc Reporting Analyte Result Limit MDL Units Dilution Batch Prepared Analyzed Method Notes SP-2(0404059-02)Soil Sampled: 11/17/04 00:00 Received: 11/19/04 14:40 Bromomethane <0.57 0.57 0.075 mg/kg dry 1 B4K1909 11/19/04 11/19/04 EPA 8260B I Carbon tetrachloride <0.29 0.29 0.057 mg/kg dry 1 " Chlorobenzene <0.29 0.29 0.034 mg/kg dry 1 " I Chloroethane <0.57 0.57 0.092 mg/kg dry 1 " ,, Chloroform <0.29 0.29 0.033 mg/kg dry 1 " II Chloromethane <0.29 0.29 0.034 mg/kg dry 1 I cis-1,2-Dichloroethene <0.29 0.29 0.052 mg/kg dry 1 01 cis-1,3-Dichloropropene <0.29 0.29 • 0.049 mg/kg dry 1 " .. Dibromochloromethane <0.29 0.29 0.040 mg/kg dry 1 " I Dibromomethane <0.57 0.57 0.037 mg/kg dry 1 " " Dichlorodifluoromethane <0.57 0.57 0.070 mg/kg dry 1 " .. Dichlorofluoromethane <0.29 0.29 0.059 mg/kg dry 1 " " I Ethyl ether <0.29 0.29 0.017 mg/kg dry 1 " 11 Ethylbenzene <0.29 0.29 0.013 mg/kg dry 1 II Hexachlorobutadiene <0.57 0.57 0.11 mg/kg dry 1 " " " I lsopropylbenzene <0.29 0.29 0.016 mg/kg dry 1 .. m,p-Xylene <0.57 0.57 0.066 mg/kg dry 1 " ., Methyl isobutyl ketone <0.57 0.57 0.13 mg/kg dry 1 " " 1 Methyl tert-butyl ether <0.29 0.29 0.038 mg/kg dry 1 " .. Methylene chloride <1.7 1.7 0.080 mg/kg dry 1 " " " I Naphthalene <0.57 0.57 0.018 mg/kg dry 1 " n-Butylbenzene <0.29 0,29 0.028 mg/kg dry 1 " " n-Propylbenzene <0.29 0.29 0.031 mg/kg dry 1 .. 1 o-Xylene <0.29 0.29 0.020 mg/kg rY dry 1 " " „ p-Isopropyltoluene <0.29 0.29 0.020 mg/kg dry 1 " . sec-Butylbenzene <0.29 0.29 0.018 mg/kg dry 1 I Styrene <0.29 0.29 0.026 mg/kg dry 1 " II tert-Butylbenzene <0.29 0.29 0.016 mg/kg dry 1 " " Tetrachloroethene <0.29 0.29 0.036 mg/kg dry 1 " I II Tetrahydrofuran <2.3 2.3 0.037 mg/kg dry 1 II II Toluene <0.29 0.29 0.021 mg/kg dry 1 " trans-1,2-Dichloroethene <0.29 0.29 0.036 mg/kg dry 1 " I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 14 of 33 , • IL E E D 775 Vandalia Street St Paul,MN 55114 1 Technical Services, Inc. 651.642.1150 IGME Consultants, Inc Project: Senior Housing Partners 14000 21st Ave N Project Number: 7735-E Date Reported: ' Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 VOC GCMS 8260B LEGEND Technical Services, Inc I . Reporting Analyte Result Limit MDL Units Dilution Batch Prepared Analyzed Method Notes ISP-2(0404059-02)Soil Sampled: 11/17/04 00:00 Received: 11/19/04 14:40 trans-1,3-Dichloropropene <0.29 0.29 0.039 mg/kg dry 1 B4K1909 11/19/04 11/19/04 EPA 8260B Trichloroethene <0.29 0.29 0.047 mg/kg dry 1 Trichlorofluoromethane <0.29 0.29 0.036 mg/kg dry 1 Vinyl chloride <0.29 0.29 0.038 mg/kg dry 1 II Surrogate:4-Bromofluorobenzene 87.2 75-125 % I Surrogate:Dibromofluoromethane 87.8 75-125 % III Surrogate:Toluene-d8 86.0 75.5-125 % N I I I I I I I I I I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance I with the chain of custody document. This analytical report must be reproduced in its entirety. IPage 15 of 33 L E G E N D I775 Vandalia Street 1 St Paul,MN 55114 Technical Services, Inc. 651.642.1150 I GME Consultants, Inc Project: Senior Housing Partners ' 14000 21st Ave N Project Number: 7735-E Date Reported: Minneapolis MN, 55447 Project Manager: Mr. Eric Stommes November 30,2004 II DRO/8015B - Quality Control LEGEND Technical Services, Inc Reporting Spike Source %REC %RPD I Analyte Result Limit Units Level Result %REC Limits %RPD Limit Notes Batch B4K1916-Sonication (Wisc DRO) 1 Blank(B4K1916-BLK1) Prepared: 11/19/04 Analyzed: 11/21/04 Diesel Range Organics <8.0 8.0 mg/kg wet Surrogate:C-30 11.5 mg/kg wet 16.0 71.9 60-130 I LCS(B4K1916-BS1) Prepared: 11/19/04 Analyzed: 11/21/04 Diesel Range Organics 58.4 8.0 mg/kg wet 64.0 91.2 70-120 Surrogate:C-30 14.8 mg/kg wet 16.0 92.5 60-130 LCS Dup(B4K1916-BSD1) Prepared: 11/19/04 Analyzed: 11/22/04 I Diesel Range Organics OR-02 46.4 8.0 mg/kg wet 64.0 72.5 70-120 22.9 20 Surrogate:C-30 13.9 mg/kg wet 16.0 86.9 60-130 I I I I 1 I I I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 16 of 33 t ■ IL E G E D 775 Vandalia Street St Paul,MN 55114 651.642.1150 ITechnical Services, Inc, tGME Consultants, Inc Project: Senior Housing Partners 14000 21st Ave N Project Number: 7735-E Date Reported: Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 GRO/8021 B - Quality Control LEGEND Technical Services, Inc IReporting Spike Source %REC %RPD Analyte Result Limit Units Level Result %REC Limits %RPD Limit Notes IBatch B4K1902 -EPA 5035 Soil (Purge and Trap) Blank(B4K1902-BLK1) Prepared&Analyzed: 11/19/04 Gasoline range organics ii. <5.0 5.0 mg/kg wet Surrogate:4-Fluorochlorobenzene 24.3 ug/L 25.0 97.2 80-120 LCS(B4K1902-BS1) Prepared&Analyzed: 11/19/04 Gasoline range organics 1050 ug/L 1000 105 80-120 Surrogate:4-Fluorochlorobenzene 28.2 ug/L 25.0 113 80-120 ILCS Dup(B4K1902-BSD1) Prepared: 11/19/04 Analyzed: 11/20/04 Gasoline range organics 1040 ug/L 1000 104 80-120 0.957 20 Surrogate:4-Fluorochlorobenzene 27.1 ug/L 25.0 108 80-120 Duplicate(B4K1902-DUP1) Source: 0403947-17 Prepared: 11/19/04 Analyzed: 11/20/04 Gasoline range organics <5.7 5.7 mg/kg dry <5.7 NA 20 �Surrogate:4-Fluorochlorobenzene 24.2 ug/L 25.0 96.8 80-120 Matrix Spike(B4K1902-MS1) Source:0403947-17 Prepared: 11/19/04 Analyzed: 11/20/04 1Surrogate:4-Fluorochlorobenzene 27.4 ug/L 25.0 110 80-120 I I I I I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance I with the chain of custody document. This analytical report must be reproduced in its entirety. • Page 17 of 33 LE E D 775 Vandaiia Street I St Paul,MN 55114 Technical Services, Inc. 651.642.1150 GME Consultants, Inc Project: Senior Housing Partners I 14000 21st Ave N Project Number: 7735-E Date Reported: Minneapolis MN, 55447 Project Manager: Mr. Eric Stommes November 30,2004 TOTAL METALS ANALYSIS - Quality Control LEGEND Technical Services, Inc Reporting Spike Source %REC %RPD I Analyte Result Limit Units Level Result %REC Limits %RPD Limit Notes Batch B4K2201 -EPA 3050B I Blank(B4K2201-BLK1) Prepared&Analyzed: 11/22/04 Arsenic <0.50 0.50 mg/kg wet I Barium <1.0 1.0 mg/kg wet Cadmium <0.25 0.25 mg/kg wet Chromium <0.50 0.50 mg/kg wet Lead <1.0 1.0 mg/kg wet Selenium <0.50 0.50 mg/kg wet I Silver <0.25 0.25 mg/kg wet LCS (B4K2201-BS1) Prepared&Analyzed: 11/22/04 I Arsenic 38.4 0.50 mg/kg wet 40.0 96.0 80-120 Barium 39.8 1.0 mg/kg wet 40.0 99.5 80-120 1 Cadmium 39.9 0.25 mg/kg wet 40.0 99.8 80-120 Chromium 39.0 0.50 mg/kg wet 40.0 97.5 80-120 Lead 39.8 1.0 mg/kg wet 40.0 99.5 80-120 III Selenium 37.9 0.50 mg/kg wet 40.0 94.8 80-120 Silver 3.95 0.25 mg/kg wet 4.00 98.8 80-120 1 LCS Dup(B4K2201-BSD1) Prepared&Analyzed: 11/22/04 Arsenic 38.5 0.50 mg/kg wet 40.0 96.2 80-120 0.260 20 1 Barium 39.2 1.0 mg/kg wet 40.0 98.0 80-120 1.52 20 Cadmium 39.9 0.25 mg/kg wet 40.0 99.8 80-120 0.00 20 1 Chromium 39.0 0.50 mg/kg wet 40.0 97.5 80-120 0.00 20 Lead • 39.8 1.0 mg/kg wet 40.0 99.5 80-120 0.00 20 Selenium 38.0 0.50 mg/kg wet 40.0 95.0 80-120 0.264 20 Silver 3.95 0.25 mg/kg wet 4.00 98.8 80-120 0.00 20 LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 18 of 33 II 1 LEGEND 775 Vandalic Street St Paul,MN 55114 651.642.1150 ITechnical Services, Inc. 1 GME Consultants, Inc Project: Senior Housing Partners 14000 21st Ave N Project Number: 7735-E Date Reported: I Minneapolis MN, 55447 Project Manager: Mr. Eric Stommes November 30,2004 TOTAL METALS ANALYSIS - Quality Control LEGEND Technical Services, Inc IReporting Spike Source %REC %RPD Analyte Result Limit Units Level Result %REC Limits %RPD Limit Notes IBatch B4K2201 -EPA 3050B Matrix Spike(B4K2201-MS1) Source:0404039-01 Prepared&Analyzed: 11/22/04 Arsenic 111 0.60 mg/kg dry 48.3 61.5 102 75-125 Barium 202 1.2 mg/kg dry 48.3 161 84.9 75-125 Cadmium g g dry 48.3 0.509 43.8 0.30 m /k d 89.6 75-125 I Chromium 9 g dry 13.7 57.4 0.60 m /k d 48.3 90.5 75-125 Lead QM-4X 288 1.2 mg/kg dry 48.3 223 135 75-125 1 Selenium g g dry <0.60 43.3 0.60 m /k d 48.3 89.1 75-125 Silver 4.64 0.30 mg/kg dry 4.83 <0.30 92.8 75-125 IMatrix Spike Dup(B4K2201-MSD1) Source: 0404039-01 Prepared&Analyzed: 11/22/04 Arsenic 105 0.60 mg/kg dry 48.3 61.5 90.1 75-125 5.56 20 Barium I214 1.2 mg/kg dry 48.3 161 110 75-125 5.77 20 Cadmium 43.7 0.30 mg/kg dry 48.3 0.509 89.4 75-125 0.229 20 Chromium 58.3 0.60 mg/kg dry 48.3 13.7 92.3 75-125 1.56 20 Lead 214 1.2 mg/kg dry 48.3 223 NR 75-125 29.5 20 QM-4X,QR- 04 Selenium 9 9 dry <0.60 43.0 0.60 m /k d 48.3 < 88.5 75-125 0.695 20 ,Silver 4.58 0.30 mg/kg dry 4.83 <0.30 91.6 75-125 1.30 20 Batch B4K2307 -EPA 7471A IBlank(B4K2307-BLK1) Prepared&Analyzed: 11/23/04 Mercury <0.10 0.10 mg/kg wet ILCS(B4K2307-BS1) Prepared&Analyzed: 11/23/04 Mercury 0.206 0.10 mg/kg wet 0.200 103 80-120 ILCS Dup(B4K2307-BSD1) Prepared&Analyzed: 11/23/04 Mercury 0.218 0.10 mg/kg wet 0.200 109 80-120 5.66 20 I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance I with the chain of custody document. This analytical report must be reproduced in its entirety. 1 Page 19 of 33 L E G E D 775 Vandalia Street L St Paul,MN 55114 Technical Services, Inc 651.642.1150 GME Consultants, Inc Project: Senior Housing Partners 1 14000 21st Ave N Project Number: 7735-E Date Reported: Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 TOTAL METALS ANALYSIS - Quality Control LEGEND Technical Services, Inc Reporting Spike Source %REC %RPD Analyte Result Limit Units Level Result %REC Limits %RPD Limit Notes Batch B4K2307-EPA 7471A I Matrix Spike(B4K2307-MS1) Source: 0404059-02 Prepared&Analyzed: 11/23/04 Mercury 0.274 0.11 mg/kg dry 0.230 <0.11 88.7 75-125 Source: 0404059-02 Prepared&Anal Matrix Spike Dup(64K2307-MSD1) P Analyzed: 11/23/04 Mercury 0.257 0.11 mg/kg dry 0.230 <0.11 81.3 75-125 6.40 20 • 1 I 1 1 t I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 20 of 33 IL E E 775 Vandalia Street St Paul,MN 55114 ITechnical Services, Inc. 651.642.1150 IGME Consultants, Inc Project: Senior Housing Partners 14000 21st Ave N Project Number: 7735-E Date Reported: I Minneapolis MN, 55447 Project Manager: Mr. Eric Stommes November 30,2004 PAH 8270C - Quality Control LEGEND Technical Services, Inc IReporting Spike Source %REC %RPD Analyte Result Limit Units Level Result %REC Limits %RPD Limit Notes IBatch B4K2216-EPA 3545 ASE Extraction Blank(B4K2216-BLK1) Prepared&Analyzed: 11/22/04 I2-Chloronaphthalene <0.33 0.33 mg/kg wet 2-Methylnaphthalene <0.33 0.33 mg/kg wet Acenaphthene <0.33 0.33 mg/kg wet Acenaphthylene <0.33 0.33 mg/kg wet Anthracene <0.33 0.33 mg/kg wet 1 Benzo(a)anthracene <0.33 0.33 mg/kg wet Benzo(a)pyrene <0.33 0.33 mg/kg wet Benzo(b)fluoranthene <0.33 0.33 mg/kg wet Benzo(g,h,i)perylene <0.33 0.33 mg/kg wet Benzo(k)fluoranthene <0.33 0.33 mg/kg wet Chrysene <0.33 0.33 mg/kg wet Dibenz(a,h)anthracene <0.33 0.33 mg/kg wet IFluoranthene <0.33 0.33 mg/kg wet Fluorene <0.33 0.33 mg/kg wet la Indeno(1,2,3-cd)pyrene <0.33 0.33 mg/kg wet ▪Naphthalene <0.33 0.33 mg/kg wet Phenanthrene <0.33 0.33 mg/kg wet IPyrene <0.33 0.33 mg/kg wet Surrogate:2-Fluorobiphenyl 4.80 mg/kg wet 6.67 72.0 38.1-115 ▪Surrogate:Nitrobenzene-d5 4.09 mg/kg wet 6.67 61.3 39.4-115 Surrogate:Terphenyl-dl4 5.38 mg/kg wet 6.67 80.7 36.1-115 �LCS (B4K2216-BS1) Prepared&Analyzed: 11/22/04 cenaphthene 4.75 0.33 mg/kg wet 6.67 71.2 37.5-115 Pyrene 4.60 0.33 mg/kg wet 6.67 69.0 30.2-115 'Surrogate:2-Fluorobiphenyl 5.35 mg/kg wet 6.67 80.2 38.1-115 LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance I with the chain of custody document. This analytical report must be reproduced in its entirety. IPage 21 of 33 I L E E D 775 Vandalia Street I St Paul,MN 55114 Technical Services, Inc. 651.642.1150 1 GME Consultants, Inc Project: Senior Housing Partners I 14000 21st Ave N Project Number: 7735-E Date Reported: Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 II PAH 8270C -Quality Control LEGEND Technical Services, Inc Reporting Spike Source %REC %RPD I Analyte Result Limit Units Level Result %REC Limits %RPD Limit Notes Batch B4K2216-EPA 3545 ASE Extraction I LCS(B4K2216-BS1) Prepared&Analyzed: 11/22/04 Surrogate:Nitrobenzene-d5 4.78 mg/kg wet 6.67 71.7 39.4-115 Surrogate:Terphenyl-d14 5.36 mg/kg wet 6.67 80.4 36.1-115 1 Matrix Spike(B4K2216-MS1) Source:0404059-03 Prepared&Analyzed: 11/22/04 Acenaphthene g 9 dry <1.5 1 5.77 1.5 m /k d 7.70 72.9 30-115 Pyrene 8.37 1.5 mg/kg dry 7.70 2.41 77.4 30-115 Surrogate:2-Fluorobiphenyl 6.87 mg/kg dry 7.70 89.2 38.1-115 Surrogate:Nitrobenzene-d5 5.88 mg/kg dry 7.70 76.4 39.4-115 I Surrogate:Terphenyl-d14 6.81 mg/kg dry 7.70 88.4 36.1-115 Matrix Spike Dup(B4K2216-MSD1) Source:0404059-03 Prepared&Analyzed: 11/22/04 1 Acenaphthene g g 5.52 1.5 mg/kg d ry 7.71 <1.5 69.5 30-115 4.43 40 Pyrene 7.55 1.5 mg/kg dry 7.71 2.41 66.7 30-115 10.3 37.8 1 Surrogate:2-Fluorobiphenyl 6.33 mg/kg dry 7.71 82.1 38.1-115 Surrogate:Nitrobenzene-d5 5.46 mg/kg dry 7.71 70.8 39.4-115 Surrogate:Terphenyl-d14 6.43 mg/kg dry 7.71 83.4 36.1-115 1 I I I I I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 22 of 33 1 111L- EGEND 775 Vendalia Street St Paul,MN 55114 ITechnical Services, Inc. 651.642.1150 1 GME Consultants, Inc Project: Senior Housing Partners 14000 21st Ave N Project Number: 7735-E Date Reported: I Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 PCB 8082 - Quality Control LEGEND Technical Services, Inc 1 Reporting Spike Source %REC %RPD Analyte Result Limit Units Level Result %REC Limits %RPD Limit Notes IBatch B4K1922 -EPA 3545 ASE Extraction Blank(B4K1922-BLK1) Prepared: 11/19/04 Analyzed: 11/22/04 it PCB-1016 <0.20 0.20 mg/kg wet PCB-1221 <0.20 0.20 mg/kg wet PCB-1232 <0.20 0.20 mg/kg wet PCB 1242 <0.20 0.20 mg/kg wet PCB-1248 <0.20 0.20 mg/kg wet PCB-1254 <0.20 0.20 mg/kg wet • PCB-1260 <0.20 0.20 mg/kg wet Surrogate:Decachlorobiphenyl 0.0613 mg/kg wet 0.0667 91.9 62.8-130 Surrogate:Tetrachloro-meta-xylene 0.0657 mg/kg wet 0.0667 98.5 72.3-130 LCS(B4K1922-BS2) Prepared: 11/19/04 Analyzed: 11/22/04 I PCB-1260 0.326 0.20 mg/kg wet 0.333 97.9 70-128 Surrogate:Decachlorobiphenyl 0.0650 mg/kg wet 0.0667 97.5 62.8-130 Surrogate:Tetrachloro-meta-xylene 0.0653 mg/kg wet 0.0667 97.9 72.3-130 Matrix Spike(B4K1922-MS2) Source: 0404059-03 Prepared: 11/19/04 Analyzed: 11/23/04 PCB-1260 0.463 0.23 mg/kg dry 0.386 <0.23 120 72.5-127 Surrogate:Decachlorobiphenyl 0.0667 mg/kg dry 0.0772 86.4 62.8-130 Surrogate:Tetrachloro-meta-xylene 0.0883 mg/kg dry 0.0772 114 72.3-130 IMatrix Spike Dup(B4K1922-MSD2) Source: 0404059-03 Prepared: 11/19/04 Analyzed: 11/23/04 PCB-1260 0.474 0.23 mg/kg dry 0.387 <0.23 122 72.5-127 2.35 30 Surrogate:Decachlorobiphenyl 0.0650 mg/kg dry 0.0774 84.0 62.8 130 Surrogate: Tetrachloro-meta-xylene 0.0894 mg/kg dry 0.0774 116 72.3-130 I I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance I with the chain of custody document. This analytical report must be reproduced in its entirety. 1 Page 23 of 33 LE E D 775 Vendalia Street I St Paul,MN 55114 Technical Services, Inc. 651.642.1150 GME Consultants, Inc Project: Senior Housing Partners I 14000 21st Ave N Project Number: 7735-E Date Reported: Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 PERCENT SOLIDS - Quality Control I LEGEND Technical Services, Inc Reporting Spike Source %REC %RPD I Analyte Result Limit Units Level Result %REC Limits %RPD Limit Notes Batch B4K2218 -General Preparation I Duplicate(B4K2218-DUP1) Source:0404010-18 Prepared: 11/22/04 Analyzed: 11/23/04 Solids 80.0 % 79.0 1.26 20 Duplicate(B4K2218-DUP2) Source:0404010-30 Prepared: 11/22/04 Analyzed: 11/23/04 %Solids 87.0 % 86.0 1.16 20 Duplicate(B4K2218-DUP3) Source: 0404059-03 Prepared: 11/22/04 Analyzed: 11/23/04 Solids 87.0 % 86.0 1.16 20 I I I I I I I I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page24of33I IIILEGEND 775 Vandalia Street St Paul,MN 55114 Technical Services, Inc. 651.642.1150 IGME Consultants, Inc Project: Senior Housing Partners 14000 21st Ave N Project Number: 7735-E Date Reported: I Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 PESTICIDES SOIL 8081A - Quality Control LEGEND Technical Services, Inc Reporting Spike Source %REC %RPD Analyte Result Limit Units Level Result %REC Limits %RPD Limit Notes IBatch B4K1922 -EPA 3545 ASE Extraction Blank(B4K1922-BLK1) Prepared: 11/19/04 Analyzed: 11/22/04 I4,4'-DDD <0.040 0.040 mg/kg wet 4,4"-DDE <0.040 0.040 mg/kg wet 4,4"-DDT <0.040 0.040 mg/kg wet a-Chlordane <0.040 0.040 mg/kg wet Aldrin <0.040 0.040 mg/kg wet Ialpha-BHC <0.040 0.040 mg/kg wet beta-BHC <0.040 0.040 mg/kg wet delta-BHC <0.040 0.040 mg/kg wet Dieldrin <0.040 0.040 mg/kg wet Endosulfan I <0.040 0.040 mg/kg wet Endosulfan II <0.040 0.040 mg/kg wet Endosulfan sulfate <0.040 0.040 mg/kg wet IEndrin <0.040 0.040 mg/kg wet Endrin aldehyde <0.040 0.040 mg/kg wet 1Endrin ketone <0.040 0.040 mg/kg wet gamma-Bl-lC(Lindane) <0.040 0.040 mg/kg wet gamma-Chlordane <0.040 0.040 mg/kg wet 'Heptachlor <0.040 0.040 mg/kg wet Heptachlor epoxide <0.040 0.040 mg/kg wet IMethoxychlor <0.040 0.040 mg/kg wet Toxaphene <0.040 0.040 mg/kg wet Surrogate:Decachlorobiphenyl 0.0613 mg/kg wet 0.0667 91.9 60-141 Surrogate: Tetrachloro-meta-xylene 0.0657 mg/kg wet 0.0667 98.5 70-133 1LCS (B4K1922-BSI) Prepared: 11/19/04 Analyzed: 11/22/04 LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance I with the chain of custody document. This analytical report must be reproduced in its entirety. IPage 25 of 33 LE E D 775 Vandalia Street I St Paul,MN 55114 Technical Services, Inc. 651.642.1150 II GME Consultants, Inc Project: Senior Housing Partners I 14000 21st Ave N Project Number: 7735-E Date Reported: Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 PESTICIDES SOIL 8081A - Quality Control LEGEND Technical Services, Inc Reporting Spike Source %REC %RPD I Analyte Result Limit Units Level Result %REC Limits %RPD Limit Notes Batch B4K1922 -EPA 3545 ASE Extraction I LCS (B4K1922-BS1) Prepared: 11/19/04 Analyzed: 11/22/04 4,4'-DDD 0.158 0.040 mg/kg wet 0.167 94.6 60-140 1 4,4"-DDE 0.169 0.040 mg/kg wet 0.167 101 60-139 4,4"-DDT 0.177 0.040 mg/kg wet 0.167 106 60-140 a-Chlordane 0.168 0.040 mg/kg wet 0.167 101 60-137 Aldrin 0.175 0.040 mg/kg wet 0.167 105 60-136 alpha-BHC 0.182 0.040 mg/kg wet 0.167 109 60-138 1 beta-BHC 0.170 0.040 mg/kg wet 0.167 102 60-140 delta-BHC 0.179 0.040 mg/kg wet 0.167 107 60-138 1 Dieldrin 0.167 0.040 mg/kg wet 0.167 100 60-137 Endosulfan I 0.167 0.040 mg/kg wet 0.167 100 60-130 Endosulfan II 0.160 0.040 mg/kg wet 0.167 95.8 60-133 I Endosulfan sulfate 0.163 0.040 mg/kg wet 0.167 97.6 60-138 Endrin 0.170 0.040 mg/kg wet 0.167 102 60-140 1 Endrin aldehyde 0.153 0.040 mg/kg wet 0.167 91.6 60-130 Endrin ketone 0.165 0.040 mg/kg wet 0.167 98.8 60-136 1 gamma-BHC(Lindane) 0.178 0.040 mg/kg wet 0.167 107 60-136 gamma-Chlordane 0.167 0.040 mg/kg wet 0.167 100 60-136 Heptachlor 0.180 0.040 mg/kg wet 0.167 . 108 60-136 1 Heptachlor epoxide 0.169 0.040 mg/kg wet 0.167 101 60-136 Methoxychlor 0.163 0.040 mg/kg wet 0.167 97.6 60-140 1 Surrogate:Decachlorobiphenyl 0.0630 mg/kg wet 0.0667 94.5 60-141 Surrogate:Tetrachloro-meta-xylene 0.0713 mg/kg wet 0.0667 107 70-133 1 Matrix Spike(B4K1922-MS1) Source: 0404059-03 Prepared: 11/19/04 Analyzed: 11/23/04 4,4'-DDD 0.223 0.047 mg/kg dry 0.193 <0.047 104 61-140 i LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be 1 reproduced in its entirety. Page 26 of 33 1 L E E D 775 Vandalia Street St Paul,MN 55114 651.642.1150 ITechnical Services, Inc. IGME Consultants, Inc Project: Senior Housing Partners 14000 21st Ave N Project Number: 7735-E Date Reported: Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 PESTICIDES SOIL 8081A - Quality Control LEGEND Technical Services, Inc Reporting Spike Source %REC %RPD Analyte Result Limit Units Level Result %REC Limits %RPD Limit Notes IBatch B4K1922-EPA 3545 ASE Extraction Matrix Spike(B4K1922-MS1) Source: 0404059-03 Prepared: 11/19/04 Analyzed: 11/23/04 4,4"-DDE 0.229 0.047 mg/kg dry 0.193 <0.047 107 60-140 I 4,4"-DDT 0.201 0.047 mg/kg dry 0.193 <0.047 93.9 60-140 a-Chlordane 0.439 0.047 mg/kg dry 0.193 0.237 105 60.4-140 Aldrin g 9 dry <0.047 0.214 0.047 m /k d 0.193 111 68.9-140 alpha-BHC 0.227 0.047 mg/kg dry 0.193 <0.047 118 70-140 1 beta-BHC dry <0.047 0.207 0.047 mg/kg d 0.193 107 70-140 delta-BHC 0.233 0.047 mg/kg dry 0.193 <0.047 121 70-140 Dieldrin 0.210 0.047 mg/kg dry 0.193 <0.047 109 60-140 Endosulfan I 0.211 0.047 mg/kg dry 0.193 <0.047 109 60-140 Endosulfan II 9 9 dry <0.047 0.205 0.047 m /k d 0.193 106 60-140 Endosulfan sulfate 0.212 0.047 mg/kg dry 0.193 <0.047 110 60.9-140 Endrin 0.218 0.047 mg/kg dry 0.193 <0.047 113 60-140 I Endrin aldehyde 0.161 0.047 mg/kg dry 0.193 <0.047 83.4 60-140 • Endrin ketone 0.204 0.047 mg/kg dry 0.193 <0.047 106 60-140 gamma-BHC(Lindane) 0.221 0.047 mg/kg dry 0.193 <0.047 115 68.8-140 II gamma-Chlordane 0.455 0.047 mg/kg dry 0.193 0.275 93.3 70-140 Heptachlor 0.226 0.047 mg/kg dry 0.193 <0.047 113 66.7-140 Heptachlor epoxide 0.216 0.047 mg/kg dry 0.193 <0.047 97.2 60-140 Methoxychlor 9 9 dry <0.047 0.184 0.047 m /k d 0.193 95.3 60-140 Surrogate:Decachlorobiphenyl 0.0674 mg/kg dry 0.0770 87.5 60-141 Surrogate:Tetrachloro-meta-xylene 0.0847 mg/kg dry 0.0770 110 70-133 'Matrix Spike Dup(B4K1922-MSD1) Source:0404059-03 Prepared: 11/19/04 Analyzed: 11/23/04 4,4'-DDD 0.224 0.047 mg/kg dry 0.194 <0.047 104 61-140 0.447 39 4,4'-DDE 0.223 0.047 mg/kg dry 0.194 <0.047 103 60-140 2.65 • 40 I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance I with the chain of custody document. This analytical report must be reproduced in its entirety. IPage 27 of 33 LE E P1 D 775 Vandalia Street • I St Paul,MN 55114 Technical Services, Inc. 651.642.1150 I GME Consultants, Inc Project: Senior Housing Partners I 14000 21st Ave N Project Number: 7735-E Date Reported: Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 1 PESTICIDES SOIL 8081A - Quality Control LEGEND Technical Services, Inc Reporting Spike Source %REC %RPD I Analyte Result Limit Units Level Result %REC Limits %RPD Limit Notes Batch B4K1922 -EPA 3545 ASE Extraction Matrix Spike Dup(B4K1922-MSD1) Source: 0404059-03 Prepared: 11/19/04 Analyzed: 11/23/04 4,4'-DDT 0.216 0.047 mg/kg dry 0.194 <0.047 101 60-140 7.19 40 I a-Chlordane 0.458 0.047 mg/kg dry 0.194 0.237 114 60.4-140 4.24 30 Aldrin 0.224 0.047 mg/kg dry 0.194 <0.047 115 68.9-140 4.57 37 alpha-BHC 9 g dry <0.047 0.239 0.047 m /k d 0.194 123 70-140 5.15 30 beta-BHC 0.213 0.047 mg/kg dry 0.194 <0.047 110 70-140 2.86 30 delta-BHC 0.244 0.047 mg/kg dry 0.194 <0.047 126 70-140 4.61 30 Dieldrin 0.202 0.047 mg/kg dry 0.194 <0.047 104 60-140 3.88 35 Endosulfan I 0.201 0.047 mg/kg dry 0.194 <0.047 104 60-140 4.85 35.5 I Endosulfan II 0.199 0.047 mg/kg dry 0.194 <0.047 103 60-140 2.97 40 Endosulfan sulfate 0.206 0.047 mg/kg dry 0.194 <0.047 106 60.9-140 2.87 30 1 Endrin 9 9 dry <0.047 0.215 0.047 m /k d 0.194 111 60-140 1.39 37.8 Endrin aldehyde 9 g dry <0.047 0.171 0.047 m /k d 0.194 88.1 60-140 6.02 40 Endrin ketone 9 g dry <0.047 0.199 0.047 m /k d 0.194 103 60-140 2.48 30 1 gamma-BHC(Lindane) 9 9 dry <0.047 0.233 0.047 m /k d 0.194 120 68.8-140 5.29 30 gamma-Chlordane 0.499 0.047 mg/kg dry 0.194 0.275 115 70-140 9.22 39.9 1 Heptachlor 9 g dry <0.047 0.238 0.047 m /k d 0.194 118 66.7-140 5.17 30 Heptachlor epoxide 0.227 0.047 mg/kg dry 0.194 <0.047 102 60-140 4.97 30 1 Methoxychlor 0.168 0.047 mg/kg dry 0.194 <0.047 86.6 60-140 9.09 38.3 Surrogate:Decachlorobiphenyl 0.0666 mg/kg dry 0.0774 86.0 60-141 Surrogate: Tetrachloro-meta-xylene 0.0902 mg/kg dry 0.0774 117 70-133 1 • I • • I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be I reproduced in its entirety. Page 28 of 33 I 1 L E E D 775 Vandalia Street St Paul,MN 55114 ITechnical Services, Inc . 651.642.1150 GME Consultants, Inc Project: Senior Housing Partners 14000 21st Ave N Project Number: 7735-E Date Reported: Minneapolis MN, 55447 Project Manager: Mr. Eric Stommes November 30,2004 VOC GCMS 8260B - Quality Control LEGEND Technical Services, Inc Reporting Spike Source %REC %RPD Analyte Result Limit Units Level Result %REC Limits %RPD Limit Notes IBatch B4K1909 -Volatiles Blank(B4K1909-BLK1) Prepared&Analyzed: 11/19/04 1,1,1,2-Tetrachloroethane I <0.50 0.50 mg/kg wet 1,1,1-Trichloroethane <0.25 0.25 mg/kg wet 1,1,2,2-Tetrachloroethane <0.25 0.25 mg/kg wet I 1,1,2-Trichloroethane <0.25 0.25 mg/kg wet 1,1,2-Trichlorotrifluoroethane <0.25 0.25 mg/kg wet 1,1-Dichloroethane <0.25 0.25 mg/kg wet 1,1-Dichloroethene <0.25 0.25 mg/kg wet 1,1-Dichloropropene <0.25 0.25 mg/kg wet 1,2,3-Trichlorobenzene <0.50 0.50 mg/kg wet 1,2,3-Trichloropropane <0.50 0.50 mg/kg wet I ,2,4-Trichlorobenzene <0.50 0.50 mg/kg wet 1,2,4-Trimethylbenzene <0.25 0.25 mg/kg wet 1,2-Dibromo-3-chloropropane I <0.50 0.50 mg/kg wet 1,2-Dibromoethane(EDB) <0.25 0.25 mg/kg wet 1,2-Dichlorobenzene <0.25 0.25 mg/kg wet ,2-Dichloroethane <0.25 0.25 mg/kg wet 1,2-Dichloropropane <0.25 0.25 mg/kg wet I ,3,5-Trimethylbenzene <0.25 0.25 mg/kg wet 1,3-Dichlorobenzene <0.25 0.25 mg/kg wet j3-Dlchloropropane <0.25 0.25 mg/kg wet 1,4-Dichlorobenzene <0.25 0.25 mg/kg wet 1,2-Dichloropropane <0.50 0.50 mg/kg wet -Butanone <2.0 2.0 mg/kg wet 2-Chlorotoluene I <0.25 0.25 mg/kg wet LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance I with the chain of custody document. This analytical report must be reproduced in its entirety. 1 Page 29 of 33 IILEGEND 775 Vandalic Street I St Paul,MN 55114 Technical Services, Inc. 651.642.1150 1 GME Consultants, Inc Project: Senior Housing Partners 1 14000 21st Ave N Project Number: 7735-E Date Reported: Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 1 VOC GCMS 8260B -Quality Control LEGEND Technical Services, Inc IReporting Spike Source %REC %RPD Analyte Result Limit Units Level Result %REC Limits %RPD Limit Notes Batch B4K1909-Volatiles Blank(B4K1909-BLK1) Prepared&Analyzed: 11/19/04 4-Chtorotoluene <0.25 0.25 mg/kg wet I Acetone <2.0 2.0 mg/kg wet Ally!chloride • <0.50 0.50 mg/kg wet Benzene <0.25 0.25 mg/kg wet Bromobenzene <0.25 0.25 mg/kg wet Bromochloromethane <0.25 0.25 mg/kg wet I Bromodichloromethane <0.25 0.25 mg/kg wet Bromoform <0.50 0.50 mg/kg wet I Bromomethane <0.50 0.50 mg/kg wet Carbon tetrachloride <0.25 0.25 mg/kg wet Chlorobenzene <0.25 0.25 mg/kg wet I Chloroethane <0.50 0.50 mg/kg wet Chloroform <0.25 0.25 mg/kg wet I. Chloromethane <0.25 0.25 mg/kg wet cis-1,2-Dichloroethene <0.25 0.25 mg/kg wet I cis-1,3-Dichloropropene <0.25 0.25 mg/kg wet Dibromochloromethane <0.25 0.25 mg/kg wet Dibromomethane <0.50 0.50 mg/kg wet I Dichlorodifluoromethane <0.50 0.50 mg/kg wet Dichtorofluoromethane <0.25 0.25 mg/kg wet I Ethyl ether <0.25 0.25 mg/kg wet Ethylbenzene <0.25 0.25 mg/kg wet I Hexachlorobutadiene <0.50 0.50 mg/kg wet lsopropylbenzene <0.25 0.25 mg/kg wet LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 30 of 331 IIILEGEND 775 Vandalic Street St Paul,MN 55114 ITechnical Services, Inc. 651.642.1150 GME Consultants, Inc Project: Senior Housing Partners 14000 21st Ave N Project Number: 7735-E Date Reported: Minneapolis MN, 55447 Project Manager: Mr. Eric Stommes November 30,2004 VOC GCMS 8260B - Quality Control ILEGEND Technical Services, Inc Reporting Spike Source %REC %RPD Analyte Result Limit Units Level Result %REC Limits %RPD Limit Notes IBatch B4K1909 -Volatiles Blank(B4K1909-BLK1) Prepared&Analyzed: 11/19/04 Im,p-Xylene <0.50 0.50 mg/kg wet Methyl isobutyl ketone <0.50 0.50 mg/kg wet Methyl tert-butyl ether <0.25 0.25 mg/kg wet Methylene chloride <1.5 1.5 mg/kg wet Naphthalene <0.50 0.50 mg/kg wet I n-Butylbenzene <0.25 0.25 mg/kg wet n-Propylbenzene <0.25 0.25 mg/kg wet o-Xylene <0.25 0.25 mg/kg wet p-Isopropyltoluene <0.25 0.25 mg/kg wet sec-Butylbenzene <0.25 0.25 mg/kg wet Styrene <0.25 0.25 mg/kg wet tert-Butylbenzene <0.25 0.25 mg/kg wet I Tetrachloroethene <0.25 0.25 mg/kg wet Tetrahydrofuran <2.0 2.0 mg/kg wet 1 Toluene <0.25 0.25 mg/kg wet trans-1,2-Dichloroethene <0.25 0.25 mg/kg wet trans-1,3-Dichloropropene <0.25 0.25 mg/kg wet Trichioroethene <0.25 0.25 mg/kg wet Trichlorofluoromethane <0.25 0.25 mg/kg wet Vinyl chloride <0.25 0.25 mg/kg wet Surrogate:4-Bromofluorobenzene 41.6 ug/L 50.0 83.2 75-125 'Surrogate:Dibromofluoromethane 44.5 ug/L 50.0 89.0 75-125 Surrogate: Toluene d8 43.1 ug/L 50.0 86.2 75.5-125 LCS (B4K1909-BS1) Prepared&Analyzed: 11/19/04 11,1-Dichloroethene 0 . 40.3 ug/L 50.0 80.6 76.1-120 in LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance . I with the chain of custody document. This analytical report must be reproduced in its entirety. Page 31 of 33 LEGEND 775 Vandalic Street St Paul,MN 55114 651.642.1150 ITechnical Services, inc. GME Consultants, Inc Project: Senior Housing Partners I 14000 21st Ave N Project Number: 7735-E Date Reported: Minneapolis MN,55447 Project Manager: Mr.Eric Stommes November 30,2004 VOC GCMS 8260B - Quality Control LEGEND Technical Services, Inc I Reporting Spike Source %REC %RPD Analyte Result Limit Units Level Result %REC Limits %RPD Limit Notes Batch B4K1909-Volatiles I LCS(B4K1909-BS1) Prepared&Analyzed: 11/19/04 Benzene 48.4 ug/L 50.0 96.8 80-120 1 Chlorobenzene 51.2 ug/L 50.0 102 80-120 Toluene 48.5 ug/L 50.0 97.0 80-120 Trichloroethene 50.9 ug/L 50.0 102 80-120 Surrogate:4-Bromofluorobenzene 43.7 ug/L 50.0 87.4 75-125 Surrogate:Dibromofluoromethane 45.6 ug/L 50.0 91.2 75-125 Surrogate:Toluene-d8 43.4 ug/L 50.0 86.8 75.5-125 Matrix Spike(B4K1909-MS1) Source: 0404044-09 Prepared&Analyzed: 11/19/04 1,1-Dichloroethene 40.9 ug/L 50.0 < 81.8 75-120 1 Benzene 48.2 ug/L 50.0 < 96.4 80-120 Chlorobenzene 51.8 ug/L 50.0 < 104 80-120 1 Toluene 48.0 ug/L 50.0 0.280 95.4 80-120 Trichloroethene 51.5 ug/L 50.0 < 103 80-120 1 Surrogate:4-Bromofluorobenzene 44.3 ug/L 50.0 88.6 75-125 Surrogate:Dibromofluoromethane 44.3 ug/L 50.0 88.6 75-125 Surrogate:Toluene-d8 42.4 ug/L 50.0 84.8 75.5-125 1 Matrix Spike Dup(B4K1909-MSD1) Source:0404044-09 Prepared&Analyzed: 11/19/04 1,1-Dichloroethene 39.9 ug/L 50.0 < 79.8 75-120 2.48 20 I Benzene 47.9 ug/L 50.0 < 95.8 80-120 0.624 20 Chlorobenzene 52.5 ug/L 50.0 < 105 80-120 1.34 20 Toluene 48.2 ug/L 50.0 0.280 95.8 80-120 0.416 20 Trichloroethene 51.6 ug/L 50.0 < 103 80-120 0.194 20 Surrogate:4-Bromofluorobenzene 43.9 ug/L 50.0 87.8 75-125 Surrogate:Dibromofluoromethane 43.3 ug/L 50.0 86.6 75-125 Surrogate:Toluene-d8 42.3 ug/L 50.0 84.6 75.5-125 I LEGEND Technical Services, Inc The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 32 of 33 EG E 0 775 Vandalia Street St Paul,MN 55114 I I Technical Services, Inc. 651.642.1150 IGME Consultants, Inc 14000 21st Ave N Project: Senior Housing Partners Project Number: 7735-E Date Reported: I Minneapolis MN,55447 Project Manager: Mr. Eric Stommes November 30,2004 Notes and Definitions IQR-04 The RPD value for the MS/MSD was outside of QC acceptance limits. Data was accepted based on LCS and/or LCSD recovery and/or RPD values. IQR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data. QM-4X The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration.The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. L1 Results in the diesel organics range are primarily due to overlap from a heavy oil range product. A Sample does not display a fuel pattern. Sample contains several discreet peaks. I < Less than value listed dry Sample results reported on a dry weight basis IRPD Relative Percent Difference NA Not applicable. The%RPD is not calculated from values less than the reporting limit. I I I I I I I I LEGEND Technical Services, Inc The results in this PAY I report apply to the samples analyzed in accordance P with the chain of custody document. This analytical report must be reproduced in its entirety. I Page 33 of 33 -n s a� A G j Fr 2 D `O CO J T v, A w N - 3 7 N o . A D., o Z z y .� ,_.i N V, v, .� •• O o p c 'C) .O c .......Ti of •■,) .""C) er..M . 7' .. W W �s % 0 I 3 ` a i Q ( 1 Wo `. CA S CA C N � .f ---ii ) cb -t- ...pet.....I. ..N ..c. s.. c... N' - c) -- -, - 6 ' 4 d- • 3 [� 1%1� ru CA cn -j -7 ao r, C7 < w e, — a a ©Vl 4 vo , rn r■) z witi.tr —I— to co ii (� 1, • - O b r. o 07 —) 7.3 w _ °c o o c H .:p - - -i 0 wU O 3 o co 3 .- �� VJ � U . C r � c \1 - f •,• o o --] d r emu ro' 1t na n' o ' rn 0 , 4i ', !I \' 1 L'-;_'' nil ` OO !. .=et t N r.y . o y a QC '- C7 0, •s e N. O '7 7( Ph Hs-T170 -C- t n o w r x -...4 OD I x > 2,9-D+ .2,yi,6---;'QCs, v , I I TestAAmerica ANALYTICAL TESTING CORPORATION I 2060 FOSTER C itEIGHfOA DRIVE•NASHVILLE,TENvessISIS 37204 800-765.0080•615-726-3404 Fax IANALYTICAL REPORT ILEGEND TECHNICAL SERVICES 9421 Lab Number: 04-A182730 Sample ID: 0404059-01 775 VANDALIA STREET II ST. PAUL, MN 55114 Sample Type: Soil Site ID: Date Collected: 11/17/04 Project : 0404059 I Project Name: Time Collected: Sampler: Date Received: 11/20/04 Time Received: 8 :10 I Analyte Report Dil Result Units Anal______________________ Limit Factor Date Time Analyst Method -__________ Unit_ Batch I ------ ---------- *PESTICIDE/PCB's/HERBICIDES* I 2,4-D mg/kg 0.167 0.0167 2,4-D ND (Silvex) 1 11/23/04 22:58 M. Ricke 8151A ND mg/kg 1 11/23/04 22:58 M. Ricke 8684 8151A 8684 ISample Extraction Data Wt/Vol Parameter Extracted Extract Vol Date Time Analyst Method ---------------- ----------- -------- ----- Herbicides 30. gm 10.0 ml 11/22/04 III J. Davis 8151 Surrogate 4 Recovery Target Range iHerbicide Surr., DCAA 108. 50. - 130. ILABORATORY COMMENTS: ND = Not detected at the report limit. B = Analyte was detected in the method blank. J = Estimated Value below Report Limit. E = Estimated Value above the calibration limit of the instrument. # = Recovery outside Laboratory historical or method prescribed limits. All results reported on a wet weight basis. I I II End of Sample Report. TestAmerica ANALYTICAL TESTING CORPORATION 2900 FosrER CKEIOMrOA DRIVE•NAEBV'ILLR,TENASSKE 37204 800-765-0980•615-726-3404 FAX ANALYTICAL REPORT TECHNICAL SERVICES 9421 Lab Number: 04-A182732 LEGEND TEC Sample ID: 0404059-03 Sample Type: Soil 775 VANDALIA STREET Site ID: ST. PAUL, MN 55114 Date Collected: 11/17/04 Time Collected: Project:Name: 9 Date Received: 11/20/04 Project Name: Time Received: 8 :10 Sampler: Report Dil Analyst Method Batch Result Units Limit Factor Date Time Y Analyte •PESTICIDE/PCB's/HERBICIDES* 8684 mg/kg 0.167 1 11/24/04 0:01 M. Ricke 8151A 2 4-D ND 2,4,5-TP (Silvex) ND mg/kg 0.0167 1 11/24/04 0:01 M. Ricke 8151A 8684 Sample Extraction Data Wt/Vol Method Parameter Extracted Extract Vol Date Time Analyst Herbicides 30. gm 10.0 ml 11/22/04 J. Davis 8151 % Recovery Target Range Surrogate 108. 50. - 130. Herbicide Surr., DCAA 111 LABORA TORY COMMENTS: 111 ND = Not detected at the report limit. B = Analyte was detected in the method blank. J = Estimated Value below Report Limit. E = Estimated Value above the calibration limit of the instrument. # = Recovery outside Laboratory historical or method prescribed limits. All results reported on a wet weight basis. 1 End of Sample Report. II 1 Test America ANALYTICAL TESTING CORPORATION 1/ 2960 FOSTNR CANIGMTON Delve•NAS8VILLN,TeNVNSSNN 37204 800-765.0980•615-726-3404 Fax II ANALYTICAL REPORT ILEGEND TECHNICAL SERVICES 9421 Lab Number: 04-A182731 Sample ID: 0404059-02 775 VANDALIA STREET I ST. PAUL, MN 55114 Sample T Site ID:YPe Soil Date Collected: Project : 0404059 I Project Name: Time Collected; 11/17/04 Sampler: Date Received: 11/20/04 8 Time Received: 11:: 10 r . Analyte Report Dil Result Units I ------------------------- Limit Factor Date Method Time Analyst Meth ---- Batch *PESTICIDE/PCB's/HERBICIDES+ 11. 1 2,4-D 2,4,5-TP (Silvex) ND mg/kg 0.167 1 11/23/04 23:30 M. ND mg/kg 0.0167 1 Ricke 8151A 11/23/04 23:30 8484 M. Ricke 8151A 8684 _________________________ Sample Extraction Data ----'-'----------------- Wt/Vol ' Parameter Extracted ---- Extract Vol Date Time Analyst Method --------- Herbicides III 30. gm 10.0 ml 11/22/04 J. Davis 8151 Surrogate Recovery Target Range Herbicide Surr., DCAA 104. 50. - 130. I/ LABORATORY COMMENTS: ND = Not detected at the report limit. B = Analyte was detected in the method blank. II J = Estimated Value below Report Limit. E = Estimated Value above the calibration limit of the instrument. # = Recovery outside Laboratory historical or method prescribed limits. All results reported on a wet weight basis. 1 IIEnd of Sample Report. i Test A merica ANALYTICAL TESTING CORPORATION 'L960 F957YSM(;ReicN•ron DRIVE•NASHVILLE,TENNESSEE 37204 800-703-(1980•615-726-3404 Fax 1 PROJECT QIIALITY CONTROL DATA Project Number: 0404059 Project Name: Laboratory 1 Receipt Date: 11/20/04 Laboratory Matrix Spike Recovery le spiked, insufficient volume was received for the defined analytical batch for Note: If Blank is referenced as the pamp reagent water was used for QC purposes. Batch Spike Sample MS/MSD analysis on an true sample matrix. Laboratory V 9 Spike Conc Recovery Target Range Q.C. units Orig. Val. MS Val Analyte --'-'"""-- 8684 04-A182732 **PEST/PCB/HERB PARAMETERS** 0.167 96 24. - 126. 111< 0.167 0.161 8684 04-A182732 mg/kg 0.167 105 18. - 121. 2,4-D 0.0167 0.175 2,4,5-TP (Silvex) mg/kg Matrix Spike Duplicate 111 units Orig. Analyte Val. Duplicate RPD Limit Q.C. Batch -----'--------- **PEST/PCB/HERB PARAMETERS** 0.161 0.146 9.77 49. 8684 0. mg/kg 3 49 qg, 8684 2,4-D 0.175 0.169 2,4,5-TP (Silvex) mg/kg Laboratory Control Data 111 Val. Analyzed Val % Recovery Target Range Q.C. Batch "-- Analyte units ----- "-----—" ---- PARAMETERS** 85 45 - 114 8684 **PEST/PCB/HERB PARAM 0.167 0.142 mg/kg 21 - 121 8684 2,4-D 0.0939 56 2 q 5_Tp (Silvex) mg/kg 0.167 Duplicates units Orig. Val. Duplicate RPD Limit Q.C. Batch Sample Dup'd Analyte Project QC continued . • • 1 1 Testt�merica ANALYTICAL TESTING CORPORATION 2960 Fosrsw CRCH:HTOr DR1VK•N:\SHVILLR,TENVISSaRR 37204 800-763-0980•615-726-3404 FAX i 1 PROJECT QUALITY CONTROL DATA Project Number: 0404059 Project Name: 1 Page: 2 Laboratory Receipt Date: 11/20/04 • Blank Data ' Analyte Blank Value Units Q.C. Batch Date Analyzed Time Analyzed I **PEST/PCB/HERB PARAMETERS** 4-D < 0.166 mg/kg 8684 11/23/04 20:52 2,4,5-TP (Silvex) < 0.0166 mg/kg 8684 11/23/04 20:52 Herbicide Surr., DCAA 52. % Rec 8684 11/23/04 20:52 # = Value outside Laboratory historical or method prescribed QC limits. 1 1 i 1 1 1 1 1 End of Report for Project 397523 1 ./ EMSL Analytical, Inc, EMSL I14375 23rd Avenue North,Minneapolis,Alfa 55447 Phone; (763)449-4922 Fax: (763)449-4924 Email minneapoli slab(5�etnsl.corn son IAttn: Michelle Hosfield Customer ID: GMEC50 GME Consultants Customer PO: 1 14000 21st Avenue Received: 11/17/04 2:00 PM Minneapolis, MN 55447 EMSL Order: 350404494 Fax: (763)559-0720 Phone: (763)559-1859 I EMSL Proj: Project: Analysis Date: 11/17/2004 Report Date: 11/17/2004 Il Asbestos Analysis of Bulk Materials - y Is via EPA 600/R 93/116 Method using Polarized I Light Microscopy Non-Asbestos Asbestos Sample Location Appearance % Fibrous % Non-Fibrous % Type ISH-1 Shingles in west Black 5% Synthetic 85% Non-fibrous(other) None Detected 350404494-0001 excavation Fibrous 10% Cellulose Heterogeneous ISH-2 Shingles in west Black 5% Synthetic 85% Non-fibrous(other) None Detected 350404494-0002 excavation Fibrous 10% Cellulose Heterogeneous ISH-3 Shingles in west Black 5% Synthetic 85% Non-fibrous(other) None Detected 350404494-0003 excavation Fibrous 10% Cellulose Heterogeneous SHTPE-1 Shingle in test pit Black 15% Synthetic 85% Non-fibrous(other) None Detected 350404494-0004 to the east Fibrous <1% Cellulose Heterogeneous SHSE-1 Shingle in test pit Black 5% Synthetic 85% Non-fibrous(other) None Detected 350404494-0005 to the southeast Fibrous 10% Cellulose Heterogeneous PFT-1 Peach floor tile& Tan 100% Non-fibrous(other) <1% Chrysotile 350404494-0006 mastic Non-Fibrous Heterogeneous i r �1 Analyst(s) / i� Ll4 .----- Erin Witt old or other approved signatory Due to magnification limitations inherent in PLM,asbestos fibers in dimensions below the resolution capability of PLM may not be detected. Samples reported as<1%or none detected may require additional testing by TEM to confirm asbestos quantities. The above test report relates only to the items tested and may not be reproduced in any form without the express written approval of EMSL Analytical,Inc. EMSL's liability is limited to the cost of analysis. EMSL bears no responsibility for sample collection activities or analytical method limitations. Interpretation and use of test results are the responsibility of the client. Analysis performed by EMSL Minneapolis(NVLAP#200019-0) LM-1 THIS IS THELASTPAGE OFTFIE REPORT. 1 I 14375 23rd Avenue North Minneapolis, MN bb441 rnone: _/ .4-444-4yLL rax: /of-44w- + i�� '' g d L EMSL �U It - ANALYTICAL CHAIN OF CUSTODY , ASBESTOS I EMSL Representative: EMSL Reference#: 3503 Your Company Name: 0/7 1�' 3' f /S _ EMSL-Bill to: Same ' Street: /yo o° 2/54 Ave /V, Street: Box#: Box#: City/State: n'/ /s MP/ Zip: Ss9y'7 City/State: Zip: IVerbal Results to: JJ/i�'/, 46 cle/ Fax Results to: Telephone#: 763 - SS 9'—r''SS Fax#: 763- Ss9-0 71.0 Project Name/Number: Qo Park ,4"eilti.A' Purchase Order# MATRIX TURNAROUND TIME II ❑ Air ❑ Floor Tile ❑ Soil ❑ Wipe RRUSH ❑ 6 Hours ❑ 24 Hours ❑ 48 Hours ,l Bulk ❑ Drinking ❑ Dust ❑ Waste Contact Lab ❑'3 Days ❑ 5 Days ❑ 6-10 days IWater water PCM PLM ❑ NIOSH 7400 •g EPA 600/R-93/116 ❑ Comments: I ❑ MN Dept of Health ❑ NOB ❑ Other: ❑ Point Count(400 point) ❑ Test Until Positive I ❑ Other: TEM AIR TEM BULK TEM WATER TEM WIPE ❑ AHERA ❑ Chatfield ❑ EPA 100.1 (all fibers) ❑ Quantitative ❑ EPA Level II ❑ NOB ❑ EPA 100.2(Long fibers>10um) ❑ Qualitative ❑ NIOSH 7402 ❑ Micro Vac-Quantitative ❑ NY 198.2 1 ❑ MN Dept of Health ❑ Micro Vac-Qualitative TEM DUST ❑ Drop Mount-Qualitative ❑ ASTM D-5755-95 ❑ Qualitative l Client Sample#(s) S#- / - 7F 7' / Total Samples: 6 Relinquished: ' Date: /l-i 7-off' Time: -2,o z 73 o--, Received: Date: I i I 1-7 Time: - ,_0-z} �x�t IReceived: Date: Time: / " SAMPLE DATE SAMPLE NUMBER LOCATION VOLUME(If Applicable) ii //--/7-09 s//-/ 5‘,4,iay1($ ill --4t/4-5/ tXCava/ibh II S//-Z. 5H=3 IS/47-FE- I Shwpt9/c '. 7i5-i y,` fo /4 .eas� SI-ts--/ 51141, L /:, s7/J p/5( 710 Soc#/6 a IV ?' T / /-Cl.c,4 �r / f/12aS'IL/G I I I i I I I 1 1 I APPENDIX E IGME PHOTOGRAPHIC RECORD 1 I 1 I i I I i GME CONSULTANTS, INC. PHOTOGRAPHIC RECORD I LOCATION: OutlotE GME PROJECT NO. : 7735-E Oakgreen Avenue North and 58th Street North Oak Park Heights,Minnesota II'°t Photograph No. : 1 'L .T Date: March 3 , 2005 1 "4 c ' A. 't kr ti F :, .. Comments ' l 4 _ View of excavation ,�C looking west (Area 1) •1 rt . I °"`t . � ,. Photograph No. : 2 ,.; ° 1�= Date: March 3 , 2005 Comments: � f View of excavation ` looking north (Area 1) . 1 I - - ,. r GME CONSULTANTS, INC. rPHOTOGRAPHIC RECORD I LOCATION: Outlot Et GME PROJECT NO' : 7735-E_735 Oakgreen Avenue North and 58th Street North Oak Park Heights,Minnesota 4, Photograph No14: 3 '101,)-9'1"E �� y� 7 xk � $P t M p, � " r � �,� �' , 1''' Date: March , 2005 +,, !' 1 2 e > + E., . ■ r lib 'Al! j',1,�9 '-' Comments err a 1. ..�. 1 ,z y 1 I e r� `r�i� View of excavtion and ��? ffeir ,� � backfilling looking , ' ""` - '! northeast (Area 1)44 H >. t r'",y x,,' t 4 n r • • ,ir , :,.., ,,:,:..,.„.,......:„...,..:.„,„:„......„.„,„:„„:„.,,.„,„,„,, , ., • •_. 1 . ., , , „..... . , . ., ,..._ ,, , , „ , . ,,,.. ,....,_. ....,:,,,..,„,,,„:„.,,T„,,,, ..... ,.:.:_..,:,...„,: :,„:,..,, ti.4.--,:i, .4.:,,,,,.,,, _., -,, -. Ia I ,': �t Photograph No. : 4 s. j — ° ' � � „4111 � ;;, Date: March 4 , 2005 I �'� ,y+� a rt Comments: � View of excavation looking east, clean fill soil is apparent I • °• in the foreground (Area 1) . I g• a ir,r is, 'tSRida u':'L.^ + r I I GME CONSULTANTS, INC. 1 PHOTOGRAPHIC RECORD LOCATION: Outlot E GME PROJECT NO. : 7735-E I Oakgreen Avenue North and 58"'Street North Oak Park Heights,Minnesota , . , Photograph No. : 5 ` Date: March 8 2005 6 9 W ".dam "t�,x . ~ xi .•'3` , -• Comments: * ° �,. ,. View of former P. .. floorslab in Area 3 . ,, `, 4 1 x _ a £ y { 1 h Y µ *,- r" v id atGt. ' .. Y I i _ Photograph No. : 6 ra < •_ „ . =. Date: March 8, 2005 ,� �:. :z. ; Comments. View of Area 2 ,. - excavation. , . r .. n , ' : " '' ' '' ' ,,,. ' .?,.iif : c .. '3^ "' - ms's #� ""_�.s ,x. a ;' .k,..e., "*:'...i.:11,.,.c- x �•+s '. J'� . *a , "° aa,'+„ te , , , ;.; • I I 1 I I i • 1 APPENDIX F ENCHEM, INC. LABORATORY REPORTS 1 1 I I I I I I En Chem Analytical Report Number: 856908 1241 Bellevue Street 1 A Division of Pace Analytical Services, Inc. Green Bay,WI 54302 920-469-2436 Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: SOIL I Project Name: OAK PARK HEIGHTS Collection Date: 03/03/05 Project Number: 7735-E Report Date: 03/29/05 Field ID: B-3(3') Lab Sample Number: 856908-003 I INORGANICS Test Result EQL Dilution Units Code Atli Date Prep Method AnI Method Arsenic 2.5 0.34 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 I Barium 54 0.34 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Cadmium < 0.11 0.11 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Chromium 17 0.34 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 I Lead 4.2 0.28 5 mg/Kg 03/17/05 SW846 30508 SW846 6020 Mercury < 0.011 0.011 1 mg/Kg 03/16/05 SW846 7471A SW846 7471A Selenium < 1.1 1.1 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Silver < 0.34 0.34 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 IPercent Solids 88.9 — 1 % 03/10/05 SM 2540G M SM 2540G M DIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 Analyte Result EQL Dilution Units Code An'Date Prep Method AnI Method Diesel Range Organics < 4.0 4.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike 90 --- 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO I DRO Blank Spike Duplicate 93 -- 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO PAH/PNA Prep Date: 03/10/05 I Analyte Result EQL Dilution Units Code An!Date Prep Method Ant Method 1-Methylnaphthalene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM 2-Methylnaphthalene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM IAcenaphthene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Acenaphthylene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Anthracene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM IBenzo(a)anthracene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(a)pyrene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(b)fluoranthene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(ghi)perylene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(k)fluoranthene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Chrysene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Dibenz(a,h)anthracene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Fluoranthene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM I Fluorene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Indeno(1,2,3-cd)pyrene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Naphthalene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM IPhenanthrene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Pyrene. < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Nitrobenzene-d5 67 -- 1 %Recov 03/10/05 SW846 3545 8270C-SIM I2-Fluorobiphenyl 69 1 %Recov 03/10/05 SW846 3545 8270C-SIM Terphenyl-d14 83 1 %Recov 03/10/05 SW846 3545 8270C-SIM PAH/PNA BLANK Prep Date: 03/10/05 IAnalyte Result EQL Dilution Units Code AnI Date Prep Method Anl Method PAH Blank ID 1497-19 1 IPESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code AnI Date Prep Method Ani Method 4,4'-DDD < 5.6 5.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A IAll soil results are reported on a dry weight basis unless otherwise noted. I En Chem Analytical Report Number: 856908 1241 Bellevue Street Green Bay,WI 54302 A Division of Pace Analytical Services, Inc. 920-469-2436 I Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/03/05 Project Number: 7735-E Report Date: 03/29/05 I Field ID: B-3(3') Lab Sample Number: 856908-003 PESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 I Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method 4,4'-DDE < 5.6 5.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A 4,4'-DDT < 5.6 5.6 1 ug/kg 03/25/05 SW846 35508 SW846 8081A I Aldrin < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A alpha-BHC < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A beta-BHC < 2.8 2.8 1 ug/kg 03/25/05 SW846 35508 SW846 8081A I Chlordane,Technical < 56 56 1 ug/kg 03/25/05 SW846 3550B SW846 8081A delta-BHC < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Dieldrin < 5.6 5.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan I < 2.8 2.8 1 ug/kg 03/25/05 SW846 35508 SW846 8081A Endosulfan II < 5.6 5.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan Sulfate < 5.6 5.6 1 ug/kg 03/25/05 SW846 35508 SW846 8081A Endrin < 5.6 5.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endrin Aldehyde < 5.6 5.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A gamma-BHC(Lindane) < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Heptachlor < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Heptachlor Epoxide < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I Toxaphene < 280 280 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Tetrachloro-m-xylene 87 — 1 %Recov 03/25/05 SW846 3550B SW846 8081A Decachlorobiphenyl 90 — 1 %Recov 03/25/05 SW846 3550B SW846 8081A I I I I I I I I I All soil results are reported on a dry weight basis unless otherwise noted. I I En Chem Analytical Report Number: 856908 1241 Bellevue Street I Green Bay,WI 54302 A Division of Pace Analytical Services, Inc. 920-469-2436 Client: GME CONSULTANTS,INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/03/05 Project Number: 7735-E Report Date: 03/29/05 Field ID: B 4(5') Lab Sample Number: 856908-004 INORGANICS Test Result EQL Dilution Units Code AnI Date Prep Method AnI Method Arsenic 2.5 0.34 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 I Barium 53 0.34 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Cadmium < 0.11 0.11 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Chromium 20 0.34 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 I Lead 4.4 0.28 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Mercury < 0.011 0.011 1 mg/Kg 03/16/05 SW846 7471A SW846 7471A Selenium < 1.1 1.1 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Silver < 0.34 0.34 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Percent Solids 88.5 --- 1 % 03/10/05 SM 2540G M SM 2540G M DIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Atli Method IDiesel Range Organics < 4.4 4.4 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike 90 -- 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO IDRO Blank Spike Duplicate 93 — 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO PAH/PNA Prep Date: 03/10/05 Analyte Result EQL Dilution Units Code AnI Date Prep Method AnI Method 1-Methylnaphthalene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 2-Methylnaphthalene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Acenaphthene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM IAcenaphthylene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Anthracene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(a)anthracene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM IBenzo(a)pyrene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(b)fluoranthene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(ghi)perylene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM IBenzo(k)fluoranthene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Chrysene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Dibenz(a,h)anthracene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Fluoranthene 32 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 1 Fluorene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Indeno(1,2,3-cd)pyrene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Naphthalene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM IPhenanthrene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Pyrene 29 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Nitrobenzene-d5 79 --- 1 %Recov 03/11/05 SW846 3545 8270C-SIM 2-Fluorobiphenyl 80 — 1 %Recov 03/11/05 SW846 3545 8270C-SIM ITerphenyl-d14 97 -- 1 %Recov 03/11/05 SW846 3545 8270C-SIM PAH/PNA BLANK Prep Date: 03/10/05 IAnalyte Result EQL Dilution Units Code AnI Date Prep Method Anl Method PAH Blank ID 1497-19 1 PESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 IAnalyte Result EQL Dilution Units Code AnI Date Prep Method Ani Method 4,4'-DOD < 5.7 5.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A All soil results are reported on a dry weight basis unless otherwise noted. En Chem Analytical Report Number: 856908 1241 Bellevue Street or umer: l y p Green Bay,WI 54302 A Division of Pace Analytical Services, Inc. 920-469-2436 I Client: GME CONSULTANTS,INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/03/05 Project Number: 7735-E Report Date: 03/29/05 I Field ID: B-4(5) Lab Sample Number: 856908-004 PESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code AnI Date Prep Method AnI Method 4,4'-DDE < 5.7 5.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A 4,4'-DDT < 5.7 5.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A 1 Aldrin < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A alpha-BHC < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A beta-BHC < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Chlordane,Technical < 57 57 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I delta-BHC < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Dieldrin < 5.7 5.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan I < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan II < 5.7 5.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan Sulfate < 5.7 5.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endrin < 5.7 5.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endrin Aldehyde < 5.7 5.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I gamma-BHC(Lindane) < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Heptachlor < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Heptachlor Epoxide < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I Toxaphene < 280 280 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Tetrachloro-m-xylene 83 -- 1 %Recov 03/25/05 SW846 3550B SW846 8081A Decachlorobiphenyl 86 — 1 %Recov 03/25/05 SW846 3550B SW846 8081A I I I I I I I I All soil results are reported on a dry weight basis unless otherwise noted. I I En Chem Analytical Report Number: 856908 1241 Bellevue Street �/ p Green Bay,WI 54302 A Division of Pace Analytical Services, Inc. 920469-2436 Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/03/05 I Project Number: 7735-E Report Date: 03/29/05 Field ID: B-5(9') Lab Sample Number: 856908-005 IINORGANICS Test Result EQL Dilution Units Code Anl Date Prep Method AnI Method Arsenic 1.9 0.33 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 I Barium 40 0.33 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Cadmium 0.13 0.11 5 mg/Kg 03/17/05 SW846 30508 SW846 6020 Chromium 14 0.33 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Lead 5.6 0.28 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 I Mercury < 0.011 0.011 1 mg/Kg 03/16/05 SW846 7471A SW846 7471A Selenium < 1.1 1.1 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Silver < 0.33 0.33 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 IPercent Solids 90.2 — 1 % 03/10/05 SM 2540G M SM 2540G M DIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 I Analyte Result EQL Dilution Units Code AnI Date Prep Method AnI Method Diesel Range Organics < 4.3 4.3 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike 90 -- 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO IDRO Blank Spike Duplicate 93 -- 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO PAH/PNA Prep Date: 03/10/05 IAnalyte Result EQL Dilution Units Code AnI Date Prep Method AnI Method 1-Methylnaphthalene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 2-Methylnaphthalene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM IAcenaphthene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Acenaphthylene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Anthracene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(a)anthracene 29 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM IBenzo(a)pyrene 36 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(b)fluoranthene 30 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(ghi)perylene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM IBenzo(k)fluoranthene 31 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Chrysene 32 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Dibenz(a,h)anthracene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Fluoranthene 47 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM I Fluorene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Indeno(1,2,3-cd)pyrene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Naphthalene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Phenanthrene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Pyrene 45 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Nitrobenzene-d5 74 -- 1 %Recov 03/11/05 SW846 3545 8270C-SIM I2-Fluorobiphenyl 80 - 1 %Recov 03/11/05 SW846 3545 8270C-SIM Terphenyl-d14 95 1 %Recov 03/11/05 SW846 3545 8270C-SIM PAH/PNA BLANK Prep Date: 03/10/05 IAnalyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method PAH Blank ID 1497-19 1 PESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 IAnalyte Result EQL Dilution Units Code AnI Date Prep Method AnI Method 4,4'-DDD < 5.5 5.5 1 ug/kg 03/25/05 SW846 35508 SW846 8081A IAll soil results are reported on a dry weight basis unless otherwise noted. En Chem Analytical Report Number: 856908 1241 Bellevue Street I y p Green Bay,WI 54302 A Division of Pace Analytical Services,Inc. 920-469-2436 I Client: GME CONSULTANTS,INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/03/05 1 Project Number: 7735-E Report Date: 03/29/05 I Field ID: B-5(9') Lab Sample Number: 856908-005 PESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method 4,4'-DDE < 5.5 5.5 1 ug/kg 03/25/05 SW846 3550B SW846 8081A 4,4'-DDT < 5.5 5.5 1 ug/kg 03/25/05 SW846 3550B SW846 8081A i Aldrin < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A alpha-BHC < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A beta-BHC < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Chlordane,Technical < 55 55 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I delta-BHC < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Dieldrin < 5.5 5.5 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan I < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I Endosulfan II < 5.5 5.5 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan Sulfate < 5.5 5.5 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endrin < 5.5 5.5 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endrin Aldehyde < 5.5 5.5 1 ug/kg 03/25/05 SW846 3550B SW846 8081A gamma-BHC(Lindane) < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Heptachlor < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Heptachlor Epoxide < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I Toxaphene < 280 280 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Tetrachloro-m-xylene 80 — 1 %Recov 03/25/05 SW846 3550B SW846 8081A Decachlorobiphenyl 85 — 1 %Recov 03/25/05 SW846 3550B SW846 8081A I I I I I I I I I All soil results are reported on a dry weight basis unless otherwise noted. I I En Chem Analytical Report Number: 856908 1241 Bellevue Street y P Green Bay,WI 54302 IA Division of Pace Analytical Services, Inc. 920-469-2436 Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/03/05 I Project Number: 7735-E Report Date: 03/29/05 Field ID: B-6(3') Lab Sample Number: 856908-006 IINORGANICS Test Result EQL Dilution Units Code Anl Date Prep Method Anl Method Arsenic 3.1 0.34 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 IBarium 67 0.34 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Cadmium < 0.11 0.11 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Chromium 22 0.34 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 ILead 5.1 0.28 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Mercury 0.016 0.011 1 mg/Kg 03/16/05 SW846 7471A SW846 7471A Selenium < 1.1 1.1 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Silver < 0.34 0.34 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Percent Solids 89.2 — 1 % 03/10/05 SM 2540G M SM 2540G M DIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 I Analyte Result EQL Dilution Units 1 mg/kg Code Anl Date Prep Method Anl Method Diesel Range Organics < 4.4 4.4 03/11/05 WI MOD DRO WI MOD DRO DRO Blank < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike 90 - 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike Duplicate 93 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO PAH/PNA Prep Date: 03/10/05 IAnalyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method 1-Methylnaphthalene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM 2-Methylnaphthalene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM IAcenaphthene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Acenaphthylene < 28 28 1 ug/Kg * 03/10/05 SW846 3545 8270C-SIM Anthracene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(a)anthracene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM IBenzo(a)pyrene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(b)fluoranthene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(ghi)perylene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM IBenzo(k)fluoranthene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Chrysene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Dibenz(a,h)anthracene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM I Fluoranthene Fluorene < 28 28 1 ug/Kg ug/Kg 03/10/05 SW846 3545 8270C-SIM < 28 28 1 03/10/05 SW846 3545 8270C-SIM Indeno(1,2,3-cd)pyrene < 28 28 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Naphthalene < 28 28 1 ug/Kg B 03/10/05 SW846 3545 8270C-SIM I Phenanthrene < 28 28 1 ug/Kg ug/Kg 03/10/05 SW846 3545 8270C-SIM Pyrene < 28 28 1 03/10/05 SW846 3545 8270C-SIM Nitrobenzene-d5 80 --- 1 %Recov 03/10/05 SW846 3545 8270C-SIM I2-Fluorobiphenyl 83 - 1 %Recov 03/10/05 SW846 3545 8270C-SIM Terphenyl-d14 96 1 %Recov 03/10/05 SW846 3545 8270C-SIM PAH/PNA BLANK Prep Date: 03/10/05 IAnalyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method PAH Blank ID 1497-19 1 IPESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Ant Date Prep Method Anl Method 4,4'-DDD < 5.6 5.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A IAll soil results are reported on a dry weight basis unless otherwise noted. I En Chem Analytical Report Number: 856908 1241 Bellevue Street Green Bay,WI 54302 A Division of Pace Analytical Services, Inc. 920-469-2436 I Client: GME CONSULTANTS,INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/03/05 Project Number: 7735-E Report Date: 03/29/05 I Field ID: B-6(3') Lab Sample Number: 856908-006 PESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method 4,4'-DDE < 5.6 5.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A 4,4'-DDT < 5.6 5.6 1 ug/kg P 03/25/05 SW846 3550B SW846 8081A I Aldrin < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A alpha-BHC < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A beta-BHC < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Chlordane,Technical < 56 56 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I delta-BHC < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Dieldrin < 5.6 5.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan I < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I Endosulfan II < 5.6 5.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan Sulfate < 5.6 5.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endrin < 5.6 5.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I Endrin Aldehyde < 5.6 5.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A gamma-BHC(Lindane) < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Heptachlor < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Heptachlor Epoxide < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I Toxaphene < 280 280 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Tetrachloro-m-xylene 82 --- 1 %Recov 03/25/05 SW846 3550B SW846 8081A Decachlorobiphenyl 87 — 1 %Recov 03/25/05 SW846 3550B SW846 8081A I I I I I I I I I All soil results are reported on a dry weight basis unless otherwise noted. I I En Chem Analytical Report Number: 856908 1241 Bellevue Street r P Green Bay,WI 54302 I A Division of Pace Analytical Services, Inc. 920-469-2436 Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/03/05 I Project Number: 7735-E Report Date: 03/29/05 Field ID: B-7(4') Lab Sample Number: 856908-007 IINORGANICS Test Result EQL Dilution Units Code Anl Date Prep Method Anl Method Arsenic 1.7 0.32 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 IBarium 43 0.32 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Cadmium < 0.11 0.11 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Chromium 17 0.32 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 ILead 3.2 0.27 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Mercury < 0.011 0.011 1 mg/Kg 03/16/05 SW846 7471A SW846 7471A Selenium < 1.1 1.1 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Silver < 0.32 0.32 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Percent Solids 93.0 -- 1 % 03/10/05 SM 2540G M SM 2540G M DIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 Analyte Result EQL Dilution Units Code AnI Date Prep Method Anl Method Diesel Range Organics < 4.2 4.2 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike 90 — 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike Duplicate 93 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO PAH/PNA Prep Date: 03/10/05 IAnalyte Result EQL Dilution Units Code Aril Date Prep Method AnI Method 1-Methylnaphthalene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM 2-Methylnaphthalene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM IAcenaphthene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Acenaphthylene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Anthracene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(a)anthracene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM IBenzo(a)pyrene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(b)fluoranthene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(ghi)perylene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM IBenzo(k)fluoranthene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Chrysene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Dibenz(a,h)anthracene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM IFluoranthene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Fluorene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Indeno(1,2,3-cd)pyrene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Naphthalene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM IPhenanthrene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Pyrene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Nitrobenzene-d5 62 -- 1 %Recov 03/10/05 SW846 3545 8270C-SIM I2-Fluorobiphenyl 72 --- 1 %Recov 03/10/05 SW846 3545 8270C-SIM Terphenyl-d14 96 1 %Recov 03/10/05 SW846 3545 8270C-SIM PAH/PNA BLANK Prep Date: 03/10/05 IAnalyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method PAH Blank ID 1497-19 1 IPESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Ani Method 4,4'-DDD < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A IAll soil results are reported on a dry weight basis unless otherwise noted. I En Chem Analytical Report Number: 856908 1241 Bellevue Street y P Green Bay,WI 54302 A Division of Pace Analytical Services, Inc. 920-469-2436 I Client: GME CONSULTANTS,INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/03/05 Project Number: 7735-E Report Date: 03/29/05 Field ID: B-7(4') Lab Sample Number: 856908-007 PESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method AnI Method 4,4'-DDE < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A 4,4'-DDT < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A 1 Aldrin < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A alpha-BHC < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A beta-BHC < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Chlordane,Technical < 54 54 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I delta-BHC < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Dieldrin < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan I < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I Endosulfan II < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan Sulfate < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endrin < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A 1 Endrin Aldehyde < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A gamma-BHC(Lindane) < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Heptachlor < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Heptachlor Epoxide < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I Toxaphene < 270 270 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Tetrachloro-m-xylene 76 --- 1 %Recov 03/25/05 SW846 35508 SW846 8081A Decachlorobiphenyl 83 -- 1 %Recov 03/25/05 SW846 3550B SW846 8081A I I I I • I I . I I All soil results are reported on a dry weight basis unless otherwise noted. I En Chem Analytical Report Number: 856908 1241 Bellevue Street Green Bay,WI 54302 A Division of Pace Analytical Services, Inc. 920-469-2436 Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/04/05 I Project Number: 7735-E Report Date: 03/29/05 Field ID: B-8(4') Lab Sample Number: 856908-008 I INORGANICS Test Result EQL Dilution Units Code Anl Date Prep Method Anl Method Arsenic 1.7 0.33 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 1 Barium 40 0.33 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Cadmium < 0.11 0.11 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Chromium 17 0.33 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Lead 3.2 0.27 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 IMercury < 0.011 0.011 1 mg/Kg 03/16/05 SW846 7471A SW846 7471A Selenium < 1.1 1.1 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Silver < 0.33 0.33 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Percent Solids 92.7 -- 1 % 03/10/05 SM 2540G M SM'2540G M DIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 Analyte Result EQL Dilution Units Code AnI Date Prep Method Anl Method IDiesel Range Organics < 4.3 4.3 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike 90 — 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO IDRO Blank Spike Duplicate 93 -- 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO PAH/PNA Prep Date: 03/10/05 I Analyte Result EQL Dilution Units Code Anl Date Prep Method AnI Method 1-Methylnaphthalene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM 2-Methylnaphthalene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM IAcenaphthene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Acenaphthylene < 27 27 1 ug/Kg * 03/10/05 SW846 3545 8270C-SIM Anthracene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(a)anthracene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM IBenzo(a)pyrene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(b)fluoranthene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(ghi)perylene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM IBenzo(k)fluoranthene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Chrysene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Dibenz(a,h)anthracene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Fluoranthene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM I Fluorene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Indeno(1,2,3-cd)pyrene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Naphthalene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM IPhenanthrene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Pyrene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Nitrobenzene-d5 70 --- 1 %Recov 03/10/05 SW846 3545 8270C-SIM I2-Fluorobiphenyl 77 -- 1 %Recov 03/10/05 SW846 3545 8270C-SIM Terphenyl-d14 93 1 %Recov 03/10/05 SW846 3545 8270C-SIM PAH/PNA BLANK Prep Date: 03/10/05 IAnalyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method PAH Blank ID 1497-19 1 PESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 IAnalyte Result EQL Dilution Units Code AnI Date Prep Method Anl Method 4,4'-DDD < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A IAll soil results are reported on a dry weight basis unless otherwise noted. I 1241 Bellevue Street En Chem Analytical Report Number: 856908 Green Bay,WI 54302 A Division of Pace Analytical Services, Inc. 920-469-2436 Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/04/05 Project Number: 7735-E Report Date: 03/29/05 Field ID: B-8(4') Lab Sample Number: 856908-008 PESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code AnI Date Prep Method Ani Method 4,4'-DDE < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A 4,4'-DDT < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I Aldrin < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A alpha-BHC < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A beta-BHC < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A i Chlordane,Technical < 54 54 1 ug/kg 03/25/05 SW846 3550B SW846 8081A delta-BHC < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Dieldrin < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan I < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I Endosulfan II < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan Sulfate < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endrin < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A 1 Endrin Aldehyde < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A gamma-BHC(Lindane) < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Heptachlor < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Heptachlor Epoxide < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I Toxaphene < 270 270 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Tetrachloro-m-xylene 74 -- 1 %Recov 03/25/05 SW846 3550B SW846 8081A Decachlorobiphenyl 77 -- 1 %Recov 03/25/05 SW846 3550B SW846 8081A I I I I I I I I All soil results are reported on a dry weight basis unless otherwise noted. • I En Chem Analytical Report Number: 856908 1241 Bellevue Street y P Green Bay,WI 54302 A Division of Pace Analytical Services, Inc. 920-469-2436 Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/04/05 I Project Number: 7735-E Field ID: B-9(7) Report Date: 03/29/05 7') Lab Sample Number: 856908-009 IINORGANICS Test Result EQL Dilution Units Code AnI Date Prep Method Anl Method Percent Solids 91.5 — 1 % 03/10/05 SM 2540G M SM 2540G M I DIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method Diesel Range Organics < 3.9 3.9 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO I DRO Blank < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike 90 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike Duplicate 93 --- 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO IPAH/PNA Prep Date: 03/10/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Aril Method 1-Methylnaphthalene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM I2-Methylnaphthalene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Acenaphthene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Acenaphthylene < 27 27 1 ug/Kg * 03/10/05 SW846 3545 8270C-SIM IAnthracene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(a)anthracene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(a)pyrene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM IBenzo(b)fluoranthene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(ghi)perylene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(k)fluoranthene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Chrysene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM IDibenz(a,h)anthracene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Fluoranthene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Fluorene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM IIndeno(1,2,3-cd)pyrene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Naphthalene < 27 27 1 ug/Kg B 03/10/05 SW846 3545 8270C-SIM Phenanthrene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM 1 Pyrene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Nitrobenzene-d5 85 1 %Recov 03/10/05 SW846 3545 8270C-SIM 2-Fluorobiphenyl 83 --- 1 %Recov 03/10/05 SW846 3545 8270C-SIM Terphenyl-d14 95 — 1 %Recov 03/10/05 SW846 3545 8270C-SIM IPAH/PNA BLANK Prep Date: 03/10/05 Analyte Result EQL Dilution Units Code Ant Date Prep Method AnI Method IPAH Blank ID 1497-19 1 I I I All soil results are reported on a dry weight basis unless otherwise noted. En Chem Analytical Report Number: 856908 1241 Bellevue Street I Green Bay,WI 54302 A Division of Pace Analytical Services, Inc. 920-469-2436 ' Client: GME CONSULTANTS,INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/03/05 Project Number: 7735-E Report Date: 03/29/05 Field ID: S-1 (2') Lab Sample Number: 856908-010 INORGANICS Test Result EQL Dilution Units Code Ani Date Prep Method Ani Method I Arsenic 2.7 0.33 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Barium 51 0.33 5 mg/Kg 03/17/05 SW846 30506 SW846 6020 Cadmium < 0.11 0.11 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 I Chromium 20 0.33 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Lead 4.0 0.27 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Mercury < 0.011 0.011 1 mg/Kg 03/16/05 SW846 7471A SW846 7471A I Selenium < 1.1 1.1 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Silver < 0.33 0.33 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Percent Solids 91.9 — 1 % 03/10/05 SM 2540G M SM 2540G M I DIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 Analyte Result EQL Dilution Units Code Ant Date Prep Method Anl Method Diesel Range Organics < 4.2 4.2 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO I DRO Blank < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike 90 — 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike Duplicate 93 — 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO 1 PAH/PNA Prep Date: 03/10/05 Analyte Result EQL Dilution Units Code Ani Date Prep Method Anl Method 1-Methylnaphthalene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM I 2-Methylnaphthalene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Acenaphthene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Acenaphthylene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM I Anthracene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(a)anthracene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(a)pyrene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(b)fluoranthene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(ghi)perylene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Benzo(k)fluoranthene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Chrysene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Dibenz(a,h)anthracene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Fluoranthene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Fluorene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM I Indeno(1,2,3-cd)pyrene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Naphthalene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Phenanthrene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM I Pyrene < 27 27 1 ug/Kg 03/10/05 SW846 3545 8270C-SIM Nitrobenzene-d5 79 --- 1 %Recov 03/10/05 SW846 3545 8270C-SIM 2-Fluorobiphenyl 80 — 1 %Recov 03/10/05 SW846 3545 8270C-SIM Terphenyl-d14 90 — 1 %Recov 03/10/05 SW846 3545 8270C-SIM I PAH/PNA BLANK Prep Date: 03/10/05 Analyte Result EQL Dilution Units Code Ani Date Prep Method Anl Method I PAH Blank ID 1497-19 1 PESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method I 4,4'-DDD < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A All soil results are reported on a dry weight basis unless otherwise noted. I I En Chem Analytical Report Number: 856908 1241 Bellevue Street Green Bay,WI 54302 III A Division of Pace Analytical Services, Inc. 920-469-2436 Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/03/05 I Project Number: 7735-E Report Date: 03/29/05 Field ID: S-1 (2') Lab Sample Number: 856908-010 IPESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Ani Date Prep Method Ani Method 4,4'-DDE < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I 4,4'-DDT < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Aldrin < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A alpha-BHC < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A beta-BHC < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A IChlordane,Technical < 54 54 1 ug/kg 03/25/05 SW846 3550B SW846 8081A delta-BHC < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Dieldrin < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I Endosulfan I < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan II < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan Sulfate < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endrin < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A IEndrin Aldehyde < 5.4 5.4 1 ug/kg 03/25/05 SW846 3550B SW846 8081A gamma-BHC(Lindane) < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Heptachlor < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A IHeptachlor Epoxide < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Toxaphene < 270 270 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Tetrachloro-m-xylene 85 — 1 %Recov 03/25/05 SW846 3550B SW846 8081A IDecachlorobiphenyl 87 — 1 %Recov 03/25/05 SW846 3550B SW846 8081A I I I I I I I I 111 All soil results are reported on a dry weight basis unless otherwise noted. En Chem Analytical Report Number: 856908 1241 Bellevue Street I Green Bay,W154302 A Division of Pace Analytical Services, Inc. 920-469-2436 I Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date:, 03/03/05 Project Number: 7735-E Report Date: 03/29/05 I Field ID: S-2(2') Lab Sample Number: 856908-011 INORGANICS Test Result EQL Dilution Units Code Anl Date Prep Method Ant Method I Arsenic 2.5 0.35 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Barium 66 0.35 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Cadmium < 0.12 0.12 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 I Chromium 18 0.35 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Lead 5.2 0.29 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Mercury < 0.012 0.012 1 mg/Kg 03/16/05 SW846 7471A SW846 7471A Selenium < 1.2 1.2 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Silver < 0.35 0.35 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Percent Solids 84.7 — 1 % 03/10/05 SM 2540G M SM 2540G M I DIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method Diesel Range Organics < 4.3 4.3 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO I DRO Blank < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike 90 — 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike Duplicate 93 -- 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO I PAH/PNA Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code AnI Date Prep Method AnI Method 1-Methylnaphthalene < 30 30 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM I 2-Methylnaphthalene < 30 30 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Acenaphthene < 30 30 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Acenaphthylene < 30 30 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM I Anthracene < 30 30 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(a)anthracene < 30 30 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(a)pyrene < 30 30 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM I Benzo(b)fluoranthene < 30 30 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(ghi)perylene < 30 30 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(k)fluoranthene < 30 30 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Chrysene < 30 30 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM I Dibenz(a,h)anthracene < 30 30 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Fluoranthene < 30 30 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Fluorene < 30 30 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM I Indeno(1,2,3-cd)pyrene < 30 30 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Naphthalene < 30 30 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Phenanthrene < 30 30 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Pyrene < 30 30 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM I Nitrobenzene-d5 69 — 1 %Recov 03/11/05 SW846 3545 8270C-SIM 2-Fluorobiphenyl 78 — 1 %Recov 03/11/05 SW846 3545 8270C-SIM Terphenyl-d14 89 — 1 %Recov 03/11/05 SW846 3545 8270C-SIM I PAH/PNA BLANK Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method AnI Method I PAH Blank ID 1497-20 1 03/11/05 PESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code AnI Date Prep Method Anl Method Ill 4,4'-DDD < 5.9 5.9 1 ug/kg 03/25/05 SW846 3550B SW846 8081A All soil results are reported on a dry weight basis unless otherwise noted. I I En Chem Analytical Report t Number: 856908 1241 Bellevue Street P Green Bay,WI 54302 A Division of Pace Analytical Services, Inc. 920-469-2436 Client: GME CONSULTANTS, INC-MINNEAPOLIS OL S Matrix Type: SO IL Project Name: OAK PARK HEIGHTS Collection Date: 03/03/05 1 Project Number: 7735-E Report Date: 03/29/05 Field ID: S-2(2') Lab Sample Number: 856908-011 IPESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Ani Date Prep Method AnI Method 4,4'-DDE < 5.9 5.9 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I4,4'-DDT < 5.9 5.9 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Aldrin < 3.0 3.0 1 ug/kg 03/25/05 SW846 3550B SW846 8081A alpha-BHC < 3.0 3.0 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Ibeta-BHC < 3.0 3.0 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Chlordane,Technical < 59 59 1 ug/kg 03/25/05 SW846 3550B SW846 8081A delta-BHC < 3.0 3.0 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Dieldrin < 5.9 5.9 1 ug/kg 03/25/05 SW846 3550B SW846 8081A IEndosulfan I < 3.0 3.0 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan II < 5.9 5.9 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan Sulfate < 5.9 5.9 1 ug/kg 03/25/05 SW846 3550B SW846 8081A IEndrin < 5.9 5.9 1 ug/kg 03/25/05 SW846 35506 SW846 8081A Endrin Aldehyde < 5.9 5.9 1 ug/kg 03/25/05 SW846 3550B SW846 8081A gamma-BHC(Lindane) < 3.0 3.0 1 ug/kg 03/25/05 SW846 3550a SW846 8081A Heptachlor < 3.0 3.0 1 ug/kg 03/25/05 SW846 3550B SW846 8081A IHeptachlor Epoxide < 3.0 3.0 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Toxaphene < 300 300 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Tetrachloro-m-xylene 89 — 1 %Recov 03/25/05 SW846 3550B SW846 8081A IDecachlorobiphenyl 91 — 1 %Recov 03/25/05 SW846 3550B SW846 8081A I 1 I I I I I 1 All soil results are reported on a dry weight basis unless otherwise noted. I En Chem Analytical Report Number: 856908 1241 Bellevue Street Green Bay,WI 54302 A Division of Pace Analytical Services, Inc. 920-469-2436 I Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/03/05 Project Number: 7735-E Report Date: 03/29/05 III Field ID: S-3(2') Lab Sample Number: 856908-012 INORGANICS Test Result EQL Dilution Units Code Anl Date Prep Method Anl Method Arsenic 2.5 0.35 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 j Barium 65 0.35 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Cadmium < 0.12 0.12 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 I Chromium 16 0.35 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Lead 5.8 0.29 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Mercury 0.015 0.012 1 mg/Kg 03/16/05 SW846 7471A SW846 7471A Selenium < 1.2 1.2 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Silver < 0.35 0.35 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Percent Solids 86.5 -- 1 % 03/10/05 SM 2540G M SM 2540G M I DIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method Diesel Range Organics < 4.1 4.1 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO I DRO Blank < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike 90 -- 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike Duplicate 93 — 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO I PAH/PNA Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method I1-Methylnaphthalene < 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 2-Methylnaphthalene < 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Acenaphthene < 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Acenaphthylene < 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM I Anthracene < 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(a)anthracene < 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(a)pyrene < 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(b)fluoranthene < 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(ghi)perylene < 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(k)fluoranthene < 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM IChrysene < 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Dibenz(a,h)anthracene < 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Fluoranthene < 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Fluorene < 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Indeno(1,2,3-cd)pyrene < 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Naphthalene < 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Phenanthrene < 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM , Pyrene < 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Nitrobenzene-d5 75 --- 1 %Recov 03/11/05 SW846 3545 8270C-SIM 2-Fluorobiphenyl 72 — 1 %Recov 03/11/05 SW846 3545 8270C-SIM ITerphenyl-d14 86 — 1 %Recov 03/11/05 SW846 3545 8270C-SIM PAH/PNA BLANK Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method I PAH Blank ID 1497-20 1 03/11/05 PESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method I 4,4'-DOD < 5.8 5.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A All soil results are reported on a dry weight basis unless otherwise noted. 1 ' 1241 Bellevue Street En Chem Analytical Report Number: 856908 g Green Ba ,WI 54302 I A Division of Pace Analytical Services,Inc. Matrix Type: SOIL Client GME CONSULTANTS,INC MINNEAPOLIS Collection Date: 03/03/05 Project Name: OAK PARK HEIGHTS Report Date: 03/29/05 Project Number: 7735-E Lab Sample Number: 856908-012 Field ID: S-3(2') PESTICIDES-PRIORITY POLLUTANT LIST I Prep Date: 03/11/05 Result EQL Dilution Units Code An!Date Prep Method Anl Method 4,4-D a 03/25/05 SW846 35508 SW846 8081A ug/kg 4,4'-DDE < 5.8 5 8 ug/kg 03/25/05 SW846 35508 SW846 8081A 4,4'-DDT < 5.8 5.8 1 < 2.9 03/25/05 SW846 35508 SW846 8081A ' Aldrin 2.9 1 ug/kg < 2 9 2 9 1 ug/kg 03/25/05 SW846 35506 SW846 8081A alpha-BHC ug/kg 03/25/05 SW846 35506 SW846 8081A beta-BHC < 2.9 2.9 1 < 58 58 1 ug/kg 03/25/05 SW846 35508 SW846 8081A Chlordane,Technical 1 ug/kg 03/25/05 SW846 35506 SW846 8081A delta-BHC < 2.9 2.9 < 5.8 5.8 1 ug/kg 03/25/05 SW846 35506 SW846 8081A Dieldrin ug/kg 03/25/05 SW846 35508 SW846 8081A Endosulfan I < 2.9 2.9 1 I < 5 8 5.8 1 ug/kg 03/25/05 SW846 35506 SW846 8081A Endosulfan II ug/kg 03/25/05 SW846 35508 SW846 8081A Endosulfan Sulfate < 5.8 5.8 1 < 5 8 5.8 1 ug/kg 03/25/05 SW846 35506 SW846 8081A Endrin 1 ug/kg 03/25/05 SW846 35508 SW846 8081A III Endrin Aldehyde < 5.8 5.8 < 2 9 2 9 1 ug/kg S 03/25/05 SW846 35506 SW846 8081A gamma-BHC(Lindane) ug/kg 03/25/05 SW846 35506 SW846 8081A Heptachlor < 2.9 2.9 1 < 2 9 2 9 1 ug/kg 03/25/05 SW846 35508 SW846 8081A ' Heptachlor Epoxide 1 ug/kg 03/25/05 SW846 35508 SW846 8081A Toxaphene < 290 290 83 – 1 %Recov 03/25/05 SW846 35506 SW846 8081A Tetrachloro-m-xylene 1 %Recov 03/25/05 SW846 35506 SW846 8081A Decachlorobiphenyl 86 — I I I 1 I I I All soil results are reported on a dry weight basis unless otherwise noted. En Chem Analytical Report Number: 856908 ' A Division of Pace Analytical Services,Inc. 6908 1241 Bellevue Street Green Bay,WI 54302 Client: GME CONSULTANTS, INC-MINNEAPOLIS 920-469-2436 Project Name: OAK PARK HEIGHTS Matrix Type: SOIL Project Number: 7735-E Collection Date: 03/03/05 Field ID: S-4(1') Report Date: 03/29/05 Lab Sample Number: 856908-013 INORGANICS Test EQL Result E Q Dilution Units Code Aril Date Prep Method Aril Method Arsenic Result 0.35 5 2.5 Barium mg/Kg 03/17/05 SW846 3050B SW846 6020 80 0.35 5 mg/Kg Cadmium 0.12 03/17/05 SW846 3050B SW846 6020 0.12 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Chromium 13 Lead 0.35 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 9.3 0.29 5 Mercury 9.361 0.012 mg/Kg 03/17/05 SW846 30508 SW846 6020 Selenium 1 mg/Kg 03/16/05 SW846 7471A SW846 7471A I < 1.2 1.2 5 mg/Kg Silver < 1.35 03/17/05 SW846 30508 SW846 6020 Percent Solids 0.35 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 86.5 — 1 03/10/05 SM 2540G M SM 2540G M DIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 Analyte Result EQL Dilution Units Diesel Range Organics < Code Anl Date Prep Method Anl iMethod 4.2 4.2 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank < 5.0 DRO Blank Spike 5.0 1 mg/kg 03/11/05 WI MOD DRO 90 — 1 %Recov WI MOD DRO DRO Blank Spike Duplicate 93 � 03/11/05 WI MOD DRO WI MOD DRO 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO PAH/PNA I Prep Date: 03/11/05 Analyte Result EQL Q Dilution Units Code Aril Date Prep Method An'Method 1-Methylnaphthalene < 29 29 2-Methylnaphthalene 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM < 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Acenaphthene < 29 29 1 Acenaphthylen 29 ug/Kg 03/11/05 SW846 3545 8270C-SIM < 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Anthracene < 29 29 Anthrac)anthracene 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM < 29 29 1 Benzo(a)pyrene ug/Kg 03/11/05 SW846 3545 8270C-SIM < 29 29 1 ug/Kg 03/11/05 SW846 3545 Benzo(b)fluoranthene < 29 29 8270C-SIM Benzo(b)fluo Benzo(b)fluoranthene < 1 ug/Kg 03/11/05 SW846 3545 29 29 1 8270C-SIM Benzo(k)fluoranthene < 29 29 ug/Kg 03/11/05 SW846 3545 8270C-SIM C < 29 29 1 � ug/Kg 03/11/05 SW846 3545 8270C-SIM Chrysene hrys (a,h)anthracene 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM < 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Dibenz(a,h)anthracene < 29 29 Fluorene 1 ug/Kg 03/11/05 SW846 3545 < 29 29 1 8270C-SIM F uoren ,2,3-cd)pyrene < ug/Kg 03/11/05 SW846 3545 8270C-SIM , 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Naphthalene < 29 29 Naphthalenee 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM < 29 29 Phena < 29 29 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Nitrobenzene-d5 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 68 --- 1 %Recov 03/11/05 SW846 3545 8270C-SIM 2-Fluo Nitrobenzene-d5 77 -_ 2-Fluo nyl d14 1 %Recov 03/11/05 SW846 3545 8270C-SIM 93 — 1 %Recov 03/11/05 SW846 3545 8270C-SIM PAH/PNA BLANK Prep Date: 03/11/05 Analyte Result EQL Dilution Units PAH Blank ID Code Date Prep Method Anl Method 111 1497-20 1 03/03/11/05 PESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Ani Date Prep Method Aril Method 4,4'-DDD < 5.8 5.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A All soil results are reported on a dry weight basis unless otherwise noted. f En Chem Analytical Report Number: 856908 1241 Bellevue Street Green Bay,WI 54302 920-469-2436 A Division of Pace Analytical Services,Inc. Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/03/05 Project Number: 7735-E Report Date: 03/29/05 Field ID: S-4(1') Lab Sample Number: 856908-013 PESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 IAnalyte Result EQL Dilution Units Code Aril Date Prep Method AnI Method 4,4'-DDE < 5.8 5.8 1 ug/kg S 03/25/05 SW846 3550B SW846 8081A I 4,4'-DDT < 5.8 5.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Aldrin < 2.9 2.9 1 ug/kg 03/25/05 SW846 3550B SW846 8081A alpha-BHC < 2.9 2.9 1 ug/kg 03/25/05 SW846 3550B SW846 8081A beta-BHC < 2.9 2.9 1 ug/kg 03/25/05 SW846 3550B SW846 8081A IChlordane,Technical < 58 58 1 ug/kg 03/25/05 SW846 3550B SW846 8081A delta-BHC < 2.9 2.9 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Dieldrin < 5.8 5.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I Endosulfan I < 2.9 2.9 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan II < 5.8 5.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan Sulfate < 5.8 5.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endrin < 5.8 5.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A IEndrin Aldehyde < 5.8 5.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A gamma-BHC(Lindane) < 2.9 2.9 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Heptachlor < 2.9 2.9 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Heptachlor Epoxide I Toxaphene < 2.9 2.9 1 ug/kg ug/kg 03/25/05 SW846 3550B SW846 8081A < 290 290 1 03/25/05 SW846 3550B SW846 8081A Tetrachloro-m-xylene 80 --- 1 %Recov 03/25/05 SW846 3550B SW846 8081A Decachlorobiphenyl 80 --- 1 %Recov 03/25/05 SW846 3550B SW846 8081A I I I I I I I I IAll soil results are reported on a dry weight basis unless otherwise noted. I En Chem Analytical Report Number: 856908 1241 Bellevue Street 111 A Division of Pace Analytical Services, Inc. Green Bay,WI 54302 920-469-2436 Client: GME CONSULTANTS, INC-MINNEAPOLIS Project Name: OAK PARK HEIGHTS Matrix Type: SOIL Project Number: 7735-E Collection Date: 03/04/05 Field ID: S-5(2') Report Date: 03/29/05 Lab Sample Number: 856908-014 ' INORGANICS Test Result EQL Dilution Units Code Anl Date Prep Method AnI Method Arsenic 3.7 0.32 5 Barium 86 0.32 mg/Kg 03/17/05 SW846 3050B SW846 6020 Cadmium mg/Kg 03/17/05 SW846 3050B SW846 6020 0.23 0.11 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Chromium 16 0.32 5 mg/Kg 03/17/05 SW846 30508 SW846 6020 Lead 69 0.27 5 I Mercury mg/K9 03/17/05 SW846 30506 SW846 6020 0.036 0.011 1 mg/Kg 03/16/05 SW846 7471A SW846 7471A Selenium < 1.1 1.1 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Silver < 0.32 0.32 5 Percent Solids 94 0 - mg/Kg 03/17/05 SW846 30506 SW846 6020 1 % 03/10/05 SM 2540G M SM 2540G M DIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 1 Analyte Result EQL Dilution Units Code AnI Date Prep Method AnI Method Diesel Range Organics < 4.0 4.0 DRO Blank 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike 90 __ 1 DRO Blank Spike Duplicate — 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO 93 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO PAH/PNA Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method AnI Method 1-Methylnaphthalene < 27 27 1 2-Methylnaphthalene < ug/Kg 03/11/05 SW846 3545 8270C-SIM 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Acenaphthene < 27 27 1 Acenaphthylene < ug/Kg 03/11/05 SW846 3545 8270C-SIM 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Anthracene < 27 27 1 Anthraa)anthracene ug/Kg 03/11/05 SW846 3545 8270C-SIM < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM I yrene Benzo(a)p < 27 27 Benzo(b)fluoranthene 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(ghi)perylene < 27 27 Benzo(k)fluoranthene < 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Chrysene < 27 27 Chrysene 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Fluoranthene 28 27 1 1 Fuorne ug/Kg 03/11/05 SW846 3545 8270C-SIM < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Indeno(1,2,3-cd)pyrene < 27 27 1 Naphthalene ug/Kg 03/11/05 SW846 3545 8270C-SIM < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM i Phenanthrene < 27 27 Pyrene 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Nitrobenzene-d5 38 -_ 1 %Recov I2-Fluorobiphenyl 03/11/05 SW846 3545 8270C-SIM 62 1 %Recov 03/11/05 SW846 3545 8270C-SIM Terphenyl-d14 70 1 %Recov 03/11/05 SW846 3545 8270C-SIM PAH/PNA BLANK Prep Date: 03/11/05 IAnalyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method PAH Blank ID 1497-20 1 03/11/05 PESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method 4,4'-DDD < 5.3 5,3 1 ug/kg 03/25/05 SW846 35508 SW846 8081A IAll soil results are reported on a dry weight basis unless otherwise noted. I En Chem Analytical Report Number: 856908 1241 Bellevue Street Green Bay,WI 54302 920-469-2436 I A Division of Pace Analytical Services,Inc. Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: SOIL Collection Date: SOIL 03/04/05 Project Name: OAK PARK HEIGHTS Report Date: 03/29/05 I Project Number: 7735-E Lab Sample Number: 856908-014 Field ID: S-5(2') PESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 I Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method 41 5.3 1 ug/kg 03/25/05 SW846 3550B SW846 8081A 4,4'-DDE 4 03/25/05 SW846 3550B SW846 8081A ' ,4'-DDT 15 5.3 1 ug/kg < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A alpha-BHC < 2.7 2.7 1 ug/kg 1prin 03/25/05 SW846 3550B SW846 8081A < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A beta-BHC 03/25/05 SW846 3550B SW846 8081A Chlordane,Technical < 53 53 1 ug/kg < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A delta-BHC SW846 3550B SW846 8081A 03/25/05 SW Dieldrin < 5.3 5.3 1 ug/kg < 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I Endosulfan I 03/25/05 SW846 3550B SW846 8081A Endosulfan II < 5.3 5.3 1 ug/kg < 5.3 5.3 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan Sulfate Endrin < 5.3 5.3 1 ug/kg 03/25/05 SW846 3550B SW846 8081A III Endrin Aldehyde < 5.3 5.3 1 ug/kg 03/25/05 SW846 3550B SW846 8081A < 2 7 2.7 1 ug/kg P 03/25/05 SW846 3550B SW846 8081A gamma-BHC(Lindane) 03/25/05 SW846 3550B SW846 8081A Heptachlor < 2.7 2.7 1 ug/kg I< 2.7 2.7 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Heptachlor Epoxide Toxaphene < 270 270 1 ug/kg 03/25/05 SW846 3550B SW846 8081A 69 -_ 1 %Recov 03/25/05 SW846 3550B SW846 8081A Te cachlorobiphelene 1 Decachlorobiphenyl 70 — 1 %Recov 03/25/05 SW846 35508 SW846 80 I I I I I 1 I I All soil results are reported on a dry weight basis unless otherwise noted. I En Chem Analytical Report Number: 856908 1241 Bellevue Street IA Division of Pace Analytical Services, Inc. Green Bay,WI 54302 Client: GME CONSULTANTS, INC-MINNEAPOLIS 920-469-2436 Project Name: OAK PARK HEIGHTS Matrix Type: SOIL I Project Number: 7735-E Collection Date: 03/04/05 Field ID: S-6(2') Report Date: 03/29/05 Lab Sample Number: 856908-015 IINORGANICS Test Result EQL Dilution Units Code Ani Date Prep Method Anl Method Arsenic 2.3 0.31 5 Bariu mg/Kg 03/17/05 SW846 3050B SW846 6020 ' Cadmium 45 < 0.10 0.31 0.10 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Chromium 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 15 0.31 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Lead 4.2 0.26 5 Mercury Selenium < mg/Kg 03/17/05 SW846 30508 SW846 6020 0.010 0.010 1 < 1.0 1,0 5 mg/Kg 03/16/05 SW846 7471A SW846 7471A Silver mg/Kg 03/17/05 SW846 3050B SW846 6020 < 0.31 0.31 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 I Percent Solids 95.6 — 1 03/10/05 SM 2540G M SM 2540G M DIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method AnI Method 1 Diesel Range Organics < 4.1 4.1 1 DRO Blank mg/kg 03/11/05 WI MOD DRO WI MOD DRO < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike 90 — 1 %Recov 1 DRO Blank Spike Duplicate 93 1 0 03/11/05 WI MOD DRO WI MOD DRO /oRecov 03/11/05 WI MOD DRO WI MOD DRO PAH/PNA Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Ani Date Prep Method Anl Method 1-Methylnaphthalene < 26 26 1 2-Methylnaphthalene < ug/Kg * 03/11/05 SW846 3545 8270C-SIM 26 26 1 ug/Kg * 03/11/05 SW846 3545 8270C-SIM I Acenaphthene < 26 26 Acenaphthylene Anthracene < 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 26 < 26 26 26 1 1 ug/Kg 03/11/05 5W846 3545 8270C-SIM Benzo(a)anthracene < ug/Kg 03/11/05 SW846 3545 8270C-SIM 26 26 1 ug/Kg * 03/11/05 SW846 3545 8270C-SIM Benzo(a)pyrene < 26 26 Benzo(b)fluoranthene < 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 26 26 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(ghi)perylene < 26 26 Benzo(k)fluoranthene Chrysene < 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 26. < 26 26 26 1 1 ug/Kg ug/Kg 03/11/05 SW846 3545 8270C-SIM Dibenz(a,h)anthracene < g 03/11/05 SW846 3545 8270C-SIM 26 26 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Fluoranthene < 26 26 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM I Fluorene Indeno(1,2,3-cd)pyrene < 26 < 26 26 26 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Naphthalene < 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 26 26 1 ug/Kg * 03/11/05 SW846 3545 8270C-SIM Phenanthrene < 26 26 Pyrene < 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 26 26 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Nitrobenzene-c15 86 -- 1 %Recov 03/11/05 SW846 3545 8270C-SIM 2-Fluorobiphenyl 87 — 1 %Recov 03/11/05 SW846 3545 8270C-SIM Terphenyl-d14 85 1 %Recov 03/11/05 SW846 3545 8270C-SIM PAH/PNA BLANK Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method PAH Blank ID 1497-20 1 03/11/05 PESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method ug/kg 03/25/05 SW846 3550B SW846 8081A All soil results are reported on a dry weight basis unless otherwise noted. I 1241 Bellevue Street En Chem Analytical Report Number: 856908 Green Bay,WI 54302 920-469-2436 A Division of Pace Analytical Services,Inc. 1 Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: SOIL Collection Date: 03/04/05 Project Name: OAK PARK HEIGHTS Report Date: 03/29/05 Project Number: 7735-E Field ID: S-6(2') Lab Sample Number: 856908-015 PESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Ani Date Prep Method Anl Method 4,4'-DDE < 5.2 5.2 1 ug/kg 03/25/05 SW846 3550B SW846 8081A 4,4'-DDT < 5.2 5.2 1 ug/kg 03/25/05 SW846 3550B SW846 8081A 1 Aldrin < 2.6 2.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A alpha-BHC < 2.6 2.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A beta-BHC < 2.6 2.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Chlordane,Technical < 52 52 1 ug/kg 03/25/05 SW846 3550B SW846 8081A delta-BHC < 2.6 2.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Dieldrin < 5.2 5.2 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan I < 2.6 2.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I Endosulfan II < 5.2 5.2 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan Sulfate < 5.2 5.2 1 ug/kg 03/25/05 SW846 3550B SW846 8081A < 5 2 5.2 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endrin Endrin Aldehyde < 5.2 5.2 1 ug/kg 03/25/05 SW846 3550B SW846 8081A gamma-BHC(Lindane) < 2.6 2.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Heptachlor < 2.6 2.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Heptachlor Epoxide < 2.6 2.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A 1 Toxaphene < 260 260 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Tetrachloro-m-xylene 85 — 1 %Recov 03/25/05 SW846 3550B SW846 8081A Decachlorobiphenyl 87 -- 1 %Recov 03/25/05 SW846 3550B SW846 8081A 111 • I I I I 1 I I All soil results are reported on a dry weight basis unless otherwise noted. I I En Chem Analytical Report Number: 856908 1241 Bellevue Street 1 A Division of Pace Analytical Services, Inc. Green Bay,WI 54302 Client: GME CONSULTANTS, INC-MINNEAPOLIS 920-469-2436 Project Name: OAK PARK HEIGHTS Matrix Type: SOIL I Project Number: 7735-E Collection Date: 03/04/05 Field ID: S-7(2') Report Date: 03/29/05 Lab Sample Number: 856908-016 III INORGANICS Test Result EQL Dilution Units Code Anl Date Prep Method AnI Method Arsenic 2.9 0.34 I arium 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Cadmium 51 < 0.11 0.34 0.11 5 5 mg/Kg 03/17/05 5W846 3050B SW846 6020 Chromium mg/Kg 03/17/05 SW846 3050B SW846 6020 19 0.34 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 I Lead 5.2 0.28 Mercury 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 Selenium < 10.019 1 0.011 1.1 1 5 mg/Kg 03/16/05 SW846 7471A SW846 7471A • Silver mg/Kg 03/17/05 SW846 3050B SW846 6020 < 0.34 0.34 5 mg/Kg 03/17/05 SW846 3050B SW846 6020 1 Percent Solids 89.2 — 1 03/10/05 SM 2540G M SM 2540G M DIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 Analyte Result EQL Dilution Units Code Ani Date Prep Method AnI Method I Diesel Range Organics < 4 0 4 0 1 DRO Blank mg/kg 03/11/05 WI MOD DRO WI MOD DRO < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike 90 -- 1 %Recov III DRO Blank Spike Duplicate 93 — 1 03/11/05 WI MOD DRO WI MOD DRO %Recov 03/11/05 WI MOD DRO WI MOD DRO PAH/PNA Prep Date: 03/11/05 Analyte 1-Methylnaphthalene < 28 Result EQL 28 Dilution Units Code Anl Date Prep Method Anl Method 2-Methylnaphthalene < 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM I Acenaphthene < 28 28 Acenaphthylene Anthracene < 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 28 < 28 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(a)anthracene < 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(a)pyrene < 28 28 Benzo(b)fluoranthene < 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(ghi)perylene < 28 28 I Benzo(k)fluoranthene Chrysene < 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 28 < 28 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Dibenz(a,h)anthracene < 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM I Fluoranthene < 28 28 Fluorene 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Indeno(1,2,3-cd)pyrene < 28 < 28 28 28 1 1 ug/Kg ug/Kg 03/11/05 SW846 3545 8270C-SIM Naphthalene < 9 03/11/05 SW846 3545 8270C-SIM 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM I Phenanthrene < 28 28 1 Pyrene < ug/Kg 03/11/05 SW846 3545 8270C-SIM 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Nitrobenzene-d5 86 --- 1 %Recov 2-Fluorobiphenyl 03/11/05 SW846 3545 8270C-SIM 91 N 1 %Recov 03/11/05 SW846 3545 8270C-SIM Terphenyl-d14 94 1 %Recov 03/11/05 SW846 3545 8270C-SIM PAH/PNA BLANK Prep Date: 03/11/05 IAnalyte Result EQL Dilution Units Code Ani Date Prep Method Ant Method PAH Blank ID 1497-20 1 03/11/05 PESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method AnI Method ug/kg 03/25/05 SW846 3550B SW846 8081A All soil results are reported on a dry weight basis unless otherwise noted. 1 I 1241 Bellevue Street En Chem Analytical Report Number: 856908 Green Bay,WI 54302 A Division of Pace Analytical Services,Inc. 920-469-2436 III Matrix Type: SOIL Client: GME CONSULTANTS,INC-MINNEAPOLIS Collection Date: 03/04/05 Project Name: OAK PARK HEIGHTS Report Date: 03/29/05 I Project Number: 7735-E Field ID: S-7(2') Lab Sample Number: 856908-016 PESTICIDES-PRIORITY POLLUTANT LIST Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method < 5.6 5.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A 4,4'-DDE 4,4'-DDT < 5.6 5.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A alpha-BHC < 2.8 2.8 1 ug/kg ldrin 03/25/05 SW846 3550B SW846 8081A beta-BHC < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A 03/25/05 SW846 3550B SW846 8081A I Chlordane,Technical < 56 56 1 ug/kg < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A delta-BHC Dieldrin < 5.6 5.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan I < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I Endosulfan II < 5.6 5.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endosulfan Sulfate < 5.6 5.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Endrin < 5.6 5.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A I Endrin Aldehyde < 5.6 5.6 1 ug/kg 03/25/05 SW846 3550B SW846 8081A gamma-BHC(Lindane) < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Heptachlor < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Heptachlor Epoxide < 2.8 2.8 1 ug/kg 03/25/05 SW846 3550B SW846 8081A Toxaphene < 280 280 1 ug/kg 03/25/05 SW846 3550B SW846 8081A 9 9 92 — 1 %Recov 03/25/05 5W846 3550B SW846 8081A Te cachlorobiphe ene ' I IDecachlorobiphenyl 92 — 1 %Recov 03/25/05 SW846 3550B SW846 808 I I I I I I All soil results are reported on a dry weight basis unless otherwise noted. I I En Chem Analytical Report Number: 856908 1241 Bellevue Street Green Bay,WI 54302 1 A Division of Pace Analytical Services, Inc. 920-469-2436 Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/04/05 I Project Number: 7735-E Report Date: 03/29/05 Field ID: S-8(3') Lab Sample Number: 856908-017 IINORGANICS Test Result EQL Dilution Units Code Anl Date Prep Method AnI Method Percent Solids 90.8 -- 1 % 03/10/05 SM 2540G M SM 2540G M I DIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 Analyte Result EQL Dilution Units Code AnI Date Prep Method Anl Method Diesel Range Organics < 4.2 4.2 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO I DRO Blank < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike 90 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike Duplicate 93 -- 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO 1 PAH/PNA Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method AnI Method 1-Methylnaphthalene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 2-Methylnaphthalene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Acenaphthene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Acenaphthylene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM IAnthracene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(a)anthracene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(a)pyrene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM IBenzo(b)fluoranthene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(ghi)perylene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(k)fluoranthene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Chrysene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 111 Dibenz(a,h)anthracene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Fluoranthene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Fluorene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM IIndeno(1,2,3-cd)pyrene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Naphthalene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Phenanthrene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Pyrene < 28 28 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Nitrobenzene-d5 35 — 1 %Recov 03/11/05 SW846 3545 8270C-SIM 2-Fluorobiphenyl 47 — 1 %Recov 03/11/05 SW846 3545 8270C-SIM Terphenyl-d14 62 -- 1 %Recov 03/11/05 SW846 3545 8270C-SIM IPAH/PNA BLANK Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method PAH Blank ID 1497-20 1 03/11/05 I I I IIAll soil results are reported on a dry weight basis unless otherwise noted. En Chem Analytical Report Number: 856908 1241 Bellevue Street I Green Bay,WI 54302 A Division of Pace Analytical Services, Inc. 920-469-2436 ' Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/04/05 Project Number: 7735-E Report Date: 03/29/05 I Field ID: S-9(3') Lab Sample Number: 856908-018 INORGANICS Test Result EQL Dilution Units Code Ant Date Prep Method Anl Method Percent Solids 92.0 -- 1 % 03/10/05 SM 2540G M SM 2540G M DIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 I Analyte Result EQL Dilution Units Code Ant Date Prep Method Anl Method Diesel Range Organics < 3.9 3.9 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO I DRO Blank Spike 90 -- 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike Duplicate 93 — 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO PAH/PNA Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Ant Date Prep Method Anl Method 1-Methylnaphthalene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 2-Methylnaphthalene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Acenaphthene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Acenaphthylene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Anthracene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(a)anthracene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(a)pyrene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(b)fluoranthene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(ghi)perylene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(k)fluoranthene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Chrysene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Dibenz(a,h)anthracene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Fluoranthene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Fluorene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Indeno(1,2,3-cd)pyrene < 27 27 . 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM I Naphthalene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Phenanthrene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Pyrene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Nitrobenzene-d5 79 -- 1 %Recov 03/11/05 SW846 3545 8270C-SIM 2-Fluorobiphenyl 88 — 1 %Recov 03/11/05 SW846 3545 8270C-SIM Terphenyl-d14 95 — 1 %Recov 03/11/05 SW846 3545 8270C-SIM PAH/PNA BLANK Prep Date: 03/11/05 1 Analyte Result EQL Dilution Units Code Anl Date Prep Method Ant Method PAH Blank ID 1497-20 1 03/11/05 I I I All soil results are reported on a dry weight basis unless otherwise noted. En Chem Analytical Report Number: 856908 1241 Bellevue Street y P Green Bay,WI 54302 A Division of Pace Analytical Services, Inc. 920-469-2436 Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/04/05 I Project Number: 7735-E Report Date: 03/29/05 Field ID: S-10(3') Lab Sample Number: 856908-019 I INORGANICS Test Result EQL Dilution Units Code Anl Date Prep Method Anl Method Percent Solids 91.5 -- 1 % 03/10/05 SM 2540G M SM 2540G M IDIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method I Diesel Range Organics < 4.3 4.3 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike 90 -- 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike Duplicate 93 -- 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO IPAH/PNA Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code An1 Date Prep Method Anl Method 1-Methylnaphthalene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM I2-Methylnaphthalene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Acenaphthene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Acenaphthylene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM IAnthracene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(a)anthracene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(a)pyrene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(b)fluoranthene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(ghi)perylene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(k)fluoranthene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Chrysene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Dibenz(a,h)anthracene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Fluoranthene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Fluorene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM IIndeno(1,2,3-cd)pyrene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Naphthalene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Phenanthrene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM 1 Pyrene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Nitrobenzene-d5 79 1 %Recov 03/11/05 SW846 3545 8270C-SIM 2-Fluorobiphenyl 88 -- 1 %Recov 03/11/05 SW846 3545 8270C-SIM Terphenyl-d14 91 -- 1 %Recov 03/11/05 SW846 3545 8270C-SIM IPAH/PNA BLANK Prep Date: 03/11/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method PAH Blank ID 1497-20 1 03/11/05 I I I IAll soil results are reported on a dry weight basis unless otherwise noted. I En Chem Analytical Report Number: 856908 1241 Bellevue Street Green Bay,WI 54302 A Division of Pace Analytical Services, Inc. 920-469-2436 1 Client: GME CONSULTANTS,INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/04/05 Project Number: 7735-E Report Date: 03/29/05 I Field ID: S-11 (3') Lab Sample Number: 856908-020 INORGANICS 111 Test Result EQL Dilution Units Code AnI Date Prep Method AnI Method Percent Solids 92.0 -- 1 % 03/10/05 SM 2540G M SM 2540G M DIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 I Analyte Result EQL Dilution Units Code AnI Date Prep Method AnI Method Diesel Range Organics < 4.1 4.1 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO I DRO Blank Spike 90 -- 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike Duplicate 93 — 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO PAH/PNA Prep Date: 03/11/05 1 Analyte Result EQL Dilution Units Code An!Date Prep Method Anl Method 1-Methylnaphthalene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Il2-Methylnaphthalene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Acenaphthene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Acenaphthylene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Anthracene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM I Benzo(a)anthracene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(a)pyrene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(b)fluoranthene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(ghi)perylene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Benzo(k)fluoranthene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Chrysene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Dibenz(a,h)anthracene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Fluoranthene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Fluorene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Indeno(1,2,3-cd)pyrene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Naphthalene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Phenanthrene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Pyrene < 27 27 1 ug/Kg 03/11/05 SW846 3545 8270C-SIM Nitrobenzene-d5 77 — 1 %Recov 03/11/05 SW846 3545 8270C-SIM 2-Fluorobiphenyl 85 — 1 %Recov 03/11/05 SW846 3545 8270C-SIM Terphenyl-d14 90 --- 1 %Recov 03/11/05 SW846 3545 8270C-SIM PAH/PNA BLANK Prep Date: 03/11/05 1 Analyte Result EQL Dilution Units Code AnI Date Prep Method AnI Method PAH Blank ID 1497-20 1 03/11/05 I 1 I All soil results are reported on a dry weight basis unless otherwise noted. I I En Chem Analytical Report Number: 856908 1241 Bellevue Street A Division of Pace Analytical Services, Inc. Green Bay,WI 54302 Client: GME CONSULTANTS, INC-MINNEAPOLIS 920-469-2436 Project Name: OAK PARK HEIGHTS Matrix Type: SOIL Collection Date: 03/08/05 I Project Number: 7735-E Field ID: DW B-10(3') Report Date: 04/21/05 Lab Sample Number: 856908-021 IINORGANICS Test Result E L Q Dilution Units Code Anl Date Prep Method An!Method Percent Solids 82.3 1 % 03/10/05 SM 2540G M I DIESEL RANGE ORGANICS SM 2540G M Prep Date: 03/10/05 Preservation Date: 03/10/05 Analyte Result E aL Dilution Units Code Anl Date Prep Method Ani Method Diesel Range Organics < 4.7 4'7 1 mg/kg 03/11/05 WI MOD DRO < 5.0 5,0 1 WI MOD DRO I DRO Blank DRO Blank Spike 81 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike Duplicate 1 %Recov 03/11/05 WI MOD DRO 94 - 1 %Recov WI MOD DRO 1 03/11/05 WI MOD DRO WI MOD DRO BTEX+MTBE Prep Date: 03/09/05 Analyte Result E L Q Dilution Units Code Anl Date Prep Method Anl Method I Benzene < 30 en 30 50 ug/kg 03/09/05 5035/50306 < 30 30 50 ug/kg WI MOD GRO Methyl Ethylb-tert-butyl-ether zene < 30 03/09/05 5035/5030B WI MOD GRO Toluene 30 50 ug/kg 03/09/05 5035/5030B WI MOD GRO I < 30 30 Xylene,o < 30 50 ug/kg 03/09/05 5035/50306 WI MOD GRO Xylene,, m+p 30 50 ug/kg 03/09/05 5035/50308 < 30 30 50 ug/kg WI MOD GRO ,a,a-Trifluorotoluene 102 03/09/05 5035/5030B WI MOD GRO a II 1 %Recov 03/09/05 5035/50306 WI MOD GRO BTEX BLANK Prep Date: 03/09/05 Analyte Result E L Q Dilution Units Code Anl Date Prep Method An!Method BT Blank ID 1607-8 1 GASEX OLINE RANGE ORGANICS Prep Date: 03/09/05 Analyte Result E L Q Dilution Units Code Anl Date Prep Method Anl Method I Gasoline Range Organics < 3.0 GRO Blank 3.0 50 mg/kg 03/09/05 WI MOD GRO WI MOD GRO < 2.5 2.5 50 mg/kg 03/09/05 WI MOD GRO WI MOD GRO GRO Blank Spike 117 1 %Recov 03/09/05 WI MOD GRO WI MOD GRO GRO Blank Spike Duplicate 114 --- 1 %Recov I 03/09/05 WI MOD GRO WI MOD GRO I I I I I IAll soil results are reported on a dry weight basis unless otherwise noted. I 1241 Bellevue Street En Chem Analytical Report Number: 856908 Green 0-469-24 6I 54302 1 A Division of Pace Analytical Services, Inc. Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: SOIL Collection Date: SOIL Project Name: OAK PARK HEIGHTS OW B- Report Date: 04/21/05 I 03/08/05 Project Number: Lab Sample Number: 856908-022 Field ID: B-11 (3') INORGANICS ' Result EQL Dilution Units Code Anl Date Prep Method Ant Method Percent Solids 90.2 — 1 %est 03/10/05 SM 2540G M SM 2540G M P DIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 1 Analyte Result EQL Dilution Units Code Ant Date Prep Method Anl Method 4 3 4.3 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO Diesel Range Organics < 03/11/05 WI MOD DRO WI MOD DRO I DRO Blank < 5.0 5.0 1 mg/kg DRO Blank Spike 81 — 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO 94 --- 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike Duplicate BTEX+MTBE Prep Date: 03/09/05 Result EQL Dilution Units Code Anl Date Prep Method An!Method Analyte ' < 28 28 50 ug/kg 03/09/05 5035/5030B WI MOD GR Benzene Ethylbenzene < 28 28 50 ug/kg 03/09/05 5035/5030B WI MOD GRO < 28 28 50 ug/kg 03/09/05 5035/5030B WI MOD GRO Toluene < 28 28 50 ug/kg T 03/09/05 5035/5030B WI MOD GRO Xylene,0 < 28 28 50 ug/kg 03/09/05 5035/5030B WI MOD GRO ,03/09/05 5035/5030B WI MOD GRO Xylenes,m+p < 28 28 50 ug/kg a,a,a-Trifluorotoluene 102 -- 1 %Recov 03/09/05 5035/5030B WI MOD GRO BTEX BLANK Prep Date: 03/09/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method BTEX Blank ID 1607-8 1 GASOLINE RANGE ORGANICS Prep Date: 03/09/05 1llI Analyte Result EQL Dilution Units Code Ant Date Prep Method Ant Method < 2 8 2.8 50 mg/kg 03/09/05 WI MOD GRO WI MOD GRO I GRRO O B Bl G Range Organics 50 mg/kg 03/09/05 WI MOD GRO WI MOD GRO lank < 2.5 2.5 GRO Blank Spike 117 -- 1 %Recov 03/09/05 WI MOD GRO WI MOD GRO 03/09/05 WI MOD GRO WI MOD GRO I GRO Blank Spike Duplicate 114 --- 1 %Recov I I I I 1 All soil results are reported on a dry weight basis unless otherwise noted. I En Chem Analytical Report Number: 856908 • 1241 Bellevue Street 1 Green Bay,WI 54302 A Division of Pace Analytical Services, Inc. 920-469-2436 Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: SOIL I Project Name: OAK PARK HEIGHTS Collection Date: 03/08/05 Project Number: 7735-E Report Date: 03/29/05 Field ID: DW S-12(1') Lab Sample Number: 856908-023 1 INORGANICS Test Result EQL Dilution Units Code Anl Date Prep Method Anl Method Percent Solids 88.0 -- 1 % 03/10/05 SM 2540G M SM 2540G M 1 DIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method Diesel Range Organics < 4.3 4.3 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike 81 -- 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike Duplicate 94 -- 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO IBTEX+MTBE Prep Date: 03/09/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Ant Method IBenzene < 28 28 50 ug/kg 03/09/05 5035/5030B WI MOD GRO Ethylbenzene < 28 28 50 ug/kg 03/09/05 5035/5030B WI MOD GRO Methyl-tert-butyl-ether < 28 28 50 ug/kg 03/09/05 5035/50308 WI MOD GRO IToluene < 28 28 50 ug/kg 03/09/05 5035/5030B WI MOD GRO Xylene,o < 28 28 50 ug/kg 03/09/05 5035/5030B WI MOD GRO Xylenes,m+p < 28 28 50 ug/kg 03/09/05 5035/5030B WI MOD GRO a,a,a-Trifluorotoluene 102 -- 1 %Recov 03/09/05 5035/5030B WI MOD GRO IBTEX BLANK Prep Date: 03/09/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Ant Method IBTEX Blank ID 1607-8 1 GASOLINE RANGE ORGANICS Prep Date: 03/09/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method IGasoline Range Organics < 2.8 2.8 50 mg/kg 03/09/05 WI MOD GRO WI MOD GRO GRO Blank < 2.5 2.5 50 mg/kg 03/09/05 WI MOD GRO WI MOD GRO GRO Blank Spike 117 — 1 %Recov 03/09/05 WI MOD GRO WI MOD GRO 1 GRO Blank Spike Duplicate 114 — 1 %Recov 03/09/05 WI MOD GRO WI MOD GRO I I I I I All soil results are reported on a dry weight basis unless otherwise noted. I En Chem Analytical Report Number: 856908 1241 Bellevue Street Green Bay,WI 54302 A Division of Pace Analytical Services, Inc. 920469-2436 Client: GME CONSULTANTS,INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/08/05 Project Number: 7735-E Report Date: 03/29/05 Field ID: DW S-13(1') Lab Sample Number: 856908-024 INORGANICS Test Result EQL Dilution Units Code AnI Date Prep Method AnI Method Percent Solids 88.8 -- 1 % 03/10/05 SM 2540G M SM 2540G M DIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method Diesel Range Organics < 4.4 4.4 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike 81 — 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike Duplicate 94 -- 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO BTEX+MTBE Prep Date: 03/09/05 1 Analyte Result EQL Dilution Units Code AnI Date Prep Method AnI Method Benzene < 28 28 50 ug/kg 03/09/05 5035/5030B WI MOD GRO I Ethylbenzene < 28 28 50 ug/kg 03/09/05 5035/5030B WI MOD GRO Methyl-tert-butyl-ether < 28 28 50 ug/kg 03/09/05 5035/5030B WI MOD GRO Toluene < 28 28 50 ug/kg 03/09/05 5035/5030B WI MOD GRO Xylene,o < 28 28 50 ug/kg 03/09/05 5035/5030B WI MOD GRO Xylenes,m+p < 28 28 50 ug/kg 03/09/05 5035/5030B WI MOD GRO a,a,a-Trifluorotoluene 102 --- 1 %Recov 03/09/05 5035/5030B WI MOD GRO BTEX BLANK Prep Date: 03/09/05 1 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method BTEX Blank ID 1607-8 1 GASOLINE RANGE ORGANICS Prep Date: 03/09/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method Gasoline Range Organics < 2.8 2.8 50 mg/kg 03/09/05 WI MOD GRO WI MOD GRO I GRO Blank < 2.5 2.5 50 mg/kg 03/09/05 WI MOD GRO WI MOD GRO GRO Blank Spike 117 — 1 %Recov 03/09/05 WI MOD GRO WI MOD GRO GRO Blank Spike Duplicate 114 — 1 %Recov 03/09/05 WI MOD GRO WI MOD GRO I I 1 I 1 All soil results are reported on a dry weight basis unless otherwise noted. I I 1241 Bellevue Street En Chem Analytical Report Number: 856908 Green Bay,WI 54302 IIIA Division of Pace Analytical Services, Inc. 920-469-2436 Client: GME CONSULTANTS,INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/08/05 t Project Number: 7735-E Report Date: 03/29/05 Field ID: DW S-14(1') Lab Sample Number: 856908-025 INORGANICS Test Result EQL Dilution Units Code Anl Date Prep Method Ani Method Percent Solids •84.2 -- 1 % 03/10/05 SM 2540G M SM 2540G M IDIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method Diesel Range Organics < 4.3 4.3 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO IDRO Blank < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike 81 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike Duplicate 94 — 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO IBTEX+MTBE Prep Date: 03/09/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method IBenzene < 30 30 50 ug/kg 03/09/05 5035/5030B WI MOD GRO Ethylbenzene < 30 30 50 ug/kg 03/09/05 5035/5030B WI MOD GRO Methyl-tert-butyl-ether < 30 30 50 ug/kg 03/09/05 5035/5030B WI MOD GRO Toluene < 30 30 50 ug/kg 03/09/05 5035/5030B WI MOD GRO ' Xylene,o < 30 30 50 ug/kg 03/09/05 5035/5030B WI MOD GRO Xylenes, m+p < 30 30 50 ug/kg 03/09/05 5035/5030B WI MOD GRO a,a,a-Trifluorotoluene 102 -- 1 %Recov 03/09/05 5035/5030B WI MOD GRO IBTEX BLANK Prep Date: 03/09/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method BTEX Blank ID 1607-8 1 IGASOLINE RANGE ORGANICS Prep Date: 03/09/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method IGasoline Range Organics < 3.0 3.0 50 mg/kg 03/09/05 WI MOD GRO WI MOD GRO GRO Blank < 2.5 2.5 50 mg/kg 03/09/05 WI MOD GRO WI MOD GRO GRO Blank Spike 117 -- 1 %Recov 03/09/05 WI MOD GRO WI MOD GRO GRO Blank Spike Duplicate 114 --- 1 %Recov 03/09/05 WI MOD GRO WI MOD GRO I I I I I All soil results are reported on a dry weight basis unless otherwise noted. • I En Chem Analytical Report Number: 856908 1241 Bellevue Street Green Bay,WI 54302 A Division of Pace Analytical Services, Inc. 920-469-2436 Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/08/05 Project Number: 7735-E Report Date: 03/29/05 Field ID: DW S-15(1') Lab Sample Number: 856908-026 INORGANICS Test Result EQL Dilution Units Code Anl Date Prep Method AnI Method Percent Solids 92.0 — 1 % 03/10/05 SM 2540G M SM 2540G M DIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method AnI Method Diesel Range Organics < 4.0 4.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO I DRO Blank Spike 81 — 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike Duplicate 94 — 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO BTEX+MTBE Prep Date: 03/09/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method AnI Method Benzene < 27 27 50 ug/kg 03/09/05 5035/5030B WI MOD GRO Ethylbenzene < 27 27 50 ug/kg 03/09/05 5035/5030B WI MOD GRO Methyl-tert-butyl-ether < 27 27 50 ug/kg 03/09/05 5035/5030B WI MOD GRO Toluene < 27 27 50 ug/kg 03/09/05 5035/5030B WI MOD GRO Xylene,o < 27 27 50 ug/kg 03/09/05 5035/5030B WI MOD GRO I Xylenes,m+p < 27 27 50 ug/kg 03/09/05 5035/5030B WI MOD GRO a,a,a-Trifluorotoluene 102 -- 1 %Recov 03/09/05 5035/5030B WI MOD GRO BTEX BLANK Prep Date: 03/09/05 Analyte Result EQL Dilution Units Code Anl Date Prep Method Anl Method BTEX Blank ID 1607-8 1 GASOLINE RANGE ORGANICS Prep Date: 03/09/05 1 Analyte Result EQL Dilution Units Code Ant Date Prep Method Atli Method Gasoline Range Organics < 2.7 2.7 50 mg/kg 03/09/05 WI MOD GRO WI MOD GRO I GRO Blank < 2.5 2.5 50 mg/kg 03/09/05 WI MOD GRO WI MOD GRO GRO Blank Spike 117 — 1 %Recov 03/09/05 WI MOD GRO WI MOD GRO GRO Blank Spike Duplicate 114 — 1 %Recov 03/09/05 WI MOD GRO WI MOD GRO I I I I I I All soil results are reported on a dry weight basis unless otherwise noted. 1 I En Chem Analytical Report Number: 856908 1241 Bellevue Street Green Bay,WI 54302 A Division of Pace Analytical Services, Inc. 920-469-2436 Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: SOIL Project Name: OAK PARK HEIGHTS Collection Date: 03/08/05 I Project Number: 7735-E Report Date: 03/29/05 Field ID: TP-10(3') Lab Sample Number: 856908-027 1 INORGANICS Test Result EQL Dilution Units Code AnI Date Prep Method Anl Method Percent Solids 85.7 -- 1 % 03/10/05 SM 2540G M SM 2540G M IDIESEL RANGE ORGANICS Prep Date: 03/10/05 Preservation Date: 03/10/05 Analyte Result EQL Dilution Units Code AnI Date Prep Method AnI Method Diesel Range Organics < 4.3 4.3 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO IDRO Blank < 5.0 5.0 1 mg/kg 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike 81 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO DRO Blank Spike Duplicate 94 — 1 %Recov 03/11/05 WI MOD DRO WI MOD DRO I I I I I I I I I I I I All soil results are reported on a dry weight basis unless otherwise noted. 1241 Bellevue Street En Chem Analytical Report Number: 856908 Green Bay,WI 54302 A Division of Pace Analytical Services, Inc. 920-469-2436 Client: GME CONSULTANTS, INC-MINNEAPOLIS Matrix Type: METHANOL Project Name: OAK PARK HEIGHTS Collection Date: 03/08/05 Project Number: 7735-E Report Date: 03/29/05 Field ID: MEOH BLANK Lab Sample Number: 856908-028 BTEX+MTBE Prep Date: 03/09/05 Analyte Result EQL Dilution Units Code Ant Date Prep Method Ant Method Benzene < 25 25 50 ug/L 03/09/05 SW846 5030B WI MOD GRO Ethylbenzene < 25 25 50 ug/L 03/09/05 SW846 5030B WI MOD GRO Methyl-tert-butyl-ether < 25 25 50 ug/L 03/09/05 SW846 5030B WI MOD GRO Toluene < 25 25 50 ug/L 03/09/05 SW846 5030B WI MOD GRO Xylene,o < 25 25 50 ug/L 03/09/05 SW846 5030B WI MOD GRO Xylenes,m+p < 25 25 50 ug/L 03/09/05 SW846 5030B WI MOD GRO I a,a,a-Trifluorotoluene 102 -- 1 %Recov 03/09/05 SW846 5030B WI MOD GRO BTEX BLANK Prep Date: 03/09/05 Analyte Result EQL Dilution Units Code Ant Date Prep Method AnI Method BTEX Blank ID 1607-8 1 GASOLINE RANGE ORGANICS Prep Date: 03/09/05 Analyte Result EQL Dilution Units Code Ant Date Prep Method Ant Method Gasoline Range Organics < 2500 2500 50 ug/L 03/09/05 WI MOD GRO WI MOD GRO GRO Blank < 50 50 1 ug/L 03/09/05 WI MOD GRO WI MOD GRO I GRO Blank Spike 117 — 1 %Recov 03/09/05 WI MOD GRO WI MOD GRO GRO Blank Spike Duplicate 114 — 1 %Recov 03/09/05 WI MOD GRO WI MOD GRO I I I I I I I I I I I En Chem 1241 Bellevue Street Green Bay,WI 54302 I A Division of Pace Analytical Services, Inc. 920-469-2436 Fax:920-469-8827 Lab Number TestGrouplD Field ID Comment 1 856908-002 PAH+-S B-2(4') B-Naphthalene present in Extraction Blank at 3.5ug/Kg. 856908-006 PAH+-S B-6(3') B-Naphthalene present in Extraction Blank at 3.5ug/Kg. II856908-009 PAH+-S B-9(7') B-Naphthalene present in Extraction Blank at 3.5ug/Kg. 856908-022 BT&MT-S-ME DW S-11 (3') Sample was received in a bottle with a cracked lid. Sample jar was replaced with a new lid. I856908-022 GRO-S-ME DW S-11 (3') Sample was received in a bottle with a cracked lid. Sample jar was replaced with a new lid. 856908-023 BT&MT-S-ME DW S-12(1') Sample was received in a bottle with a cracked lid. Sample jar was replaced with a new lid. III856908-023 GRO-S-ME DW S-12(1') Sample was received in a bottle with a cracked lid. Sample jar was replaced with a new lid. 1 I I I I I I 1 I I I I I Qualifier Codes I Flag Applies To Explanation A Inorganic Analyte is detected in the method blank. Method blank criteria is evaluated to the laboratory method detection limit. Additionally, method blank acceptance may be based on project specific criteria or determined from analyte concentrations in the sample and are evaluated on a sample by sample basis. B Inorganic The analyte has been detected between the method detection limit and the reporting limit. B Organic Analyte is present in the method blank. Method blank criteria is evaluated to the laboratory method detection limit. Additionally, method blank acceptance may be based on project specific criteria or determined from analyte concentrations in the sample and are evaluated on a sample by sample basis. C All Elevated detection limit. I D D All Analyte value from diluted analysis or surrogate result not applicable due to sample dilution. E Inorganic Estimated concentration due to matrix interferences. During the metals analysis the serial dilution failed to meet the established control limits of 0-10%.The sample concentration is greater than 50 times the IDL for analysis done on the ICP or 100 times the IDL for analysis done on the ICP-MS. The result was flagged with the E qualifier to indicate that a physical interference was observed. E Organic Analyte concentration exceeds calibration range. F Inorganic Due to potential interferences for this analysis by Inductively Coupled Plasma techniques(SW-846 Method 6010),this analyte has been confirmed by and reported from an alternate method. F Organic Surrogate results outside control criteria. G All The result is estimated because the concentration is less than the lowest calibration standard concentration utilized in the initial calibration.The method detection limit is less than the reporting limit specified for this project. H All Preservation,extraction or analysis performed past holding time. HF Inorganic This test is considered a field parameter,and the recommended holding time is 15 minutes from collection. The analysis was - performed in the laboratory beyond the recommended holding time. IIJ All Concentration detected equal to or greater than the method detection limit but less than the reporting limit. K Inorganic Sample received unpreserved. Sample was either preserved at the time of receipt or at the time of sample preparation. K Organic Detection limit may be elevated due to the presence of an unrequested analyte. III L All Elevated detection limit due to low sample volume. M Organic Sample pH was greater than 2 N All Spiked sample recovery not within control limits. O Organic Sample received overweight. P Organic The relative percent difference between the two columns for detected concentrations was greater than 40%. Q All The analyte has been detected between the limit of detection(LOD)and limit of quantitation(LOQ). The results are qualified due to the uncertainty of analyte concentrations within this range. S Organic The relative percent difference between quantitation and confirmation columns exceeds internal quality control criteria. Because the result is unconfirmed,it has been reported as a non-detect with an elevated detection limit. U All The analyte was not detected at or above the reporting limit. V All Sample received with headspace. W All A second aliquot of sample was analyzed from a container with headspace. X All See Sample Narrative. I & All Laboratory Control Spike recovery not within control limits. • All Precision not within control limits. < All The analyte was not detected at or above the reporting limit. 1 Inorganic Dissolved analyte or filtered analyte greater than total analyte;analyses passed QC based on precision criteria. 2 Inorganic Dissolved analyte or filtered analyte greater than total analyte;analyses failed QC based on precision criteria. 3 Inorganic BOD result is estimated due to the BOD blank exceeding the allowable oxygen depletion. 4 Inorganic BOD duplicate precision not within control limits. Due to the 48 hour holding time for this test,it is not practical to reanalyze and try to correct the deficiency. 5 Inorganic BOD result is estimated due to insufficient oxygen depletion. Due to the 48 hour holding time for this test,it is not practical to reanalyze and try to correct the deficiency. 6 Inorganic BOD laboratory control sample not within control limits. Due to the 48 hour holding time for this test,it is not practical to reanalyze and try to correct the deficiency. 7 Inorganic BOD result is estimated due to complete oxygen depletion. Due to the 48 hour holding time for this test, it is not practical to reanalyze and try to correct the deficiency. I I I En Chem Analysis Summary by Laboratory 1241 Bellevue Street A Division of Pace Analytical Services, Inc. Green Bay,WI 54302 1090 Kennedy Avenue I Kimberly,WI 54136 co CO 03 rn rn 03 CO CO con CO CO con (1 con CM C31(31 CT CM CO O CO CO 03 CO CO (31 CO m0 0 CO 0) CA 0) 0) 0) 0) 0) 01 0) 0) COO CO C0)01 01 01 CO 0) 0 0) rn CO CO CO CO 0 0 0 0 D00 0 800 0 0 `O 0 0 c00 0) 0 0 01 0 ao m 0 T 935° 9' 5° 939' T 0 (0 0 03 0 CO c0 Test Group Name x 0 0 0 0 0 0 0 00 00 00 0 0 0 0 00 0 ° ° ° x 0 0 0 0 o Cb N W 0 (31 0) O O o O O O O V CO O (O 0 -+ N W A Cr 0) V CO CO O N3 N W A 01 T III ARSENIC G G G G G G G G G G G G G G G BARIUM G G G G G G G G G G G G G G G i BTEX+MTBE BTEX BLANK G G G G G G 1 CADMIUM G G G G G G G G G G G G G G G G G G G G G CHROMIUM G G G G G G G G G G G G G G G DIESEL RANGE ORGANICS G G G G G G G G G G G G G G G G G G G G G G G G G G IGASOLINE RANGE ORGANICS LEAD G G G G G G G G G G G G G G G G G G G G G MERCURY G G G G G G G G G G G G G G G PAH/PNA G G G G G G G G G G G G G G G G G G G G PAH/PNA BLANK G G G G G G G G G G G G G G G G G G G G PERCENT SOLIDS G G G G G G G G G G G G G G G G G G G G G G G G G G PESTICIDES-PRIORITY POLLUTANT K K K K K K K K K K K K K K K SELENIUM G G G G G G G G G G G G G G G SILVER G G G G G G G G G G G G G G G I o 0 01 C.T1 0) CD 0 0 OD 03 Test Group Name N N V CO BTEX+MTBE G BTEX BLANK G iDIESEL RANGE ORGANICS G GASOLINE RANGE ORGANICS G PERCENT SOLIDS G I Minnesota Certification 1 G=En Chem Green Bay 055-999-334 K=En Chem Kimberly 055-999-107 S=En Chem Superior Not Applicable C=Subcontracted Analysis I=Other Pace Lab Analysis I I I Y (x10^4) O O N Is N N N W W W W . -N 4. 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M -, 0 Is 0 I-. •• 0 -4 0.. 0 • • 1=1 al Is I Is• V- !I Is 03- i Q .' 10 0T I Al: I-.- rf:S...-..:. I -13 U NC AO 0 (.4 10 I I , FORM 1 CLIENT SAMPLE NO. , VOLATILE ORGANICS ANALYSIS DATA SHEET BLKL 1607-8 il Lab Name: ENCHEM, A DIVISION OF PAC Contract: Lab Code: ENCHEMGB Case No. : SAS No. : SDG No. : GRO7-030905A' Matrix: (soil/water) SOIL Lab Sample ID: BLKL 1607-8 Sample wt/vol: 10 .0 (g/mL) G Lab File ID: 003F0101 I Level : (low/med) MED Date Received: % Moisture: not dec. Date Analyzed: 03/09/05 ' GC Column: DB-624 ID: 0.53 (mm) Dilution Factor: 50 .0 Soil Extract Volume: 10 (mL) Soil Aliquot Volume: 1000 (uL) ' CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG 4 I 1634-04-4 Methyl test-butyl ether! 25.00 U 71-43-2 Benzene 25.00 U II 108-88-3 Toluene 25.00 U 100-41-4 Ethylbenzene 25.00 U 108-38-3 m/p-Xylene 50.00 U . 1' - 95-47-6 o-Xylene 25.00 U 108-67-8 1,3, 5-Trimethylbenzene 25.00 U 95-63-6 1,2,4-Trimethylbenzene 25.00 U . el 91-20-3 Naphthalene 14.67 J Total Xylenes 75.00 U II 1 r I I II 11 FORM I VOA II 1 1 1497-19 I PAH Sand Blank IAnal by: aro Anal date-03/10/2005 Blank#1497-19 I REPORTED LOD LOQ RESULT UNITS QUALIFIER INIT RES WEIGHT CALC RES I Acenaphthene 1.59 25 ND ug/kg 0 0.02 0 Acenaphthylene 5.58 25 ND ug/kg 0 0.02 0 Anthracene 2.15 25 ND ug/kg 0 0.02 0 IBenzo(a)anthracene 12.44 25 ND ug/kg 0 0.02 0 Benzo(a)pyrene 10.08 25 ND ug/kg 0 0.02 0 I Benzo(b)fluoranthene 8.20 25 ND ug/kg 0 0.02 0 Benzo(g,h,i)perylene 5.56 25 ND ug/kg 0 0.02 0 Benzo(k)fluoranthene 11.02 25 ND ug/kg 0 0.02 0 Chrysene 11.44 25 ND ug/kg 0 0.02 0 I Dibenzo(a,h)anthracene 3.32 25 ND ug/kg 0 0.02 0 Fluoranthene 9.50 25 ND ug/kg 0 0.02 0 Fluorene 1.33 25 ND ug/kg 0 0.02 0 I Indeno(1,2,3-c,d)pyrene 5.30 25 ND ug/kg 0 0.02 0 1-Methylnaphthalene 2.29 25 ND ug/kg 0 0.02 0 I 2-Methylnaphthalene 3.24 25 ND ug/kg 0 0.02 0 Naphthalene 2.45 25 3.50 ug/kg 3.5 0.02 0 Phenanthrene 5.64 25 ND ug/kg 0 0.02 0 Pyrene 12.44 25 ND ug/kg 0 0.02 0 1 Nitobenzene-c15 zene d5 107.1 % recov 1 107.1 I 2-Fluorobiphenyl 104.1 % recov 1 104.1 Terphenyl-d14 116.2 % recov 1 116.2 I I I I I I 1 1497-20 I PAH Sand Blank Anal by: aro Anal date-03/11/2005 Blank#1497-20 REPORTED LOD LOQ RESULT UNITS QUALIFIER INIT RES WEIGHT CALC RES Acenaphthene 1.59 25 ND ug/kg 0 0.02 0 Acenaphthylene 5.58 25 ND ug/kg 0 0.02 0 Anthracene 2.15 25 ND ug/kg 0 0.02 0 Benzo(a)anthracene 12.44 25 ND ug/kg 0 0.02 0 0.02 0 Benzo(a)pyrene 10.08 25 ND ug/k 0 g 0 0.02 0 Benzo(b)fluoranthene 8.20 25 ND ug/kg 0 0.02 0 I Benzo(g,h,i)perylene 5.56 25 ND u g/kg 0 0.02 0 Benzo(k)fluoranthene 11.02 25 ND u9/ kg 0 0.02 0 Chrysene 11.44 25 ND ug/kg Dibenzo(a,h)anthracene 3.32 25 ND ug/kg 0 0.02 0 Fluoranthene 9.50 25 ND ug/kg 0 0.02 0 Fluorene 1.33 25 ND ug/kg 0 0.02 0 Indeno(1,2,3-c,d)pyrene 5.30 25 ND ug/kg 0 0.02 0 1-Methylnaphthalene 2.29 25 ND ug/kg 0 0.02 0 2-Methylnaphthalene 3.24 25 ND ug/kg 0 0.02 0 Naphthalene 2.45 25 ND ug/kg 0 0.02 0 Phenanthrene 5.64 25 ND ug/kg 0 0.02 0 Pyrene 12.44 25 ND ug/kg 0 0.02 0 I Nitobenzene-d5 94.3 % recov 1 94.33 2-Fluorobiphenyl 96.3 % recov 1 96.34 Terphenyl-d14 104.9 % recov 1 104.87 I I I I I I I I I Effective Date:July 14,2002 Surrogates IRevised: 8/17/2004 En Chem-Green Bay IAqueous Low Level Solids Methanol Solids GC VOA ( LCL UCL LCL UCL LCL UCL a,a,a-Trifluorotoluene I 80 { 124 I 65 I 139 I 80 I 119 I Aqueous Low Level Solids Methanol Solids I GCMS VOA UCL LCL UCL Dibromofluoromethane 69 LCL 140 UCL 59 LCL 105 62 123 72 137 63 118 73 123 Toluene-de 4-Bromoflurobenzene 65 133 44 107 66 119 I Aqueous Solids GCMS PAH LCL UCL LCL UCL Nitrobenzene-d5 10 136 20 119 I 2-Fluorobiphenyl 14 111 30 97 Terphenyl-d14 46 137 41 119 IAqueous Solids GCMS BNA LCL UCL LCL UCL 2-Fluorophenol 13 70 35 113 Phenol-ds 8 44 29 114 2-Chlorophenol-d4 29 104 34 107 1,2-Dichlorobenzene-d4 34 112 27 116 INitrobenezene-ds 34 126 32 118 2-Fluorobiphenyl 36 126 26 126 2,4,6-Tribromophenol 39 133 17 129 ITerphenyl-d14 56 139 23 141 I Aqueous Solids GC PCB L UCL IDecachlorobiphenyl I 22 LCL I 133 UCL I 11 CL I 142 Aqueous Solids If TPH Diesel Terphenyl J LCL 33 I UCL 133 LCL 34 UCL 106 o- I IAqueous Solids ITPH Gas I LCL UCL 124 L69 CL UCL a,a,a-Trifluorotoluene I I I 146 I IP:IEVERYONE\FORMSIQUALITYCONTROL\Surrogate Summary KIM-GB I .�^/ En Chem, Inc. Cooler Receipt Log I Batch No. (6,1-70 1 O ?�. Q 0 Project Name or ID di� ` / 1 / _ _'. 0 • No.of Coolers: / Temps: C r/G� On_ A.Receipt Phase: Date cooler was opened: eio/or`� By: 62P ' 1: Were samples received on ice?(Must be 5 6 C) 40 NO2 NA 2. Was there a Temperature Blank? NO 3: Were custody seals present and intact on cooler? (Record on COC) YES 4: Are COC documents present?.. 1/344 NO2 I 5: Does this Project require quick turn around analysis? YES 6) 6: Is there any sub-work? YES CO 7: Are there any short hold time tests? YES sCS 1 8: Are any samples nearing expiration of hold-time?(Within 2 days) YES1 r0 Contacted by/Who 9: Do any samples need to be Filtered or Preserved in the lab?lab? YES1 Contacted by/Who I B.Check-in Phase:Date samples were Checked-in: 3/9A.S By: ` 2 1: Were all sample containers listed on the COC received and intact? OP NA I 2: Sign the COC as received by En Chem. Completed '63 NO 3: Do sample labels match the COC? NO2 , 4: Completed pH check on preserved samples . YES NO 8 (This statement does not apply to water* VOC, O&G, TOC,DRO, Total Rec. Phenolics) 5: Do samples have correct chemical preservation? YES NO2 (This statement does not apply to water: VOC, O&G, TOC,DRO, Total Rec. Phenolics)YES NO2 6: Are dissolved parameters field filtered? 7: Are sample volumes adequate for tests requested? 4§11 NO2 I 8: Are VOC samples free of bubbles>6mm YES NO2 9: Enter samples into logbook.Completed g NO 10: Place laboratory sample number on all containers and COC. Completed lie NO I 11: Complete Laboratory Tracking Sheet(LTS). Completed YES NO I 12: Start Nonconformance form. YES NO NI 13: Initiate Subcontracting procedure. Completed YES NO 69 14: Check laboratory sample number on all containers and COC. 3 r 0 1 0 NO NA I Short Hold-time tests: . 24 Hours or less 48 Hours Ash days Footnotes 1 BOD 1 Notify proper lab group Corrosivity=pH Color Aqueous Extractable Organics-ALL immediately. Complete nonconformance Dissolved Oxygen Nitrite or Nitrate Flashpoint memo 2 Com p Hexavalent Chromium Ortho Phosphorus Free Liquids HPC Surfactants Sulfide Ferrous Iron Turbidity TDS Eh En Core Preservation TSS Odor Power stop preservation Total Solids Residual Chlorine TVS Sulfite TVSS Unpreserved VOC's Rev.2/05/04,Attachment to 1-REC-5. Reviewed by/date W 3111`cam I Subject to QA Audit. p:/everyone/forms/samplereceiving/crl.doc I